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氢氧化钠

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The monomer ofbromostyrene was synthesized fromβ-bromobenzene by eliminating hydrogenbromide under sodium hydrate.

溴乙基溴代苯在氢氧化钠的作用下,发生溴化氢脱除反应,得到溴代苯乙烯单体。

Methods:total alkaloids of radix Sophora lavescens were extracted by acidified water,then adjusted to neutral by sodium hydroxide solution, dissolved with buffer solution,then were mixed with 0.025% of bromothymol solution and chloroform,and then the mixture was shaken,standing and demixed,the absorbability of chloroform layer was detected at the wavelength of 413nm.

将苦参的酸水提取液用氢氧化钠溶液调节至中性后,依次加入pH=7.6缓冲溶液,溴代麝香草酚蓝指示液、氯仿混合振摇,静置分层,于413 nm波长处测定氯仿层吸收度。

The main steps include as follows: CO2 is led into the mother liquor of sodium meta-aluminate to carry out carbon content decomposing; the primary separation between the aluminum and the gallium is realized by primary carbonatation to filter out sodium hydroxide; secondary carbonatation is carried out on the filtrate to obtain the deposit of the complex salt of gallium and aluminum; a sodium carbonate crystal is obtained after the filtered filtrate is condensed and vaporized; the deposit of the complex salt of gallium and aluminum is dissolved in the mother liquor of sodium meta-aluminate; the processes are repeated until the proportion of gallium and aluminum in the complex salt of gallium and aluminum is larger than 1/340; then the complex salt of gallium and aluminum is added into the NaOH liquor and electrolyzed, thus obtaining the metal gallium with a purity larger than 99.9 percent which reaches the level of 3; simultaneously, the byproducts of the aluminum hydroxide and the sodium carbonate during the process of carbonatation by steps are obtained.

主要步骤包括:向铝酸钠母液中通入CO 2 进行碳分分解,一次碳酸化实现铝镓的初次分离;过滤出氢氧化钠,滤液进行二次碳酸化获得镓铝复盐沉淀,过滤后滤液经浓缩蒸发获得碳酸钠晶体,铝镓复盐沉淀溶解在偏铝酸钠母液中,重复上述过程直至铝镓复盐中的镓铝比例大于1/340,将其加入到NaOH溶液中,电解可获得纯度>99.9%的金属镓,达到3N级水平同时在分步碳酸化的过程中获得氢氧化铝和碳酸钠副产品。

Experiment showed that the hydrolysis product of chloroisopentene in sodium hydroxide solution was mixture of isopentenol and methyl butenol , which indicated that displacement reaction of chloroisopentene was accompanied by isomerization reaction of carbonium ion.

在以氢氧化钠水溶液进行氯代异戊烯水解时发现,水解产物为异戊烯醇和甲基丁烯醇的混合物,这说明氯代异戊烯在进行取代反应的同时,伴有正碳离子的异构化反应,由此开发了一条全新的由氯代异戊烯生产甲基丁烯醇和异戊烯醇的新的工艺路线。

Extraction of fish oil is done in the temperature of 65℃,70℃, 75℃,80℃,85℃,90℃and95℃ in turn in the condition of pH8.0,55mins in hydrolyzing,20mins in salting out with 4.5 percent of potassium nitrate and 30mins in centrifugalization with 3000r/min.

在传统淡碱水解工艺的基础上,将氢氧化钾和硝酸钾分别替换原工艺中的氢氧化钠和氯化钠,在pH8.0、水解时间55min、用4.5%的硝酸钾盐析30min、用3000转的离心机离心30min的条件下,分别在65℃、70℃、75℃、80℃、85℃、90℃、95℃时提取粗鱼油。

Based on traditional technology of light alkaline bydrolysis,sodium hydroxide and sodium chloride in original technology will be replaced by potassium hydroxide and potassium nitrate differently.Extraction of fish oil is done in the temperature of 65℃,70℃, 75℃,80℃,85℃,90℃and95℃ in turn in the condition of pH8.0,55mins in hydrolyzing,20mins in salting out with 4.5 percent of potassium nitrate and 30mins in centrifugalization with 3000r/min.

在传统淡碱水解工艺的基础上,将氢氧化钾和硝酸钾分别替换原工艺中的氢氧化钠和氯化钠,在pH8.0、水解时间55min、用4.5%的硝酸钾盐析30min、用3000转的离心机离心30min的条件下,分别在65℃、70℃、75℃、80℃、85℃、90℃、95℃时提取粗鱼油。

Purified water, VP/VA copolymer, vegetable glycerin, hydrolyzed wheat protein, biotin, panthenol, niacin, extracts of camellia sinensis and serenoa serrulata, certified organic extracts of salvia officinalis, aloe barbadensis leaf, lavandula angustifolia, melissa officinalis, calendula officinalis and chamomilla recutita, sodium hydroxide, carbomer, phenoxyethanol.

纯水、VP / VA共聚物、蔬菜甘油、水解小麦蛋白、素、泛醇、烟酸、提取物的茶树和serenoa serrulata,经认证的有机液(鼠尾草、琴柱草酝酿索芦荟叶片,)小甜甜沙枣淡紫色,酝酿和chamomilla金盏花酝酿recutita(matricaria、氢氧化钠、萃取。所有发质都适合。

Naphthoxyacetic acid was synthesized from 2-naphthol , sodium hydroxide and chloroacetic acid under the microwave radiation.

在微波辐射下,以2-萘酚、氢氧化钠和氯乙酸为原料合成了2-萘氧乙酸。

The chemical structure of the product was characterized by means of the melting point and IR. The results show that tetraethylammonium bromide which was used as a phase transfer catalyst in this reaction had optimization effect on the interfacial diffusive reaction of BTC and PNP. Higher concentration of sodium hydroxide, lower temperature and a higher dosage of BTC produced a small amount of 4-nitrophenyl chloroformate, while lower concentration of sodium hydroxide and a lower dosage of BTC made reaction incomplete, which affected the yield.

结果表明,在碳酸二(4-硝基苯基)酯合成中使用的相转移催化剂四乙基溴化铵对受界面扩散控制的BTC气与对硝基酚钠反应有良好的相转移催化效果;氢氧化钠质量分数较低时,酚钠盐向溶有BTC的油相扩散速度较小,较高时会产生氯甲酸对硝基苯酯;温度较低、BTC量较高时,会产生少量氯甲酸对硝基苯酯,BTC用量较低会使反应不完全,这些都影响着收率。

Synthesis process of 2,6-dichloro-3-methylaniline was investigated 3-methylaniline was first N-acetylated with acetic anhydride,then treated with chlorosulphonic acid and ammonia yielding the 2-methyl-4--benzenesulfonic amide,which wasin turn deacetylated,chlorinated and hydrolyzed to the title compound.Hydrochloric acid was used instead of sodium hydroxide in deacetylation and sodium chlorate instead of hydrogen peroxide as oxidant in chlorination.

合成工艺2,6-二氯-3-甲基苯胺调查3-甲基首次N-乙酰与醋酸酐,然后与氯磺酸和氨产量 2-甲基-4--苯磺酰胺基,而擅转乙酰,氯化和水解的标题compound.hydrochloric酸代替氢氧化钠乙酰氯酸钠代替双氧水为氧化剂,加氯。

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