氢化

During the reaction of alkylation, general contained 0.2%~2.0% butadiene will produce viscous heavy composite materials, which will raise final boiling point of alkylate and decrease octane, what is more, it will react with acid to produce corresponding ester, which will increase the consumption of acid, Therefore, we must remove butadiene by selective hydrogenation, at the same time, it will convert some of 1- butane to 2- butane by isomerization and raise octane of alkylate.

一般含有0.2%~2.0%的丁二烯，其在烷基化反应中，可生成一种分子量很高的粘稠重质迭合物，使烷基化油的干点升高，辛烷值降低，并且它还和酸反应生成相应的酯而加大酸耗量。因此必须经过选择性加氢除掉丁二烯，同时，将部分1-丁烯异构化为2-丁烯，以提高烷基化油的辛烷值。

The method on trans fatty acids analysis in food is very important. The effects of methylate sodium, potassium hydroxide, sulfuric acid and boron trifluoride in methanol and their different concentration and dosage on TFA analysis were studied. The chromatographic condition and the influence of time and temperature on the esterifation of TFA using boron trifluoride in methanol were optimized. A method for analyzing TFA were established by GC based on boron trifluoride in methanol and RT-2560(100m×0.25mm×0.2μm) capillary column.

研究了甲醇钠－甲醇、氢氧化钾－甲醇、浓硫酸－甲醇和三氟化硼－甲醇4种甲酯化试剂的浓度、用量及甲酯化时间和温度对反式脂肪酸检测的影响，优化了色谱条件，建立了以三氟化硼－甲醇法甲酯化，RT-2560(100m×0.25mm×0.2μm)毛细管柱为基础的反式脂肪酸气相色谱检测方法，C18：1-9 t， C18：1-11 t， C18：2-9 t， 12 t和C22：1-13 t 4种反式脂肪酸的最小检出浓度在0.774.08 mg/kg之间。4种反式脂肪酸不同添标浓度回收率为98.44%101.23%，重复测定的相对标准差在0.22%1.31%之间，有较好的准确度和重现性。

Other products are: ammonium bromide, potassium bromide, zinc bromide, lithium bromide, potassium bromate, protopine, hydrobromide potassium bromate, phenol and so on.

其它产品有：溴化铵、溴化钾、溴化锌、溴化锂、溴酸钾、片碱、溴酸钾氢溴酸、苯酚等。

Potassium bromide produced in the elimination step was cleaned with steam treatment, then used to bromize tert-Butyl alcohol, producing tert-butyl bromide.

为了回收中间元素澳，用水蒸汽蒸馏方法除去脱漠化氢后生成演化钾盐中的杂质，通过添加硫酸以再生漠化钾用于叙丁醇漠化制漠代叔丁烷。

Based on the absorbance change of indicators with the concentration of hydrogen ion released from the enzyme-catalyzed reaction, a convenient colorimetry method is established for the assay of acidic phospholipase 〓 and glycogen phosphorylase b Brilliant yellow and bromothymol blue are chosen as indicators for assays of acidic phospholipase 〓 and glycogen phosphorylase b by following the absorbance changes at 495 nm and 615nm respectively The method is simple, sample-saving, sensitive and valid for a wide range of enzyme concentrations.

为了研究糖原磷酸化酶的激活动力学和酸性磷脂酶〓的复性过程，我们根据酶催化反应中释放氢离子浓度的变化引起相应的指示剂的光吸收发生变化的原理，建立了一种简捷的比色法，用于测定酸性磷脂酶〓和糖原磷酸化酶b的活性。选用亮黄和溴麝香草酚兰分别作为酸性磷脂酶〓和糖原磷酸化酶b测活的指示剂，在495 nm和615 nm处检测二者的光吸收值的变化，可以测定酶活。本方法的优点是，可在比较宽的酶浓度范围内进行活力测定，而且操作简单、节省样品、灵敏度高。

The main steps include as follows: CO2 is led into the mother liquor of sodium meta-aluminate to carry out carbon content decomposing; the primary separation between the aluminum and the gallium is realized by primary carbonatation to filter out sodium hydroxide; secondary carbonatation is carried out on the filtrate to obtain the deposit of the complex salt of gallium and aluminum; a sodium carbonate crystal is obtained after the filtered filtrate is condensed and vaporized; the deposit of the complex salt of gallium and aluminum is dissolved in the mother liquor of sodium meta-aluminate; the processes are repeated until the proportion of gallium and aluminum in the complex salt of gallium and aluminum is larger than 1/340; then the complex salt of gallium and aluminum is added into the NaOH liquor and electrolyzed, thus obtaining the metal gallium with a purity larger than 99.9 percent which reaches the level of 3; simultaneously, the byproducts of the aluminum hydroxide and the sodium carbonate during the process of carbonatation by steps are obtained.

