氟氧化物

The orthogonal design method is used for preparation of rare earth fluoride by rare earth oxide(Gd_2O_3) fluorination with NH_4HF_2 in this paper.

采用正交试验法，研究了用氟化氢铵作氟化剂直接与稀土氧化物(Gd2O3)反应，制备稀土氟化物的工艺，确定了氟化的最佳工艺条件，并进行了分析讨论。

A selective and mild PS-DIB/ionic-liquid immobilized 2, 2, 6, 6-tetramethyl-piperidin-4-ol-N-oxyl catalytic oxidation procedure of alcohols to the corresponding aldehydes and ketones in ionic liquid BF4 at room temperature was developed. The oxidant PS-DIB was prepared via the iodation and acetylation of polystyrene resin. For the preparation of the ionic-liquid immobilized TeMPO catalyst, 4-(2, 2, 6, 6-Tetramethyl-1-oxyl-4-piperidoxyl)butyl bromide was first synthesized from TeMPO and 1, 4-dibromobutane.

将聚苯乙烯树脂先碘化再乙酰基化，制得了负载型二乙酰氧碘苯作为氧化剂。2， 2， 6， 6-四甲基－N-氧自由基哌啶醇与1， 4-二溴丁烷反应生成4-溴丁氧基－2， 2， 6， 6-四甲基－哌啶－1-氧化物，再与N-甲基咪唑发生季铵化反应，生成的溴化季铵盐与四氟硼酸钠进行离子交换制得氟硼酸型2， 2， 6， 6-四甲基－N-氧自由基哌啶负载离子液体。

A selective and mild PS-DIB/ionic-liquid immobilized TEMPO catalytic oxidation procedure of alcohols to the corresponding aldehydes and ketones in ionic liquid BF4 at room temperature was developed. The oxidant PS-DIB was prepared via Iodation and acetylation of polystyrene resin. For the preparation of the ionic-liquid immobilized TEMPO catalyst, 4-(2,2,6,6-Tetramethyl-1-oxyl-4-piperidoxyl)butyl bromide was first synthesized from 2,2,6,6-tetramethyl-piperidin-4-ol-N-oxyl and 1,4-dibromobutane.

将聚苯乙烯树脂先碘化再乙酰基化，制得了负载型二乙酰氧碘苯(diacetoxyiodo polystyrene，PS-DIB)作为氧化剂。2，2，6，6-四甲基-N-氧自由基哌啶醇(2，2，6，6-tetramethyl-piperidin-4-ol-N-oxyl，TEMPO)与1，4-二溴丁烷反应生成4-溴丁氧基-2，2，6，6-四甲基-哌啶-1-氧化物，再与N-甲基咪唑发生季铵化反应，生成的溴化季铵盐与四氟硼酸钠进行离子交换制得氟硼酸型2，2，6，6-四甲基-N-氧自由基哌啶负载离子液体TEMPO-IL。

Up-conversion luminescence ; Er~3+ ion ; Volumetric display ; Multi-step excitation ; Oxyfluoride glass material

上转换发光； Er~（3+）离子；立体三维显示；多步激发；氟氧化物玻璃材料

In this paper we study the indirect upconversion-sensitization luminescence of Tm(0.1)Yb(10.9):oxyfluoride glass induced by 800nm diode laser.

研究了Tm(0.1)Yb(10.9)氟氧化物玻璃在800 nm半导体激光激发下的间接上转换敏化发光现象。

In this paper, transparent Er(superscript 2+) ions doped oxyfluoride glass-ceramics was prepared by high temperature melting and thermal treatment technology. The changes of micro-crystals structure, UV-VIS absorption spectra and NIR emitting spectra occurred with the variety of Er(superscript 3+) concentrations were studied.

采用高温熔融及热处理工艺，制备了透明度良好的Er(上标 3+)离子掺杂的氟氧化物玻璃陶瓷，并研究了不同Er(上标 3+)离子掺杂浓度下，玻璃陶瓷微晶结构、紫外－可见波段吸收光谱、近红外发射光谱的变化。

The up-conversion properties of Er3+ in the oxyfluoride glass-ceramics codoped with Er3+ and Yb3+ were studied using the 960 nm semiconductor laser as a pumped source.

金杰用960 nm半导体激光器作泵浦源，研究了Er3+和Yb3+共掺杂的氟氧化物玻璃陶瓷中Er3+的上转换发光的性质。

A set of 61 ion polarizabilities has been derived from the dielectric constants of 129 oxides and 25 fluorides using a least squares refinement technique in conjunction with the Clausius–Mosotti equation.

61离子的极化设置了129名来自25个氟氧化物和介电常数使用与克劳Mosotti方程，联最小二乘改进技术。

A set of 61 ion polarizabilities has been derived from the dielectric constants of 129 oxides and 25 fluorides using a least squares refinement technique in conjunction with the Clausius–Mosotti equation.

61离子的极化设置了129名来自25个氟氧化物和介电常数使用与克劳米斯蒂方程，联最小二乘改进技术。

A set of 61 ion polarizabilities has been derived from the dielectric constants of 129 oxides and 25 fluorides using a least squares refinement technique in conjunction with the Clausius–Mosotti equation.

61离子的极化成立了129名来自25个氟氧化物和介电常数运用与克劳Mosotti方程，联最小二乘纠正本领。

I am accused of being overreligious," she said in her quiet, frank manner,"but that does not prevent me thinking the children very cruel who obstinately commit such suicide.""

客人们在卡罗利娜·埃凯家里，举止就文雅一些，因为卡罗利娜的母亲治家很严厉。

Designed by French fashion house Herm è s, this elegant uniform was manufactured in our home, Hong Kong, and was the first without a hat.

由著名品牌 Herm è s 设计，这件高贵的制服是香港本土制造，是我们第一套不配帽子的制服。