氧化合物

Whenpyridine was used as reductive decomposing agent, the expecting cholest-4-en-3,6-dione-22-al was obtained. However, when Zn/HOAc was used to decomposethe ozonide, C-4,5 double bond was further reduced to give cholest-3,6-dione-22-al as main product. 2 For the side-chain construction of compound (1), the solid-liquid phase-transfer Wittig reaction was used. When (3-methyl-2-oxobutyl)-triphenylarsonium bromide was used as reagent, the reaction can be carried out inmild reaction condition and the yield is higher than that when phosphorane wasused.

但使用Zn／HOAc作为分解剂时，却得到其氢化产物胆甾-3， 6-二酮-22-醛；2在甾体支链引入过程中，采用固-液相转移Wittig反应的方法，用(3-甲基)-2-氧丁基三苯基溴化胂作为试剂，反应在非常温和的条件下便可完成，而且产率比传统采用膦烷的方法更高；3在对某些甾酮化合物的选择性还原反应研究时，发现在〓还原体系中，当加入某些金属离子后，反应有更好的区域选择性和立体选择性。

Solvent dosage is 10mL/ gram epichlorohydrin. The yield of 5-chloromethyl-2-oxazolidinone was more than 65.2%. 5-Chloromethyl-2-oxazolidinone and sodium phenolate were condensated to give 5-phenoxymethyl-2-oxazolidinone after taking off the sodium chloride in yield of 63.0%~78.0%. Dimethylsulfoxide was used as the solvent, and orthogonal experiment to the reaction condition had been carried out.

用5-氯甲基-2-噁唑烷酮和酚钠缩合，脱去氯化钠后生成5-芳氧甲基-2-噁唑烷酮类化合物，选用二甲亚砜为溶剂，对反应条件进行了正交实验，最佳条件为：反应温度120℃、反应时间20h、物料配比1：1，产率为63.0%～78.0%。

This proteolysis and anaerobic breakdown of proteins that yields foul -smelling amine compounds is called putrefaction.

蛋白水解及厌氧裂解会产生具有恶臭气味的胺类化合物的反应叫做腐败。

The design, synthesis, and angiotensin Ⅱ antagonist activities of several quinazolinone and quinazoline phenoxyphenylacetic acids are described.

本文设计、合成了一系列喹唑啉酮和喹唑啉苯氧基苯乙酸类化合物，并检测了它们的血管紧张素Ⅱ受体拮抗活性。

The five quinazoline compounds were prepared by using 2 amino 4,5 dimethoxy benzoic acid as original material, which underwent ring closing, halogenation and substitution.

以2 氨基 4，5 二甲氧基苯甲酸为原料，分别经过环化、氯代、取代等反应，合成了五种目标化合物。

Special attention was directed toward finding inhibitors selective against KDR tyrosine kinase in order to ensure that the in vivo profile of a specific Src inhibitor could be determined. The 4-aminobenzodioxole quinazoline series gave compounds with excellent potency and selectivity.

一直以来，人们为了确保能够在体内测定Src酶专属性抑制剂的特性，把研究焦点放在对KDR酪氨酸激酶选择性的抑制剂的寻找上。4-氨基苯并间二氧五环喹唑啉系列化合物具有极好的效力和选择性。

The fluorescent behaviors of different ruthenium complexes in solution and ormosil film were studied.

研究结果表明，在sol gel膜内，Ru化合物的荧光寿命都有不同程度的增加，同时对氧的猝灭程度增加。

F. Their structures were identified as betulone (1), 3,4,5-trimethoxyphenol-β-D-glucopyranoside (2),α-amyrin (3),β-amyrin (4),β-sitosterol (5), and stigmasterol (6) by spectroscopic evidence (IR, NMR, MS, etc.) and comparision of their spectral data with those of the literatures.

F。 的乙醇提取物中分离得到6个化合物，经波谱分析及与文献数据对照确定其结构分别为：betulone (1)、3，4，5-三甲氧基苯酚-β-D-吡喃葡萄糖苷(2)、α-香树脂醇(3)、β-香树脂醇(4)、β-谷甾醇(5)和豆甾醇(6)。

Results Seven known compounds: ocotillol (1), ursolic acid (2), betulin (3), lupeol (4), 1β-hydroxy-lupeol (5),β-sitosterol (6) and sitosterol-4-en-3-one (7) were isolated.

结果 分离得到7个化合物，分别鉴定为：20S，24R-环氧达玛烷－3β，25-二醇(ocotillol， 1)、熊果酸(2)、白桦脂醇(3)、羽扇豆醇(4)、1β-羟基羽扇豆醇(5)、β-谷甾醇(6)、谷甾－4-烯－3-酮(7)。

Result: Seven compounds were obtained and they are identified as luteolin, 5,7,4′-trihydroxy-3′-methoxy flavone, luteolin-7-O-β-D-glucoside, apigenin,β-sitosterol, stigmasterol, ursolic acid.

结果：从乙醇提取物中分离并鉴定了7个化合物，分别为：5 ，7，3′，4′-四羟基黄酮，5 ，7，4′-三羟基- 3′-甲氧基黄酮，5 ，3′，4′-三羟基黄酮- 7- O-β- D-葡萄糖苷，5 ，7，4′-三羟基黄酮，β-谷甾醇，豆甾醇和熊果酸。

She gently rebuff ed him, but agreed that they could be friends

她婉言拒绝了，但同意作为朋友相处。

If in the penal farm, you were sure to be criticized.

要是在劳改农场，你等着挨绳子吧！