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①postoperative pain after hemorrhoidectomy can be safely and effectively controlled by Acuepoint inject of lappaconitine hydrobromide ②Using the Ashi-points-injection of lappaconitine hydrobromide after hemorrhoidectomy can reduce the pain for a longtime ③Combined with Yaoshu-point-injection can enhance the anaesthetic effect at the day of surgery④The edema at anal margin can be reduced by using of Ashi-points-injection of lappaconitine hydrobromide

①穴位注射氢溴酸高乌甲素对痔术后镇痛是安全而有效的;②术毕时使用氢溴酸高乌甲素阿是穴注射具有术后长效镇痛作用;③联合使用氢溴酸高乌甲素腰俞穴注射可增强手术当天的镇痛效果;④氢溴酸高乌甲素穴位注射具有防止痔术后肛缘水肿的作用。

In this paper, initiator is dissolved in 1-bromopropane which is solvent. Then the propene and hydrogen bromide that can be dissolved in 1-bromopropane are inlet in l-bromopropane when initiator is decomposing. The reaction occurs in fluid phase and high-purity 1-bromopropane is synthesized by one step method. In this paper, the material HBr is synthesized with NaBr and sulfuric acid at the presence of hydrobromic acid.

本论文以1-溴丙烷为溶剂,将引发剂溶于其中,加热到引发剂开始分解时再通入丙烯和HBr,使二者溶解于1-溴丙烷中,在液相中进行反应,实现丙烯"一步法"合成高纯1-溴丙烷利用NaBr与硫酸在氢溴酸存在下反应制备HBr气体,以作为合成1-溴丙烷的原料。

The main products are: calcium sulfate / calcium nitrate / calcium carbonate / copper sulfate / chloride, copper / zinc sulfate / nitric acid zinc / zinc chloride / potassium sulfate / potassium chloride / potassium bromide / potassium aluminum sulfate / potassium dihydrogen phosphate / 2 of potassium hydrogen phosphate / sodium bromide / sodium chloride / sodium nitrate / sodium fluoride / trisodium phosphate / sodium dihydrogen phosphate / disodium hydrogen phosphate / crystallization of sodium carbonate / anhydrous sodium carbonate / aluminum sulfate / nitrate aluminum / crystallization of aluminum chloride / aluminum hydroxide / nitrate Fe / hydrobromide / oxalic acid / boric acid / citric acid / barium chloride / Azone / magnesium sulfate / magnesium nitrate / magnesium chloride / ammonium chloride / ammonium sulfate / Bifluoride ammonium / ammonium aluminum sulfate / ferrous ammonium sulfate / ammonium dihydrogen phosphate / diammonium hydrogen phosphate / bromide / tetrabutylammonium bromide / chloride, nickel / nickel nitrate / sulfate nickel / cadmium chloride / cadmium sulfate / nitrate Cadmium / Cadmium Carbonate / Strontium / strontium nitrate / sulfuric acid manganese / manganese chloride / 50% manganese nitrate solution / stannous chloride / zinc chloride, such as crystallization of the four largest packing of chemical reagents AR and CP level.

主要产品有:硫酸钙/硝酸钙/碳酸钙/硫酸铜/氯化铜/硫酸锌/硝酸锌/氯化锌/硫酸钾/氯化钾/溴化钾/硫酸铝钾/磷酸二氢钾/磷酸氢二钾/溴化钠/氯化钠/硝酸钠/氟化钠/磷酸三钠/磷酸二氢钠/磷酸氢二钠/结晶碳酸钠/无水碳酸钠/硫酸铝/硝酸铝/结晶三氯化铝/氢氧化铝/硝酸铁/氢溴酸/草酸/硼酸/柠檬酸/氯化钡/氮酮/硫酸镁/硝酸镁/氯化镁/氯化铵/硫酸铵/氟化氢铵/硫酸铝铵/硫酸亚铁铵/磷酸二氢铵/磷酸氢二铵/溴化铵/四丁基溴化铵/氯化镍/硝酸镍/硫酸镍/氯化镉/硫酸镉/硝酸镉/碳酸镉/碳酸锶/硝酸锶/硫酸锰/氯化锰/50%硝酸锰溶液/氯化亚锡/结晶四氯化锌等大包装化学试剂的AR和CP级别。

The effect of various conditions on the reaction, such as solvent, temperature, the amount of catalyst, the concentration of hydrobromic acid, oxygen/air and so on, was studied.

