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In the process, 2, 4-difluoroaniline is used to carry out ammoniated reaction. Then through a series of similar reactions, the important intermediate of temafloxacin, which is called 7-chloro-6-fluoro-1-(2, 4-difluorophenyl)-1, 4-dihydro-4-oxo-3-quinoline acid, is gained.

与环丙沙星和二氟沙星类似,用2,4-二氟苯胺进行胺化反应,再进行一系列类似的反应,制得合成替马沙星的关键中间体7-氯-6-氟-1-(2,4-二氟苯基)-1,4-二氢-4-氧代喹啉-3-羧酸。

Chloro 2 hydroxypropyl trimethyl ammonium chloride an etherizing agent ,for modified starch, was synthesised from epichlorohydrin.

以环氧氯丙烷为原料合成了 3-氯- 2 -羟丙基基三甲基氯化铵,后者作为改性淀粉的醚化剂。

Terpolymer of acrylic acid/acrylic amide/malefic anhydride was synthesized and mixed with polyepoxysuccinic acid in order to improve the scale and corrosion performance of the latter in this study.

为了提高PESA的阻垢缓蚀性能,合成了丙烯酸/丙烯酰胺/马来酸酐三元共聚物,与聚环氧琥珀酸进行物理复配,考察了温度、反应物配比及浓度对复配产品阻垢和缓蚀性能的影响。

A method for the simultaneous analysis of 19 quinolone residues, enrofloxacin, ciprofloxacin, norfloxacin, ofloxacin, difloxacin, oxolinic acid, flumequine, sarafloxacin, sparfloxacin, danofloxacin, fleroxacin, marbofloxacin, enofloxacin, orbifloxacin, pipemidic acid, pefloxacin, lomefloxacin, cinofloxacin, and nalidixic acid in honey was developed by high performance liquid chromatography-tandem mass spectrometry. In comparison of the three different extraction methods, i.e.

建立了高效液相色谱-电喷雾串联质谱联用测定蜂蜜中恩诺沙星、环丙沙星、诺氟沙星、氧氟沙星、双氟沙星、恶喹酸、氟甲喹、沙拉沙星、司帕沙星、丹诺沙星、氟罗沙星、马波沙星、伊诺沙星、奥比沙星、吡哌酸、培氟沙星、洛美沙星、西诺沙星和萘啶酸等19种喹诺酮类药物残留的方法。

a simple and accurate method is established for determination of ciprofloxacin in oxygen flask combustion method

氧瓶燃烧法定量准确、灵敏度高,可作为测定环丙沙星含量的一种新方法。

This novel reagent was treated with LDA to produce polystyrene-supported a-seleno carbanions, which reacted with alkyl halides and epoxides, followed by stereospecific selenoxide syn-elimination to give olefins and allylic alcohols respectively.

它与LDA反应形成α—硒基稳定的碳负离子,再与卤代烃或环氧化合物发生α—烷基化反应,烷基化后的树脂可以在30%的双氧水中进行氧化-消除,以良好产率和较高纯度合成了取代烯烃或烯丙基醇。

By synthesizing the hapten LBc starting from the metabolite of bifenthrin (2-methyl-3-phenylbenzyl alcohol), LBs (2-methyl[1,1-biphenyl]-3-ylmethyl 3-carboxyl-2,2-dimethylcyclopropane carboxylate and Lby (2-methyl[1,1-biphenyl]-3-ylcarboxylic acid , Three haptens were praparaed which were used in next step.

利用联苯菊酯的代谢物联苯醇合成了联苯菊酯的半抗原LBc(2-甲基-3-苯基苄基氧基羰基丙酸)、LBs(2-甲基-3-苯基苄基-3-羧基一2,2-二甲基环丙烷羧酸)和LBy(2-甲基-3-苯基苯甲酸)。

Three standard and two isolated strains of E.coli were used for drug sensitivity test on Chloramphenicol, Ciprofloxacin Lactate, Rifampicin, sulfamonomethoxine, Florfenicol, Ceftiofur Sodium as well as the antimicrobial synergists sulbactam sodium and TMP. The bacteriostasis results of the antibiotics against E.coli In vitro were compared when they were used separately or combined with the synergist.

试验用3株大肠杆菌标准株和2株地方分离株,选择氯霉素、乳酸环丙沙星、利福平、磺胺-6-甲氧嘧啶钠、氟苯尼考、头孢噻呋和抗菌增效剂舒巴坦钠、TMP进行药敏试验,比较几种药物单一或与增效剂合用对大肠杆菌的体外抑菌效果。

The results showed that:(1) The drug micropellet with reasonable drug entrapment ratio and release velocity would be obtained if the amountof crosslinking agent and drugs was controlled successfully;(2) The Ibuprofen micropellet had a suitable release rate in artificial intestinal juice but it was a very low release rate in artificial succus gastrius because it had a low solubility in acid medium.

以环氧氯丙烷为交联剂,羟丙基壳聚糖为载体,将布洛芬做成缓释控释药物微丸,讨论了包埋条件对微丸性能的影响以及药物在人工胃液和人工肠液中的释放行为。结果表明:(1)合理控制交联剂用量和药物投入量,能够得到药物包封率和释放性能良好的药物微丸;(2)布洛芬药物微丸在人

A novel hydroxyl terminated aminosilicone oil was synthesized using octamethylcyclo tetrasiloxane (D4) and the hydrolysis product of γ-piperazinepropylmethyldimethoxysilane (HD-110) as raw material and potassium hydrate as catalyst.

以八甲基环四硅氧烷(D4)、γ-哌嗪基丙基甲基二甲氧基硅烷(HD-110)水解物为原料,在氢氧化钾催化下,制备了羟基封端的新型氨基硅油。

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This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。

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双标记神经干细胞的增殖、分化活力与未标记神经干细胞相比无改变。