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氧化滴定

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The results showed that the Mulberry fruit surface carried large numbers of yeast but little other mixed fungi; ethanol fermentation reached the peak value in 48h'; before vinegar production the acetification bed breeding took 9~10d, but the vinegar fermentation cycle was only about 24h during production .

结果表明,桑椹果实表面携带有大量的酵母菌而几乎不带其他杂菌,酒精发酵醪除含有大量的酵母菌之外未发现有其他杂菌,酒精度在发酵 48h 时达到高峰;桑椹醋生产前的醋酸菌床培育需要9~10d 时间,投入生产后醋酸发酵周期仅需要24h ;桑椹醋总黄酮含量高达6.68 mg/mL ,对 DPPH 自由基的清除作用远高于山西陈醋、镇江香醋和山楂果醋,具有良好的抗氧化作用;利用桑椹醋自身色素颜色变化可判断酸度测定时酸碱滴定终点。

The results showed that the mulberry fruit surface carried large numbers of yeast but little other mixed fungi; ethanol fermentation reached the peak value in 48h'; the acetification bed breeding took 9~10 d before vinegar production, but the vinegar fermentation cycle was only about 24h during production.

结果表明,桑椹果实表面携带有大量的酵母菌而几乎不带其他杂菌,酒精发酵醪除含有大量的酵母菌之外未发现有其他杂菌,酒精度在发酵48h时达到高峰;桑椹醋生产前的醋酸菌床培育需要9~10d,投入生产后酷酸发酵周期仅需要24h;桑椹醋总黄酮含量高达6.68mg/mL,对DPPH的清除作用远大于山西陈醋、镇江香醋和山楂果醋,具有良好的抗氧化作用;利用桑椹醋自身色素颜色变化可判断酸度测定时酸碱滴定终点。

The drying process of chrome liquor was studied. The structure and property of chrome complex reducing by alcohol were analysed and tokened by many present well-rounded separation and analysis methods such as IR, UV-Vis Spectrum, IEC and pH potentiometry. Application tests of chrome tanning agents were conducted and tanning methods of tanning at high pH were studied. A systematic study was conducted on high alkalinity chrome tanning agents application in leather making process and possibility of clean chrome tanning was discussed.

本文系统地研究了多种小分子醇与重铬酸盐之间的氧化-还原反应,对反应过程进行了认真的剖析;对铬鞣液的干燥过程进行了研究;用红外光谱法、紫外及可见分光光度法、离子色谱法以及pH电位滴定法等多种比较成熟的现代分离分析方法相结合,对醇还原铬配合物的结构与性能进行了分析与表征;对铬鞣剂的鞣革性能进行了应用实验,研究了醇铬鞣剂在高pH值下的鞣制方法,并就高碱度铬鞣剂在制革过程中的应用进行了系统研究,探讨了用其实施清洁化铬鞣的可能性。

The drying process of chrome liquor was studied. The structure andproperty of chrome complex reducing by alcohol were analysed and tokened by manypresent well-rounded separation and analysis methods such as IR, UV-Vis Spectrum,IEC and pH potentiometry. Application tests of chrome tanning agents wereconducted and tanning methods of tanning at high pH were studied. A systematic studywas conducted on high alkalinity chrome tanning agents application in leather makingprocess and possibility of clean chrome tanning was discussed.

本文系统地研究了多种小分子醇与重铬酸盐之间的氧化-还原反应,对反应过程进行了认真的剖析;对铬鞣液的干燥过程进行了研究;用红外光谱法、紫外及可见分光光度法、离子色谱法以及pH电位滴定法等多种比较成熟的现代分离分析方法相结合,对醇还原铬配合物的结构与性能进行了分析与表征;对铬鞣剂的鞣革性能进行了应用实验,研究了醇铬鞣剂在高pH值下的鞣制方法,并就高碱度铬鞣剂在制革过程中的应用进行了系统研究,探讨了用其实施清洁化铬鞣的可能性。

A method for the determination of potassium ferrate based on the oxidation of chromite was introduced in this paper.

以亚铬酸盐氧化还原反应为基础建立了高铁酸钾的滴定分析方法。

In the presence of the combination of sulphuric and phosphoric acid, with sodium diphenylamine sulfonate as the indicator, standard solution of potassium dichromate was used to titrate total iron value.

试样以盐酸溶解后,在酸性介质中,先以氯化亚锡将三价铁大部分还原为二价,然后在钨酸钠指示下,再以三氯化钛将剩余的三价铁还原为二价,过量的三氯化钛以重铬酸钾氧化消除干扰,在硫磷混合酸存在下,以二苯胺磺酸钠为指示剂,用重铬酸钾标准溶液滴定全铁量。

Amphoteric tapioca starch with carboxyl groups was produced via crosslinking, oxidation and etherization reactions. The product was then characterized by means of SEM, XRD and colloid titration, with the preparation mechanism being also investigated.

采用交联、氧化和醚化反应制备羧酸型两性淀粉,通过扫描电子显微镜、X射线衍射、胶体滴定等方法对该淀粉进行表征,并研究了该两性淀粉的合成机理。

After the solution was kept in the dark for five minutes,chloroform was added into it to adsorb selenium formed by previous reaction,then iodine separated out was determined by sodium hyposulfite titration using starch as the indicator,at last the content of selenium dioxide in the sample was foun.

在溶有二氧化硒的0.4~0.5mol/L盐酸介质中,加入过量的碘化钾,于暗处放置5min后,加入三氧甲烷吸附反应生成的硒,以淀粉为指示剂,用硫代硫酸钠标准溶液滴定析出的碘,测得二氧化硒的含量。

Antioxidant activity of extract of Eleocharis Tuberosa peel were studied by pyrogallol autoxidation method Feton reaction and Na2S2O-I2 titrimetric method.

用邻苯三酚自氧化法、Feton反应法、Na2S2O3-I2滴定法研究了荸荠皮提取物的抗氧化活性。

The kinetics of iridium catalyzed oxidation of isobutyl alcohol by cerium in aqueous sulphuric acid medium has been investigated by titrimetric technique in the temperature range of 25~40℃.

在酸性介质中用氧化还原滴定法研究了鈰离子在痕量铱离子催化作用下,於25~40℃区间氧化异丁醇的反应动力学。

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