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Whenpyridine was used as reductive decomposing agent, the expecting cholest-4-en-3,6-dione-22-al was obtained. However, when Zn/HOAc was used to decomposethe ozonide, C-4,5 double bond was further reduced to give cholest-3,6-dione-22-al as main product. 2 For the side-chain construction of compound (1), the solid-liquid phase-transfer Wittig reaction was used. When (3-methyl-2-oxobutyl)-triphenylarsonium bromide was used as reagent, the reaction can be carried out inmild reaction condition and the yield is higher than that when phosphorane wasused.

但使用Zn/HOAc作为分解剂时,却得到其氢化产物胆甾-3, 6-二酮-22-醛;2在甾体支链引入过程中,采用固-液相转移Wittig反应的方法,用(3-甲基)-2-氧丁基三苯基溴化胂作为试剂,反应在非常温和的条件下便可完成,而且产率比传统采用膦烷的方法更高;3在对某些甾酮化合物的选择性还原反应研究时,发现在〓还原体系中,当加入某些金属离子后,反应有更好的区域选择性和立体选择性。

Also, some enzymes are named according to the type of reaction they catalyze, such as phosphorylase or dehydrogenases.

此外,某些酶是根据它们所催化的反应类型来命名的,例如磷酸化酶或脱氢化酶。

The measurement of 1/f noise in amorphous, microcrystalline and polymorphous silicon film was performanced with a self-design semiconductor system.

研究不同厚度的非晶、微晶和多形硅三种氢化硅薄膜的热导率结果表明微晶硅薄膜的晶化增大了薄膜的热导率。

Results The best experimental conditions for the new method were as follows: hydrochloric acid concentration 5%; sodium borohydride solution, potassium bromate and potassium bromide solution, 2ml each; flow rate 0.6L/min.

结果]本法的最佳实验条件为盐酸溶液浓度5%,硼氢化钠溶液和澳化剂的用量各为2ml,载气流量0.6L/min。

Methods The mercury in urine, which is the total amount of inorganic mercury in urine, including those produced from organic mercury after treated by potassium bromate and potassium bromide, is determined by atomic absorption spectrophotometer after reduction into mercury atom with sodium borohydride.

方法]尿样中汞(尿中无机汞和经溴酸钾-溴化钾处理尿中有机汞生成的无机汞之和)以硼氢化钠还原生成汞原子蒸气,用原子吸收光谱仪测定其汞的含量。

New metalized films were obtained by the reduction of PAN/metal salt chelate films with NaBH4 aqueous solution.

以硼氢化钠(NaBH4)水溶液还原聚丙烯腈/金属盐络合膜后,就可得到一种新的高分子表面金属化材料。

The production method and processing conditions of sulfur,sodium hyposulfite, sodium hydrosulfide and thiourea from hydrogen sulfide tail-gas in the production of barium carbonate by carbonation method are introduced.

介绍了利用碳化法生产碳酸钡的硫化氢尾气生产硫磺、硫代硫酸钠、硫氢化钠和硫脲的生产方法和工艺条件,指出硫化氢的综合利用生产工艺简单,产品质量稳定,容易工业化,产品成本低,同时消除了硫化氢尾气对环境的污染,有巨大的经济效益和社会效益,发展前景非常广阔。

The process improvement of flaky sodium hydrosulfide production;2. The production method and processing conditions of sulfur,sodium hyposulfite, sodium hydrosulfide and thiourea from hydrogen sulfide tail-gas in the production of barium carbonate by carbonation method are introduced.

介绍了利用碳化法生产碳酸钡的硫化氢尾气生产硫磺、硫代硫酸钠、硫氢化钠和硫脲的生产方法和工艺条件,指出硫化氢的综合利用生产工艺简单,产品质量稳定,容易工业化,产品成本低,同时消除了硫化氢尾气对环境的污染,有巨大的经济效益和社会效益,发展前景非常广阔。

Ambient conditions that include toxic gases such as hydrogen sulfide, sulfurous acid, nitrous acid, chlorine, bromine, methyl bromide, ammonium, etc.

b 周围环境中有氢化硫、亚硫酸、亚硝酸、氯气、溴气、溴化甲烷、氨气等有毒气体。

The synthesis of nalbuphine hydrochloride from thebaine as starting material was through following processes:oxidation,high-pressure hydrogenation,acetylation,removing methyl of 3-methoxy,hydrolysis,condensation,reduction and finial salification.

以蒂巴因为起始原料,经氧化、高压氢化、乙酰化、氰化、脱3-位甲氧基的甲基、水解、缩合、还原、成盐,合成了盐酸纳布啡,总收率达18。

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I didn't watch TV last night, because it .

昨晚我没有看电视,因为电视机坏了。

Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

今年以来,在北京的很多小区里,电梯液晶电视被撤了下来。

I'm running my simile to an extreme.

我比喻得过头了。