氧丙环

In this paper , two fluorocarbon amphoteric phosphate surfactants were synthesized and their performances were determined.

首先，磷酸二氢钠与环氧氯丙烷开环加成合成2-羟基-3-氯丙基磷酸酯钠，分离提纯后，分析其红外。

Three ways leads to the synthesis of fenclorin, one way discussed here has 3 steps. Stepl :benzonitrile using as raw material goes though dry hydrogen chloride and becomes a-imino phenylmethyl ether after meet carbinol.

解草啶的合成主要有三条路线，本文选取合成路线是以苯甲腈为原料，经三步反应而成：1、苯甲腈在干燥的氯化氢通入，与甲醇形成亚氨基苯甲醚，通入氨气后置换甲氧基得到苯基脒盐酸盐(收率76.18%)。2、苯基脒盐酸盐在碱性条件下与丙二酸二乙酯环合而得嘧啶醇(收率84.39%)。3、嘧啶醇在三氯氧磷中羟基被氯化得到产品解草啶(收率87.29%)。

Products has led caprate cobalt, cobalt naphthenate, TY series of high-performance polyimide resin, FLQ type latent epoxy curing promoting agent, diallyl bisphenol A Product dozens of top-five.

主导产品有癸酸钴、环烷酸钴、TY系列高性能聚酰亚胺树脂、FLQ型潜伏性环氧固化促进剂、二烯丙基双酚A五大类数十种产品。

The intermediate of flazasulfuron weedicide ,2-amino-4,6-dimethoxypyrimidineis conveniently obtained by treating 2-amino-4,6-dihydroxypyrimidinewith diazomethane at 20 °C for 24h.

本文利用硝酸胍和丙二酸二乙酯为起始原料，经环合及甲氧基化两步反应得到除草剂啶嘧磺隆的中间体：2-氨基-4，6-二甲氧基嘧啶。

Cyclization: cyclization occurs at 100℃in polyphosphoric acid for 4h in the mass ratio of 3-(4-methoxyanilino) propionic acid to PPA with 1:8, and 6-methoxy-2,3-dihydro-4-quinolone is formed in 50.5% yield with a method of rapid chromatographic column, c.

成环反应：质量比[3-(4-甲氧苯氨基)丙酸∶多聚磷酸]=1∶8，反应温度为100℃，反应时间4h，柱层析纯化后6-甲氧基-2，3-二氢-4-喹啉酮的收率为50.5％；c。

By using tetramethylammonium hydroxide as catalyst, a new silicone, amino and long-chain alkyl co-modified polysiloxanes was synthesized by bulk polymerization of octamethylcyclotetrasiloxane (D4), N-β-aminoethyl-γ-aminoproylmethyldimethoxysilane (YDH-602), dodecylmethyldimethoxysilane (HD-109) and hexamethyldisiloxane. The optimum experimental conditions were studied.

以八甲基环四硅氧烷(D4)、长链烷基甲基二甲氧基硅烷(HD-109)、N-β-氨乙基－γ-氨丙基甲基二甲氧基硅烷(YDH-602)和六甲基二硅氧烷为原料，在四甲基氢氧化铵催化下，采用本体聚合反应合成了一种新型硅油－氨基与长链烷基共改性硅油。

Bezaldehyde was used as protective agent in first method.S-Epichloeohydrin was aminated and acidulated to give(2S)-1-Amino-3-chloro-propanol Salts.The acetylation of (2S)-1-Amino-3-chloro-propanol by acetic anhydride produced the intermediate-N-[2--3-chloropropyl]acetamide.And then at 20℃,in the presence of lithium tert-butoxide,benzyl 3-fluoro-4-morpholinophenyl carbamate react with-N-[2--3-chloropropyl]acetamide to give linezolid in total yield of 43.6%.

路线一采用苯甲醛作保护剂，使S-环氧氯丙烷氨解、酸化生成S-1-氨基-3-氯-2-丙醇盐酸盐，然后经乙酰化反应后，生成中间体-N-[2-乙酰氧基-3-氯丙基]乙酰胺，再用N-(3-氟-4-吗啉苯基)氨基甲酸苄酯和中间体在催化剂叔丁醇锂存在下25℃反应生成利奈唑酮，总产率达到43.6%。

Intend to use the most advanced technologies in building the 20,000 t/y propylene oxide plant, hydrogen peroxide and propylene as raw materials. Process control using phase transfer catalyst reaction of propylene oxide technology, non-polluting, non-joint products.

拟采用国内先进技术建设2万吨/年环氧丙烷生产装置，以双氧水和丙烯为主要原料，生产工艺采用反应控制相转移催化丙烯氧化技术，无污染、无联产品。

E. . The epoxidation of cis-allylic alcohols is difficult, and with 20％mol Ti 〓 and 30％mol tartrates, up to 80％e.

的对映选择性被得到；对难于环氧化的顺式烯丙基醇，使用20％mol四异丙氧基钛和30％mol酒石酸酯得到最高80％e.e。

ABSTRACT: In the presence of sodium t-butoxide and DMSO,ethyl 2-oxocyclopentanecarboxylate was subjected to C-alkylation with 2-(4-bromomethylphenyl)propanoic acid with high regioselectivity to give 2-［4-(1-ethoxycarbonyl-2-oxo-1-cyclopentanylmethyl)phenyl］propanoic acid (4) which was followed by hydrolysis,decarboxylation and salt formation to afford loxoprofen sodium in about 72% overall yield.

在叔丁醇钠和二甲基亚砜的存在下，2-丙酸对2-乙氧羰基环戊酮进行C-烷基化，再经水解脱羧，成盐即得洛索洛芬钠，以2-丙酸计算，总收率为72%。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。