在此基础上,系统地考察了溶剂、温度、催化剂用量、氢溴酸的浓度、氧气/空气等因素对芳香化合物氧化溴化反应的影响。

Methods Naloxone was synthesized starting from oxidation of thebaine, followed by hydrogenation, acylation, cyanidation, O-demethylation, hydrolyzation and N-allylation. The alternative method of O-demethylation, methane sulfonic acid/DL-methionine and hydrobromic acid were investigated.

在以蒂巴因为原料,经氧化、氢化、酰化、氰化、去氧甲基、水解、N-烯丙基化得到纳洛酮的合成路线中,分别采用甲磺酸/DL-甲硫氨酸和氢溴酸代替三溴化硼进行去氧甲基化和后续水解反应。

In this work , 1,8-octodiol, the starting material, reacted with 40% hydrobromic acid to produce 8-bromooctan-1-ol, with the catalytic action of PPTs, its hydroxyl group was protected by 2,3-dihydropyran. Then it coupled with 1-heptaalkyne, by means of P-2 nickel as catalyst, stereoselectivity catalysis hydrogenated, with the catalytic action of acid to take off extremital 2, 3-dihydropyran which protected hydroxy group, then used PCC to oxidize alcohol into corresponding aldehyde.

以1,8-辛二醇为原料,与40%氢溴酸进行单溴代反应,得到8-溴-1-辛醇,在对甲苯磺酸吡啶盐的催化下与2,3-二氢吡喃反应,保护分子中的羟基,再与1-庚炔进行偶联,以P-2镍为催化剂立体选择性催化加氢,酸性条件下脱末端的2,3-二氢吡喃对羟基的保护,使用氯铬酸吡啶盐将醇氧化成醛。

Bromododecane was synthesized from n-dodecyl alcohol using byproduct hydrobromic acid from 1-bromoadamantan process as raw material in the presence of the concentrated sulfuric acid.

以生产溴代金刚烷得到的副产品氢溴酸为原料,在浓硫酸存在的条件下与正十二醇进行反应合成1-溴代十二烷。

The alternative method of O-demethylation,methane sulfonic acid/DL-methionine and hydrobromic acid were investigated.

方法在以蒂巴因为原料,经氧化、氢化、酰化、氰化、去氧甲基、水解、N-烯丙基化得到纳洛酮的合成路线中,分别采用甲磺酸/DL-甲硫氨酸和氢溴酸代替三溴化硼进行去氧甲基化和后续水解反应。

In this paper, initiator is dissolved in 1-bromopropane which is solvent. Then the propene and hydrogen bromide that can be dissolved in 1-bromopropane are inlet in l-bromopropane when initiator is decomposing. The reaction occurs in fluid phase and high-purity 1-bromopropane is synthesized by one step method. In this paper, the material HBr is synthesized with NaBr and sulfuric acid at the presence of hydrobromic acid.

本论文以1-溴丙烷为溶剂,将引发剂溶于其中,加热到引发剂开始分解时再通入丙烯和HBr,使二者溶解于1-溴丙烷中,在液相中进行反应,实现丙烯&一步法&合成高纯1-溴丙烷利用NaBr与硫酸在氢溴酸存在下反应制备HBr气体,以作为合成1-溴丙烷的原料。

Methods The rat stress gastric ulcer models induced by ethol and burned acetic acid were established and the effect of arecoline hydrobromide on the secretion of gastric acid and pepsase in rats was observed.

方法用化学测定法观察氢溴酸槟榔碱对大鼠胃液胃酸、胃蛋白酶分泌的影响;采用小鼠应激性胃溃疡模型、大鼠乙醇型胃溃疡模型和乙酸灼烧型大鼠胃溃疡模型来观察氢溴酸槟榔碱对胃溃疡动物模型的作用。

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