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氢氧化钠

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The method is characterized in that:(1) the reflux of the 2-[N, N- 2amino]-3-cyano-group-4-thiopheneacetic-5-carboxylic acid tetra ester is carried out in the proper sodium hydroxide aqueous solution of alcohol for 5h to 6h and the pH value is kept over 10 during hydrolysis;(2) the ethanol of 20 per cent to 60 per cent is added and then the strontium chloride aqueous solution with 2times to 2.5times molal weight is directly added, precipitates the crystal, is filtered and dried;(3) water is added to carry out the reflux and the little salt packed in the crude product is removed, and the product is collected through heat filtration.

其特征在于:①将2--3-氰基-4-羧甲基噻吩-5-羧酸四酯在适量氢氧化钠水醇溶液中回流5~6小时,水解过程保持pH值10以上;②然后再加入20-60%乙醇,随后直接加入2-2.5倍摩尔量氯化锶水溶液,析出结晶,过滤,晾干;③加水回流,除去粗品中包裹少量盐,热过滤,收集产品。

In the CMKGM preparation section,with the indicators of DS andη, the optimum laboratory conditions preparation of a certain molecular weight of the high DS of CMKGM: reaction time (5~6) h, the theory of the degree of substitution (2~3), the molar ratio of monochloroacetic acid to Sodium hydroxide (2:1~3:1),the reaction temperature (55~65)℃, liquid ratio (10:1~12:1)mL/g, containing enthanol (50~70)%.

CM(来源:5e60ABC论文网www.abclunwen.com)KGM制备工艺研究中,以取代度、表观粘度为指标,建立了制备一定摩尔质量的高DS的CMKGM的实验室制备条件:反应时间(5~6)h、理论取代度(2~3)、氢氧化钠与氯乙酸摩尔比(2:1~3:1)、反应温度(55~65)℃、液料比(10:1~12:1)mL/g、乙醇体积分数(50~70)%。

Gel consists of: Testosterone, ethanol, purified water, sodium hydroxide, Carbomer 940 and isopropyl myristate.

凝胶组成:睾酮,乙醇,纯净水,氢氧化钠,卡波姆940和十四酸异丙酯。

The process is carried out by rubbing into filament raw materials, digesting in plasticizing liquid of sodium hydrate and sodium silicate at 100-130degree for 1-2hrs to obtain plasticized raw material, high-speed agitating plasticized raw materials with non-metallic minerals, octadecanoic acid and silicon oil at 100-130degree for 15-45hrs, coating and drying to obtain the final product.

先用农用搓揉机直接搓揉成丝状物料,然后丝状物质在含氢氧化钠和硅酸钠的塑化液中于100~130℃下蒸煮1~2小时,得到塑化物料,最后将塑化物料同改性非金属矿粉、硬脂酸和硅油在100~130℃下高速搅拌15~45分钟进行包覆处理,干燥后便得到目标产物。

ConclusionThis process is the best and it can be used for extraction of Panax japonicus protein.

结果氢氧化钠浓度为0.15 mol/L,用量为样品体积的20倍,提取时间1.5 h,提取 3 次为最佳工艺。

It is shown that the adsorption of propiolic alcohol on the surface of pure aluminium is the important reason resulted from corrosion inhibition and that the rule of adsorption conforms with Langmuir's isotherm.

采用失重法研究了氢氧化钠溶液中丙炔醇在不同温度和浓度下对铭的缓蚀作用,发现丙炔醇在铝表面上的吸附是产生缓蚀作用的重要原因,且吸附规律服从Langmuir吸附等温式。

The effects of ratio of formaldehyde to phenol r(subscript F/P, ratio of NaOH to phenol r(subscript NaOH/P and resinification temperature on chemical properties of liquefied wood resins were investigated.

考察不同甲醛与苯酚物质的量之比值r(下标 F/P、氢氧化钠与苯酚物质的量之比值r(下标 NaOH/P和树脂化温度对树脂理化性能的影响。

To broaden desert shrub new utilizing fields, accelerate desert shrub developing to the direction of high added-value and high benefit, the paper studied on the liquefaction of Salix, Caragana and Poplar in the presence of Phenol under sulfuric acid catalysis. The optimum processing parameters for Salix, Caragana and Poplar liquefaction and resinification were investigated. The effect of molar ratio of formaldehyde to liquefied products and NaOH to liquefied products on the character and glue strength of liquefied products resin was studied.

摘 要:为了开辟沙生灌木资源新的应用领域,促使沙生灌木资源的利用向高附加值、高效益的方向发展,本文以苯酚作液化剂,以稀硫酸作催化剂对沙柳、柠条和杨木进行液化实验,分析了反应温度、液比、催化剂用量及液化时间对液化反应的影响;并研究了沙柳、柠条和杨木液化产物树脂化合成工艺和配方,分析了不同的甲醛与液化产物摩尔比以及氢氧化钠与液化产物摩尔比对沙柳、柠条和杨木液化产物树脂的各项性能的影响。

Black-yonggu dahongyu reaumuria 2b pigments(ⅲ, pgment index number: p.R.48: 2, purple-red powder, insoluble in water and ethanol, in case of concentrated sulphuric acid radiofrequent purple-red, red is blue, in case of concentrated nitric acid, radiofrequent Rufous red concentrated sodium hydroxide, thermotolerance.

永固红2B颜料,颜料索引号:p.R.48:2,紫红色粉末,不溶于水和乙醇,遇浓硫酸呈紫红色,稀释后呈蓝光红色沉淀,遇浓硝酸呈棕红色,遇浓氢氧化钠呈红色,耐热性好。

The influences of ratio of liquid to solid, concentration of ethanol in solvent and leaching time on recovery of phenol and caustic soda and yield of fatty acid and sebacic acid were investigated.

在癸二酸传统生产工艺中的裂解工序后增加浸取工序回收游离碱和苯酚,通过正交试验,考察了液固比、浸取剂浓度和浸取时间对氢氧化钠和苯酚回收及对脂肪酸和癸二酸产率的影响,确定最佳回收工艺条件为:液固比2.5,浸取剂为95%的乙醇水溶液,浸取时间为15min。

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