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氧化乙酰

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BACKGROUND AND AIM: To study the effects of acephate on oxidative damage and ovarian function in female rats.

背景与目的:研究乙酰甲胺磷对雌性大鼠氧化损伤及卵巢功能的影响。

Our use Co2 as a catalyst in this work, exploring new way to produce nitrobenzoic acid from nitrotoluene under the prue oxygen in basic medium.

本文探讨了以乙酰丙酮钴为催化剂,分子氧为氧源,在NaOH-CH_3OH的反应环境下,氧化硝基甲苯制备硝基苯甲酸的新方法。

In the experiment,glass chest was used to simulate indoor roomage environment.The formaldehyde concentration in the simulative room was measured by the method of acetyl acetone with spectrophotometer.

实验以玻璃箱模拟室内空间环境,应用乙酰丙酮分光光度法和邻苯三酚自氧化法测定在不同甲醛含量下芦荟对甲醛的吸收及其体内过氧化物酶活性的变化情况。

Objective To explore the effect on the capability of antioxidizing in testis of male rats.

目的 探讨乙酰甲胺磷对雄性大鼠睾丸组织抗氧化能力的影响。方法 24只健康成年SD雄性大鼠,随机分为4组,每组6只。

Objective To explore the effect on the capability of anti-oxidizing in testis of male rats.

目的 探讨乙酰甲胺磷对雄性大鼠睾丸组织抗氧化能力的影响。方法 24只健康成年SD雄性大鼠,随机分为4组,每组6只。

The synthesis of nalbuphine hydrochloride from thebaine as starting material was through following processes:oxidation,high-pressure hydrogenation,acetylation,removing methyl of 3-methoxy,hydrolysis,condensation,reduction and finial salification.

以蒂巴因为起始原料,经氧化、高压氢化、乙酰化、氰化、脱3-位甲氧基的甲基、水解、缩合、还原、成盐,合成了盐酸纳布啡,总收率达18。

Permethylation analysis, periodate oxidation,Smith degradation, acetolysis and partial acid bydrolysis revealed the main chains of XP as mannose of (1-6)-linkages and its side chains were mannose of (1-2)linkages.

甲基化分析、过碘酸盐氧化、Smith降解、乙酰解和部分酸水解显示XP的主链是1→6连接的甘露糖,侧链是1→2连接的甘露糖。1H及13CNMR谱表明所有糖苷键均为a型,结合元素分析XP基本是酵母甘露多糖和蛋白质以及锌的络合物。

Their structures were detailedly identified on the basis of chemical methods (sugar composition analysis, glycosyl residue linkage analysis, partial acid hydrolysis, periodate oxidation, Smith degradation, acetolysis, Congo Red experiment, etc.), spectral technologies 1D, 2D NMR, ESI-MS, IR, etc.

通过各种化学方法(糖组成分析,糖残基连接方式分析,部分酸水解,高碘酸氧化,Smith降解,乙酰解,刚果红实验等)、光谱方法(1D、2DNMR,ESI-MS,GC-MS,IR等)和物理化学方法(分子量分析,粘度分析,旋光度分析等)对各纯化多糖的化学结构及糖链构象进行了鉴定。

Supporting the acetylacetone on ionic liquid was established for the purpose of catalyst recycling. The following works focused on what kind of supporting methods can enhance the catalytic ability of acetylacetone.

从提高催化剂可回收性方面考虑,论文计划将乙酰丙酮支载在离子液体上,接下来研究采用怎样的离子液体如何支载能够提高催化剂的催化氧化活性。

The first asymmetric synthesis of trans-β-hydroxy-γ-butyrolactones:-(3R, 4R, 5S)-4-(1-acetoxy-isopropyl)-3-hydroxy-butyrolactone 65a was achieved starting from isobutylaldehyde through nine steps. The key steps involve the construction of three chiral carbon centers by the Sharpless's asymmetric epoxidation and Substrate directable chemical reaction.

以异丁醛为起始原料,经过九步反应首次设计合成了具有三个手性中心的trans-β-羟基-γ-丁内酯:-(3R,4〓,5S)-4-(1-乙酰氧基-异丙基)-3-羟基-丁内酯65a,关键步骤是Sharpless不对称环氧化和底物定向不对称合成反应。

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