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These data were used to infer the molecular formula and the elemental compositions of all the fragmental ions through software interpretation and, by further applying fragmentation regularities of mass spectrometry, the majority of ions were fully assigned. A base peak at m/z 402 in the mass spectrum was found as the molecular ion. The fragments were created mainly from the fragmentations of the tetrahydrofuran rings and the hydroxyl group. The most fragment products contain the dimethoxy phenyl group.

利用这些数据通过软件导出了分子式和所有碎片离子的元素组成,由此进一步根据质谱裂解规律对石梓醇分子的电子轰击质谱的主要裂解碎片给出了完全的归属,质谱中发现基峰为分子离子峰(m/z402),裂解碎片主要来自双骈四氢呋喃环的裂解和羟基引起的裂解,绝大部分裂解产物包含二甲氧基苯基基团。

The disubstituted ureas and the catalyst could be separated by addition of water and the catalyst could be reused without deactivation.

新型高效的菲咯啉钯-离子液体含氮化合物羰化催化剂体系,以苯胺为反应物时该体系的转化频率可以达到6000mol/mol/h;氢氧化铯-离子液体催化剂体系,可以在不加入化学计量脱水剂的条件下活化二氧化碳与脂肪族胺反应得到二取代脲,反应结束后可以通过加入水实现产品和催化剂体系的分离,催化剂体系可以重复使用。

YTY paper reinforcement of the recently developed a new water soluble polymer material, it is a high molecular weight polymer compound ionictype, mechanim, numberrepresentationof exesting non-ionic, and numberrepresentationof anions and cations, so this in paper-making process, you can and pulp fiber molecules multi-spots adsorption, which increases the fine celluiose filler and retention; at the same time it can also promote hydrogen between cellulose, and gives the paper jiantiao dry strength significantly increase, because the reinforcement of the unique structure, so it can be used with other paper cocatalyst compouding, a broad pH range as a reinforcement of the paper is available at wood pulp and wood pulp-straw gamasid mixed pulp and paper pulp etc.

YTY纸张补强剂系近期研制成功的新型水溶性高分子材料,它是一种高分子量复合离子型的高聚物,在其分子结构中,既有非离子基团,还有阴离子、阳离子基团,因此这在造纸过程中,可以与纸浆中的纤维分子形成多点吸附,从而提高填料与细纤维素的留着率;同时它还可促进纤维素分子之间的氢健作用,使纸张干强度明显提高,由于该补强剂分子的独特结构,因此它可与其它造纸助剂复配使用,能在较宽广的pH范围内,作为纸张补强剂,可以在木浆、木浆——草浆混合浆、革浆等多种纸浆中使用。

A method for the determination of Acetic acid and Hydrobromic acid in air and environmental sample by ion-chromatography is described.

用同一吸收液采集、离子色谱法测定空气中的乙酸和溴化氢,采样体积为60L时,乙酸和溴化氢的检出限分别为0.03mg/m3和0.11mg/m3,相对标准偏差分别为1.9%和1.7%,实际样品的加标回收率分别为90.1%~102%和

The comparisons of electron ionization energies, ionic total energies and electron transition energies calculated respectively by More, Faussurier and the relativistic screened hydrogenic models, have been performed and the precisions of these physical quantities verify the preponderance of the relativistic screened model based on the analytical potentials.

与More和Faussurier屏蔽类氢模型比较,在电子电离能、离子总能量和电子跃迁能量的计算结果精度方面,基于解析势的相对论性屏蔽类氢模型占有优势。

On the basis of the preparation of special-grade sodium hypophosphite by one-step method in the high-speed reactor,the produced sodium hypophosphite and the byproduct calcium phosphite were further converted to higher-purity hypophosphorous acid and phosphorous acid products by ionic membrane electrodialysis.

在作者开发的高速反应器一步法制专用级次磷酸钠的基础上进一步将生成的次磷酸钠和副产的亚磷酸氢钙用离子膜电渗析法制成纯度更高的次磷酸及亚磷酸产品,产品质量升级,回收利用了副产亚磷酸氢钙,并减少了原料烧碱的用量。

It results from theformation of infusible salt or hydrates by the complexing reaction of metal ion andnegative ions in alkaline solution. The stability mechanism was discussed byemploying scanning electronic microscope and x ray photoelectronspectroscopy.

结果表明,在中性介质中,其稳定性较好,而在碱性介质中的稳定性较差,这是因为在碱性介质中金属离子与介质中的阴性离子络合形成难溶性的盐或氢氧化物,加速了GIC的分解所致。

A mild and convenient method for the synthesis of 4(3)-substituted 3(4)-nitro-1H-pyrroles and 3-substituted 4-methyl-2-tosyl-1H-pyrroles from nitroolefins and tosylmethyl isocyanide in ionic liquid 1-butyl-3- methylimidazolium bromide was developed.

本文以离子液体-溴化1-丁基-3-甲基咪唑为溶剂,采用对甲苯磺酰基甲基异腈与硝基烯反应生成4(3)-取代-3(4)-硝基-1-氢吡咯或3-取代-4-甲基-2-对甲苯磺酰基-1-氢吡咯。

The hepatic glycogen and the activities of ACP, LDH, returned to normal at 7th postoperative day in the Labiatae group.

3丹参组术后3天琥珀酸脱氢酶、镁离子激活三磷酸腺苷酶、葡萄糖-6-磷酸酶活性升高,术后7天肝糖原和乳酸脱氢酶、酸性磷酸酶活性回到正常水平。

Results show that the adoption of stainless steel anode wrapped with anion membrane improves the bath stability and avoids the oxidation of manganous ions.

结果表明:采用不锈钢阳极和阴离子膜可提高镀液稳定性,防止二价锰被氧化,加入氢氧化钡可消除因补充锌锰离子而积累的硫酸根离子。

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