氧化合物

Two compounds were isolated from ethyl acetate extract of the fermentation of fungus 07-11,which obtained from the soil of Yunnan Province. They were identified as N-(4-hydroxy-2-methoxyphenyl)acetamide (1) and ergosta-7,22-diene-3,6-dione (2) respectively on the basis of spectral analyses and physical and chemical identifications.

从云南土壤真菌07-11号菌株的发酵液乙酸乙酯萃取物中分离得到2个化合物，通过理化鉴别和光谱测定，鉴定两化合物分别为N-(4-羟基-2-甲氧苯基)乙酰胺(1)和麦角甾7，22-二烯-3，6-二酮(2)。

Covalent modification of four isolated alkannin derivatives (alkannin, acetylalkannin,β,β dimethylacrylalkannin and β acetoxyisovalerylalkannin, respectively) on rabbit muscle latate dehydrogenase and yeast Alcohol Dehydrogenase has been studied.

为研究紫草萘醌类化合物的细胞毒性作用机制，从新疆软紫草根中分离出四种紫草萘醌类化合物β，β二甲基丙烯酰阿卡宁(1)，乙酰阿卡宁(2 )，β乙酰氧基异戊酰阿卡宁(3)和阿卡宁(4)。

Nitrogen heterocyclics ; Oxygen heterocyclics ; Cobalt ; Ammine complexes

氮杂环化合物；氧杂环化合物；钴；氨络合物

The callus of barnyard grass was treated with compound 5 1-phenyl-4-(3,4-methylenedioxy-phenyl-diacetylene under UV-A irradiation for 3 h, which forms an inner environment of oxidizing stress in the cells.

摘 要：用多炔类化合物 1-苯基-4-（ 3 ， 4-亚甲二氧）-苯基丁二炔（简称化合物 5 ）处理稗草愈伤组织，经紫外光（ 320~400 nm ）照射后，诱导细胞内形成氧化胁迫环境。

METHODS 3-methoxy-7α-methylestra-1,3,5(10)-trien-17β-ol was reducted with lithium and ammonia,then the intermediate was hydrolyzed in oxalic acid and reacted with malonic acid to get 3,3-dimethoxo-7α-methylestra-5(10)-en-17-ol(compound 4),which was oxidated by pyridium bichromate ,reacted with acetylene,and hydrolyzed in oxalic acid again to get the product tibolone.

方法以3-甲氧基-7α-甲基雌甾-1，3，5(10)-三烯-17β-羟基为起始原料经锂胺还原、草酸水解、缩酮化得3，3-二甲氧基-7α-甲基雌甾-5(10)-烯-17β-羟基(化合物4)，然后用温和的氧化剂重铬酸吡啶盐氧化、炔化、再水解得目的产物。

AIM:To assess the antioxidative activity of a new cyclic diaryheptanoid (compound 1) from ginger on free radical damage. METHODS:Hemolysis, MDA levels of mice liver tissue homogenates, the conformation changes of irradiated PUC18 were used as indices.

目的和方法：采用溶血实验，小鼠肝组织脂质过氧化物测定，采用受辐射质粒构象改变等方法测定从生姜中分离得到的一新的环状二苯基庚烷类化合物(化合物1)的抗氧自由基损伤活性。

They had suppressed the cathodic process of carbon steel electrode. Their inhibition performance was also related with their molecule stereo conformation and electron configuration. Four of bis-(1, 1'-benzotriazoly)-α,β-diamide compounds linked via-CO 〓CO-chain were synthesized and certified by IR and 〓H-NMR. The minimum energy conformations of these compounds were obtained by MM2 forcefield program. The two benzotriazole moiety in BBT1 was more planar than in other compounds. This was beneficial in increasing the inhibition effects of BBT1. In 0.5M H〓SO〓 solution, BBT1 suppressed anodic corrosion reaction. In 3%NaCl solution, BBT1 suppressed both cathodic and anodic corrosion reactions. 1- [ (1'-imidazolly)-methyl] benzotriazole was synthesized by Mannich reaction.

