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A novel Pd/C catalyst with high activity,high selectivity and good stability developed by our group was used for the hydrogenation of N-(3-nitro-4-methoxyphenyl)acetamide into N-(3-amino-4-methoxyphenyl)acetamide in methanol and water,respectively.

笔者开发了一种高效的Pd/C催化剂,分别选用甲醇和水作为反应溶剂,实现了高活性、高选择性和高稳定性地催化加氢制备N-(3-氨基-4-甲氧基苯基)乙酰胺。

Analogous complexes 3a" and 4a"= CpRu(PPh32, Ar = para-C6H4OMe containing methoxy group at the para-position of gem-diphenyl group were similarly obtained from protonation of the corresponding acetylide complexes via formation of vinylidene intermediate. But only complex 3a'= CpRu(PPh32, Ar2 = fluorenyl is stable in solution, and decomposed to unidentified complex when heated to reflux in THF. Deprotonation of complex 4a in the presence of base gives neutral acetylide complex 6a.

在两个相邻位置的苯基对位位置上接有一甲氧基的衍生物3a"和4a"也可利用类似的质子化反应合成,唯有错合物3a'= CpRu(PPh32, Ar2 = fluorenyl 可以稳定於溶液中,不会进行上述反应,如将其溶於四氢呋喃溶液加热至沸腾则会分解产生无法鉴定的化合物。

A process for preparing alkylene glycols including reacting an alkylene oxide with water in the presence of a combination of additives and an anion exchange resin, wherein the combination of additives comprises carbon dioxide and an organic or inorganic base provided in an amount sufficient to maintain a pH of the reaction mixture between about 5.0 and 9.0, with the proviso that, when the base is bicarbonate or carbonate, then the anion exchange resin is a trimethyl benzyl ammonium anion exchange resin.

制备亚烷基二醇的方法,包括让烯化氧与水在添加剂组合和阴离子交换树脂存在下进行反应,其中添加剂组合包括二氧化碳和以足以保持反应混合物的pH值在约5.0和9.0之间的量提供的有机或无机碱,前提条件是当碱是碳酸氢盐或碳酸盐时,阴离子交换树脂是三甲基苄基铵阴离子交换树脂。

It contains formaldehyde, aluminum hydroxide, and 2-phenoxyethanol, a toxic chemical comparable to antifreeze.

包含了甲醛,铝的氢氧化物,以及2-含苯氧基乙醇,一种可以与防冻剂类比的有毒化学物质。

In this paper , two fluorocarbon amphoteric phosphate surfactants were synthesized and their performances were determined.

首先,磷酸二氢钠与环氧氯丙烷开环加成合成2-羟基-3-氯丙基磷酸酯钠,分离提纯后,分析其红外。

The two companies are integrated enterprises specialized in the production of spice, API, leather, building chemical products, and rubber. We have rich production experience, advanced production equipment, considerable technological force to produce products of top class quality. Our production and business concept is "service and credit first". We have invested 25 million RMB yuan in our companies and have totally 108 employees, 25% of whom are medium-level and senior technicians. We produce series products of Purple Mink brand including the spice: Raspberry ketone, Piperonal, Anisaldehyde, 99% isosafrole, 99% safrole; APIs: Diphenylmethanol, 4-Octyloxyphenol, 2,3-Dihydrofuran; leather chemical products: XD Alkaline chromium sulphate, XD Liming agent; building materials: productivity of 15000 tons of naphthalene series high-efficient high-concentration water reducing agent and 8000 tons of environment-friendly aliphatic water reducing agent; rubber chemical products: F101 Composite resin rubber sulfidizer. The annual sales amount is 80 million RMB.

本公司生产产品涉及香料、医药原料、皮革化工、建材化工、橡胶化工综合性化工企业,具有生产经验丰富、生产设备先进、技术力量雄厚、产品质量一流,服务、信誉第一的生产经营理念,资本投入2500万元,公司员工108人,各类中、高级技术人材占总人数的25%,生产的"紫貂"牌系列产品主要有香料类:覆盆子酮、洋茉莉醛、天然大茴香醛、99%异黄樟素、99%黄樟素,医药原料类:二苯甲醇、4-辛氧基苯酚、2,3-二氢呋喃,皮化类:XD碱式硫酸铬、XD浸灰助剂,建材化工类:萘系列高效、高浓减水剂15000吨、绿色环保型脂肪族减水剂8000吨的母体生产力,橡胶化工类:F101复合树脂橡胶硫化剂系列产品。

Under an atmospheric pressure of H2, the conversion of m-phenoxy benzaldehyde was beyond 99% after 12 h of reaction at 40℃.

以间苯氧基苯甲醛催化加氢反应为模型反应,研究了Pt和Pd金属纳米粒子的催化反应性能。

Mainly engaged in: Hydrogen-imide hydrochloride, o-chlorophenyl cyclopentanone, 3.4 dimethoxy ethyl benzene, butyn single potassium acid, potassium ethyl malonyl, Ding amide, amide isobutyraldehyde , allyl chloroacetate, isopropyl chloroacetate Benzyl aluminum, cyclopentene, cyanide-o-chlorophenyl, o-methyl chloride, sulfuric acid chloride, p-chlorophenol, imidazole, Pinacolone, one chlorine Pinacolone.

主要经营:盐酸氢亚胺、邻氯苯基环戊酮、3.4二甲氧基苯乙酯、丁炔二酸单钾盐、丙二酸单乙酯钾盐、丁酰胺、异丁酰胺、氯乙酸烯丙酯、氯乙酸苄酯异丙醇铝、环戊烯、邻氯苯氰、邻氯苯甲酯氯、硫酸氯、对氯苯酚、咪唑、频呐酮、一氯频呐酮。

In these complexes, there are hydrogen bond reciprocity between carboxyl groups and crystal lattice water molecules.

在这些配合物中,羧基氧、配位水分子和晶格水分子之间存在大量的氢键相互作用。

A series of pH- and temperature-sensitive hydrogels carrying pendant phosphategroups have been synthesized by copolymerizing 2-methacryloyloxyethyl dihydrogenphosphate with N-isopropylacrylamide. The swelling ratio, swelling and deswellingkinetics have been investigated. High loading percentage of lysozyme into hydrogelshas been achieved and the release profile has been studied.

通过N-异丙基丙烯酰胺和含磷酸基团的单体2-甲基丙烯酰乙氧基二氢磷酸酯的共聚合,合成了一类含磷酸基团的既对温度敏感又对pH敏感的水凝胶,研究了它们在不同pH及温度时的溶胀率及溶胀动力学,并初步研究了其对溶菌酶的释放行为。

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This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

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