氟苯

The obtained compound (2) was treated with borane-tetrahydrofuran (B2H6–THF) complex under nitrogen atmosphere in excessive THF for 18 h to give a kind of dark brown oil,followed by ammonolysis with NH3·H2O in autoclave at 100 ℃ for 6 h to produce 2-(5-amino-2- nitrophenyl) ethanol (3) in 84.4% yield.

用硼烷还原5-氟-2-硝基苯乙酸后，接着用氨水在高压釜中加热到100 ℃氨解，得到2-(5-氨基-2-硝基苯)乙醇（84.4%）。

The overall yield was 43.6%.The yield of reduce of ester was increased nearly one times than the past method because of KBH4-LiCl as the reducing agent instead of NaBH4. Changing the reaction conditions of bromization, the one-way yield enhanced 30%. The yield of reduce of the bromide was added by one times by improving the process. Tefluthrin was achieved by the catalytic esterification of DCC and DMAP.

优化后工艺对四氟对苯二甲酯的还原采用了廉价高效的还原试剂KBH4-LiCl，使收率比NaBH4法提高了近一倍；对溴化反应条件进行了优化，单程收率提高了30%；对溴化物还原条件的优化，使其收率提高了近一倍；采用了催化剂DCC和DMAP合成了最终产品七氟菊酯。

At present, since fluorobenzene liquid crystal and cyclohexyl crystal are very popular liquid crystals. some research have done on the synthesis of the intermediate, fluorophenol and alkylcyclohexylbenzene compounds in this thesis.

本论文的主要内容分为两部分：第一部分，针对目前液晶材料研究的热点：含氟液晶和环己烷类液晶，就其液晶材料中间体氟代苯酚和烷基环己基苯类化合物的合成进行研究。

Factory engaged in medicine, veterinary medicine, agricultural chemicals and raw materials development and production of intermediates, the series of export products: 2,2 - bipyridine, 2,6 - dihydroxy toluene, propiconazole intermediates, phenol line P , Fluometuron, fluorine pyronaridine oxadiazon, oxadiazon pyronaridine fluorine intermediates, Robenidine hydrochloride and so on.

本厂从事医药、兽药、农用化学品原料药及中间体的研制与生产，系列出口产品：2，2-联吡啶，2，6-二羟基甲苯，丙环唑中间体，酚线磷，伏草隆，氟咯草酮，氟咯草酮中间体，盐酸氯苯胍等等。

objective to explore the curative effects and safety of fluoxetine in senile hypertensive patients with depression .methods 72 senile patients were randomly divided into: control group(n=36) treated with benazepril 10mg/d routine hypotensor therapy and research group(n=36) with combination of benazepril 10mg/d and fluoxetine 20mg/d and psychotherapy for 6 weeks.

目的 探讨氟西汀治疗老年性高血压合并抑郁障碍的疗效及安全性。方法将72例老年性高血压合并抑郁障碍患者随机分为研究组36例和对照组36例。两组患者均给予苯那普利10mg？d-1？po常规降压治疗，研究组在常规治疗的基础上加服抗抑郁剂氟西汀20mg？

Benzene perfluorous nonene ether was prepared by the reaction of perfluo-rous nonene (C9F18) and phenol,and the molecular structure of which was identified by IR and NMR spectra.

以全氟壬烯、苯酚和氯磺酸为主要原料，经醚化、磺化和中和反应制备对全氟壬烯氧基苯磺酸表面活性剂，用红外光谱和19FNMR，1HNMR对分子结构进行了表征。

Some useful fluorine-containing intermedi-ates were synthesized by the reaction of activated methylenecompounds or silyl enol ether with 2,2-dihydropolyfluoro-alkanoates or 2-hydropolyfluoroalk-2-enoates in the presenceof different bases.

进一步研究表明，在氢化钠的作用下，苯乙腈，苄基苯基甲酮也可以与2-氢多氟-2-烯酸乙酯发生亲核加成反应，苄基苯基甲酮的加成中间体经多聚磷酸环化，得到了间位氟烷基取代的α-萘酚衍生物。

The intermediates 2a～2f of cyclic (1-arylseleno)glycerol phosphate and tegafur conjugates were synthesized by one-pot reaction of hexaethyl phosphorous triamide, activated by a catalytic amount of iodine, with (N3-tegafur)alkanol, 1-arylselenoglycerol and sulphur successively in refluxing benzene.

以碘作催化剂，无水苯为溶剂，六乙基亚磷酰三胺依次与羟乙基替加氟、1-芳硒基甘油及硫反应，得中间体硒代环甘油磷脂替加氟缀合物2a～2f。

Fluoroalkyl acetic acids were converted to their corresponding carbonyl chlorides, and the latter reacted with o-aminpbenzyl aldehyde and ammonia gas to give 3-(1-imino-fluoroalkyl)-1H-quinolin-2-ones in moderate yields.

将2-氟烷基乙酸转化成相应酰氯，后者与邻氨基苯甲醛在通氨气条件下以较高产率转化为相应的3-（1-亚胺基-氟烷基）-1H-喹啉-2-酮。

By the use of standard substance, a standard spectrum library was established for 10 drugs, metformin, ephedrine, pseudoephedrine, caffeine, phenformin, fenfluramine, indapamide, phenolphthalein, fluoxetine and sibutramine. The identification for illegally added drugs was performed by comparing the accordance of retention time and the three-grade mass spectrum with the standard spectrum library.

利用标准物质建立10种药物（二甲双胍、麻黄碱、伪麻黄碱、咖啡因、苯乙双胍、芬氟拉明、吲达帕胺、酚酞、氟西汀、西布曲明）标准谱库，通过与标准谱库保留时间和三级质谱图的比较对非法添加的药物进行定性鉴别。

The labia have now been sutured together almost completely.The drains and the Foley catheter come out at the top.

此刻阴唇已经几乎完全的缝在一起了，排除多余淤血体液的管子和Foley导管从顶端冒出来。

To get the business done, I suggest we split the difference in price.

为了做成这笔生意，我建议我们在价格上大家各让一半。