氟化的

It is prepared from pentachluorobenzonitrile by using KF as fluoride to substitute chlorine in the presence of benzonitrile under high temperature. But owing to the low solubility of KF and rigor synthesis condition, and the parallel auxiliary reactions, the speed of reaction as well as the yield is very low.

五氟苯甲腈的合成开发以五氯苯甲腈为原料在较高的温度下用氟化钾做氟化剂，通过取代苯环上氯原子而得到的，由于氟化钾在溶剂中溶解度低，合成条件要求苛刻，反应速度较慢，同时存在有平行竞争副反应，因而反应收率较低，国内尚无厂家生产。

Said mineralizing agent is the fluoric alkali-earth metal salts or alkali metal salts (potassium fluoride or calcium fluoride).

其特征是在磷酸钙盐与碳酸钙盐以2∶1比混合物中，加入0.5～3wt％的含氟离子碱土金属或碱金属盐矿化剂，例如氟化钾、氟化钙等。

Reaction conditions are studied, and the result shows that it is better to adopt mercuric oxide or mercuric fluoride as fluorination catalyst with reaction temperature -20~-10℃.

结果表明，采用氧化汞或氟化汞作氟化催化剂、氟化氢作溶剂较好，适宜的反应温度为－20~-10℃，较长的反应时间(48 h)和增加氟化氢和催化剂的量有利于氟化。2-氯－5-三氯甲基吡啶的转化率和选择率均可达到97%以上。

Reaction mechanism for 11,1,2-tetrafluoroethane preparation is carried out through gas phase fluorination by hydrogen fluoride over chromium-magnesium fluorination catalysts with trichloroethylene as main materials and dynamics models are set up.

研究了以三氯乙烯为主要原料，在铬镁氟化催化剂存在下，用氟化氢气相氟化制备1，1，1，2-四氟乙烷的反应机理，建立了动力学模型。

Difluorodiphenylsulfone and 4, 4"-difluorodiphenylketone are sulfonated by 50 % sulfuric acid. A new biphenol monomer containing six-membered ring imide is synthesized by reaction of 1, 4, 5, 8-naphthelenetetracarboxylic acid dianhydride with 3-aminophenol or 4-aminophenol sodium.

以50%发烟硫酸为磺化试剂，以4，4′-二氟二苯砜和4，4′-二氟二苯酮为原料反应得到双磺化的4，4′-二氟-3，3′-二磺酸钠-1，1′-二苯砜和4，4′-二氟-3，3′-二磺酸钠-1，1′-二苯酮。

The company produces boron trifluoride acetonitrile and family of products based on technology Zhejiang Huangyan chemical synthesis, the plant is the first production of boron trifluoride etherate, one of the manufacturers, with thirty years of history, there is a group engaged in research boron trifluoride and a group of experts with practical experience of staff.

本公司生产三氟化硼乙腈及系列产品的技术主要依托浙江黄岩合成化工厂，该厂是全国最早生产三氟化硼乙醚的厂家之一，具有三十多年的历史，有一批从事研究三氟化硼的专家和一批具有实际操作经验的工作人员。

I was founded in 2005, is a professional Chemical Industry Co., Ltd, Main BF3 acetonitrile complex, boron trifluoride diethyl ether complex, boron trifluoride DMC complex and Inorganic chemical raw materials, pharmaceutical intermediates.

我公司成立于2005年，是一家专业的化工实业有限公司，主营三氟化硼乙睛络合物、三氟化硼乙醚络合物、三氟化硼碳酸二甲酯络合物及无机化工原料、医药中间体。

The catalysts such as tetraphenyl tin,aluminium isopropoxide and boron trifluoride etherate complex were used to catalyze the copolymerization.In addition,the copolyester can be given by copolycondensation after monomers were hydrolyzed by phosphoric acid.Boron trifluoride etherate complex was chosen as the catalyst because the catalytic activity was the best among the catalysts.

由于γ-戊内酯为五元环结构，难以进行开环聚合，因此分别考察了四苯基锡、异丙醇铝、三氟化硼乙醚络合物等催化剂，以及以磷酸为催化剂的水解缩聚反应，结果发现三氟化硼乙醚络合物的催化活性最高，因此选择三氟化硼乙醚为本体开环聚合的催化剂。

Lithium perfluoroalkylphosphonate was synthesized by LiF and perfluoroalkylphosphonate acid obtained by electrochemically fluorinating chlorodiisopropylphosphine. Some properties of a kind of electrolyte that was made from dissolving the lithium perfluoroalkylphosphonate in the mixed solvent with ethylene carbonate and dimethyl carbonate mass ratio 1∶1 were investigated, such as conductivity, stability toward hydrolysis and oxidative decomposition potential, and so on.

选取氯代二异丙基膦(C6H14PCl)为原料，利用电化学氟化方法，得到全氟烷基膦酸[(C3F7)2PF3]，(C3F7)2PF3与氟化锂反应得到全氟烷基膦酸锂Li[(C3F72PF4]，将其溶于碳酸乙烯酯和碳酸二甲酯质量比为1∶1的混合溶剂中得到电解液，考察电解液的电导率、抗水性及氧化分解电位。

Chiral nonracemic fluoro-organic molecules with a fluorine atom on a stereogenic center are readily prepared via chiral electrophilic fluorinating reagent-mediated enantioselective fluorinations, substrate-controlled enantioselective electrophilic fluorinations, chiral metal complexes and asymmetric catalyst—directed catalytic enantioselective fluorinations.

高光学活性的手性氟化物可通过手性亲电氟化试剂诱导的立体选择性氟化反应，基于底物的手性氟化反应以及手性催化剂诱导的不对称催化氟化反应等来制备。

The labia have now been sutured together almost completely.The drains and the Foley catheter come out at the top.

此刻阴唇已经几乎完全的缝在一起了，排除多余淤血体液的管子和Foley导管从顶端冒出来。

To get the business done, I suggest we split the difference in price.

为了做成这笔生意，我建议我们在价格上大家各让一半。