主要步骤包括：向铝酸钠母液中通入CO 2 进行碳分分解，一次碳酸化实现铝镓的初次分离；过滤出氢氧化钠，滤液进行二次碳酸化获得镓铝复盐沉淀，过滤后滤液经浓缩蒸发获得碳酸钠晶体，铝镓复盐沉淀溶解在偏铝酸钠母液中，重复上述过程直至铝镓复盐中的镓铝比例大于1/340，将其加入到NaOH溶液中，电解可获得纯度＞99.9％的金属镓，达到3N级水平同时在分步碳酸化的过程中获得氢氧化铝和碳酸钠副产品。

To be different from the already chloromethylation catalyst, it has a certain amount of moisture wet, which will not produce huge amounts of doughtic cancerogenic chloromethyl methyl ether during and after the reaction.4,4\'-bisbiphenyl, 1,4-bisbenzene, 1,4-bis(chloro- methyl)-2,5-dimethylbenzene, 1,5-bis-2,4-dimethylbenzene, 4-(chlor- omethyl)-1,2-dimethylbenzene, 1,2-bis-4,5-dimethylbenzene, 5,8-bis-1,2,3,4-tetrahydronaphthalene, 3,3\',5-tris-4,4\'-bisbiphenyl and 3,3\', 5,5\'-tetrakis-4,4\'-bisbiphenyl were synth- esized by using this new catalyst. Results indicated that when the reaction temperature was 55～60℃, the reaction time was 12h, the catalyst which consists of the concentration of 80%H_2SO_4, HAc and Lewis acid, the amount of Lewis acid 0.15 mol(nLewis:nbiphenyl=1.5:1), yield of biphenyl chloromethylation product 4,4\'-bis(chrolomethylbiphenyl can reach a maximum 85%.

采用这种催化体系完成了4，4′-二氯甲基联苯、对二氯甲基苯、1，4-二氯甲基-2，5-二甲基苯、1，5-二氯甲基-2，4-二甲基苯、4-氯甲基-1，2-二甲基苯、1，2-二氯甲基-4，5-二甲基苯、5，8-二氯甲基-四氢萘、3，3'，5-三氯甲基-4，4'-二甲基苯和3，3'，5，5'-四氯甲基-4，4'-二甲基苯的合成，结果表明：在反应条件为：反应温度55～60℃，反应时间12h，选择80%H_2SO_4、冰醋酸和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.15mol(和原料比为1.5：1)，反应效果最好，联苯氯甲基化产物(4，4′-二氯甲基联苯)收率为85%；在反应条件为：反应温度70℃，反应时间8h，80%H_2SO_4、冰醋酸和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.1mol(和原料比为1：1)时，反应效果最好，苯的氯甲基化产物收(来源：ABd0C论文eded网www.abclunwen.com)率为75%；在反应条件为：在反应条件为：反应温度40℃，反应时间10h，60%H_2SO_4和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.1mol(和原料比为1：1)时，反应效果最好，对二甲苯氯甲基化产物(1，4-二氯甲基-2，5-二甲基苯)收率为78.5%；在反应条件为：反应温度35℃，反应时间10h，60%H_2SO_4、冰醋酸和Lewis酸为催化剂，反应最佳反应Lewis酸用量是0.1mol(和原料比为1：1)时，反应效果最好，间二甲苯氯甲基化产物(1，5-二氯甲基-2，4-二甲基苯)收率为81.5%。

Our main products are oilfield chemicals—Calcium Bromide、 Zinc Bromide、Sodium Bromide; Pharmaceutical and Photographic Grade Potassium Bromide、 Ammonium Bromide、Hydrobromic Acid、 Lithium Bromide as well as organic bromine flame retardants including Tetrabromobisphenol A and so on.

主要生产油田化学品---溴化钙、溴化锌、溴化钠；医药及照相用溴化钾、溴化铵、氢溴酸、溴化锂及有机溴系阻燃剂四溴双酚A等。

The influence of CFC-12 content, effect of fluorination temperature and fluorinating time on the structure and hydrodesulfurization activity of the catalysts were examined systematically. The results revealed that hydrodesulfurization activity of the catalyst fluorinated by 1% CFC-12 at 623 K was obviously improved With an increase of 20%-30% as compared With that of the unfluorinated catalyst, the commercially available BY2 catalyst, and NH4F-fluorinated catalysts.

通过对0.5%~7%各种氟里昂浓度和473~773K各种温度及不同时间氟化处理的样品进行详细考察，发现在623K下由含氟里昂1%的湿空气氟化的载体制备的催化剂样品，其噻吩的加氢脱硫的活性有明显改善，相对於非氟化样品、BY-2工业催化剂以及氟化铵溶液浸渍处理的催化剂活性提高20%~30%，且非常稳定。

On the discussion about mechanism of mutation of methylating, we explored thermodynamics and dynamic properties on base pairs, investigating the proton transfer on base pairs.

从甲基化对嘌呤碱基电荷的影响，到甲基化引起碱基配对的改变造成碱基配对的诱变等都作了较为详细的探讨；在对甲基化诱变的探讨中，我们进行了热力学和动力学方面的研究，同时对碱基之间的质子迁移的难易程度也作了探讨；并在充分考虑水分子存在的情况下研究了甲基化对碱基之间的氢键作用和堆积作用的影响。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。