合成了四个通过-CO〓CO-连接的双（1，1'-苯并三唑）-α，ω-二酰胺化合物，采用MM2分子力学程序优化了它们的分子结构，双（1，1'-苯并三唑）-α，ω-二酰胺化合物的缓蚀作用与其分子内两个苯并三唑单元的空间取向有关系，良好的平面性有利于苯并三唑二聚体的吸附和缓蚀作用，苯并三唑二聚体BBT1分子内两个苯并三唑单元近似平行，所以显示出较好的缓蚀效果。0.5M硫酸中BBT1主要抑制铜的阳极溶解的电化学反应；3％NaCl溶液中，BBT1对铜的阳极溶解和氧的阴极还原过程均有抑制作用，相比较而言对阴极过程的抑制作用更大一些。

The invention relates to a continuous method for the intermediate separation of the oxirane produced by the reaction of a hydroperoxide with an organic compound, characterised in that the product mixture generated during the synthesis is separated in a partition-wall column into a low-, middle and high-boiling fraction and the oxirane is taken off with the middle-boiling fraction at the side tap point of the column and the hydroperoxide is taken off with the high-boiling fraction from the bottom of the column.

一种对在环氧烷合成中通过氢过氧化物与有机化合物反应形成的环氧烷进行中间分离的连续方法，其中在隔离壁塔中将该合成中形成的产物混合物分馏得到低沸点馏分、中间沸点馏分和高沸点馏分，并在侧线采出处从中间沸点馏分中取出所述环氧烷，在该塔的底部从高沸点馏分中取出所述氢过氧化物。

By further comparing the retention time of the profounds and that of the impurities,the main impurities in triadimefon technical was conformed as following:First, 1-(4-bromophenoxy)-3,3-dimethyl-1 -(1H-1,2,4-triazol-1 -yl)-2-butanone;Second, 1-(2,4-dichlorophenoxy)-3,3-dimethyl-1 -(1H-1,2,4-triazol-1 -yl)-2-butanone;Third, 1,1 -bis(4-chlorophenoxy)-3,3 -dimethy 1-2-butanoneour conclusion is conformed right.

再经过化合物的保留时间与杂质保留时间的比照，证实了三唑酮原药中的主要杂质是：杂质Ⅰ：1-(4-溴苯氧基)-3，3-二甲基-1-(1H-1，2，4-三氮唑-1-基)-2-丁酮；杂质Ⅱ：1-(2，4-二氯苯氧基)-3，3-二甲基-1-(1H-1，2，4-三氮唑-1-基)-2-丁酮；杂质Ⅲ：1，1-二(4-氯苯氧基)-3，3-二甲基-2-丁酮。

The flame-retardant/smoke-suppressant of PVC may be divided into three kinds. The first is FRs , includes the compounds lying in IVB～VIB, such as TiO〓, V〓O〓, Cr〓O〓 and MoO〓; The second is FRs , includes the compounds lying in VⅡB～IB, such as MnO〓, Fe〓O〓, Co〓O〓, CuO and ZnO. The third is FRs , includes the compounds of subgroup A, for example Mg 〓, Al 〓, Sb〓O〓, carbonate and phosphate.

PVC的阻燃抑烟剂可分为三大类，第一类阻燃抑烟剂为元素周期表中IVB～VIB族的化合物，以TiO〓，V〓O〓，Cr〓O〓和MoO〓为代表，第二类阻燃抑烟剂为元素周期表中VⅡB～ⅡB族的化合物，以MnO〓，Fe〓O〓，Co〓O〓，CuO和ZnO为代表，第三类阻燃抑烟剂为三氧化二锑，氢氧化镁，氢氧化铝等主族元素的化合物。

She gently rebuff ed him, but agreed that they could be friends

她婉言拒绝了，但同意作为朋友相处。

If in the penal farm, you were sure to be criticized.

要是在劳改农场，你等着挨绳子吧！