氧化乙酰

In this dissertation, the stable radical cation salts ofphenothiazine and 10 - alkylphenothiazine alky=〓(〓 hexachloroantimonate,perchlorate and iodide were prepared by one- electron oxidationwith 2,2,6,6-tetramethyl - 4 -acetyloxypiperidine oxoammoniumhexachloroantimonate, perchloric acid/hydrogen peroxide andmolecular iodine respectively, and they were characteried by UV -Vis spectroscopy and ESR spectroscopy.

本文的主要内容有：吩噻嗪和10-烃基吩噻嗪分别被碘、高氯酸／过氧化氢，2，2，6，6-四甲基-4-乙酰氧基哌啶氧铵六氯锑酸盐氧化为相应的正离子自由基碘盐、高氯酸盐、六氯锑酸盐，并用UV-Vis光谱和ESR波谱进行了鉴定和研究。

The method controls the catalytic speed of the microencapsulation glucose oxidase through adjusting the molecular weight and the degree of deacetylation of microcapsule exine chitose, thereby the method is beneficial for oxidation-linking of gluten protein and for increasing the quality of the flour and flour products, simultaneously, the glucose oxidase after microencapsulation avoids the contact between enzyme and the flour and improves storage and the stability, and the microencapsulation glucose oxidase is excellent flour modifying agent and accords with practical production and application.

该方法通过调节微胶囊外壁壳聚糖的分子量和脱乙酰度，控制微胶囊内葡萄糖的催化速度，从而有利于面筋蛋白的氧化交联，提高面粉及其制品的品质；同时葡萄糖氧化酶经微胶囊化以后避免了酶与面粉的接触改善了贮藏和稳定性，是优良的面粉改良剂，符合实际生产应用。

The Nterminal cyclization of peptides, as one of a variety of modification introduced in sample preparation, has been preliminarily studied in this work.

目前，肽段鉴定时常用的添加残基修饰有甲硫氨酸的氧化和半胱氨酸的氨乙酰化，而对其它修饰研究很少。

These results show the level of diacetyl produced in Enterobacter aerogenes UV-3 would be dependent on the nonenzymatic oxidative decarboxylation of ALA.

通过主要代谢酶的酶学性质分析，确定产气肠杆菌突变株UV-3积累丁二酮的代谢途径是由α-乙酰乳酸的非酶氧化直接生成。

In young human umbilical vein endothelial cells, human aortic endothelial cells, and human coronary artery endothelial cells, miR-217 induces a premature senescence-like phenotype and leads to an impairment in angiogenesis via inhibition of SirT1 and modulation of FoxO1 (forkhead box O1) and endothelial nitric oxide synthase acetylation.

在婴儿脐静脉内皮细胞、人类主动脉内皮细胞以及冠状动脉内皮细胞中，miR-217可以诱导这些细胞出现一种早衰样表型，进而通过抑制SirT1的表达、调控Fox01以及内皮细胞一氧化氮合酶的乙酰化来损伤新生血管的形成。

The GV should be sprayed in the peak period of the eggs and the low instar larvae.

喷布的雾滴细，可以提高防治效果。病毒与乐果、氧化乐果、乙酰甲胺磷等农药临时混用。

Instructed by this method, the structure-reactivity relation of the oxidation reaction catalysts was found and a way was proposed to enhance the catalytic ability of traditional acetylacetone catalysts by supporting them on ionic liquid.

在该方法的指导下，发现了氧化催化剂结构活性关系，提出了一套用离子液体支载来提高乙酰丙酮金属催化剂催化氧化活性的方案。

These new ionic liquid-supported acetylacetone catalysts were used for the oxidation of the intermediates of Vitamin E (2,3,5-trimethylphenol and 3,5,5-trimethylcyclohex-3-en-l-one). It not only checked the rationality of the design, but also established the base for the green oxidation of corresponding reactions.

论文进一步将此类离子液体支载乙酰丙酮金属催化剂应用于维生素E中间体三甲基苯酚和β—异佛尔酮的氧化过程，一方面检验了催化剂设计过程及结果的可靠性，另一方面为相关氧化反应的绿色化改造提供相关的基础。

Synthesis 3,5-dihydroxytoluene by ethyl acetoacetate and diketene as material(yield 6%),by 3-methyl-4-chlorophenol and KOH as material(yield 30-40%)respectively,It was solved for product separation and purify.

分别以乙酰乙酸乙酯与双乙烯酮为原料(收率6%)、3-甲基-4-氯苯酚与氢氧化钾为原料(收率30-40%)合成了3，5-二羟基甲苯，解决了产品分离纯化问题。3-甲基-4-氯苯酚路线进行了中试，中试收率为20%。

Structures of glycosyl ester of 13-cis-4-restinoic acid(5) and 6 were characterized by 1H NMR,13C NMR,IR and MS and confirmed to be β-configuration.

13-顺维甲酸与溴代-2，3，4，6-四-O-乙酰基-α-D-吡喃葡萄糖在4-二甲氨基吡啶催化下合成了13-顺维甲酸葡萄糖酯(5)，以二氧化锰为氧化剂，5经氧化成功地合成了新化合物13-顺-4-羰基维甲酸葡萄糖酯(6)。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。