氟化的

The article includes three parts. The first, a steroselective and regioselective synthesis of digitoxin with glycosyl ortho-alkynylbenzoates as doners. The second, synthesis of different length chain of L-fucose with a SO3Na group in the position of C-2 hydroxy.

本文工作主要包括三部分内容，分别为采用全新发展的一种邻炔基苯甲酸酯的糖基供体进行地高辛的全合成并与常规的Schimidt供体及三氟亚胺酯供体进行结果比较；合成不同长度的2位硫酸化的岩藻糖糖链；对现有的合成伏格列波糖的一条合成路线进行工艺优化。

"It has valence 2 or 4 in compounds, including stannous chloride (used in tin galvanizing and manufacturing polymers and dyes), stannous oxide (used to make tin salts for chemical reagents and plating), stannous fluoride (used as an anticavity ingredient in toothpastes), stannic chloride (a stabilizer for perfumes and a source of other tin salts), and stannic oxide (a catalyst and a polish ing powder for steel)."

在化合物中的原子价为2和4。化合物包括氯化亚锡(用于电镀锡以及制造聚合物和染料)、氧化亚锡(制备化学试剂和电镀用的锡盐)、氟化亚锡、氯化锡(香水的稳定剂以及其它锡盐的原料)以及氧化锡(催化剂以及钢材的拋光粉)。

"It has valence 2 or 4 in compounds, including stannous chloride (used in tin galvanizing and manufacturing polymers and dyes), stannous oxide (used to make tin salts for chemical reagent s and plating), stannous fluoride (used as an anticavity ingredient in toothpastes), stannic chloride (a stabilizer for perfumes and a source of other tin salts), and stannic oxide (a catalyst and a polishing powder for steel)."

在化合物中的原子价为2和4。化合物包括氯化亚锡(用于电镀锡以及制造聚合物和染料)、氧化亚锡(制备化学试剂和电镀用的锡盐)、氟化亚锡、氯化锡(香水的稳定剂以及其它锡盐的原料)以及氧化锡(催化剂以及钢材的拋光粉)。

"It has valence 2 or 4 in compounds, including stannous chloride (used in tin galvanizing and manufacturing polymers and dyes), stannous oxide (used to make tin salts for chemical reagents and pla tin g), stannous fluoride (used as an anticavity ingredient in toothpastes), stannic chloride (a stabilizer for perfumes and a source of other tin salts), and stannic oxide (a catalyst and a polishing powder for steel)."

在化合物中的原子价为2和4。化合物包括氯化亚锡(用于电镀锡以及制造聚合物和染料)、氧化亚锡(制备化学试剂和电镀用的锡盐)、氟化亚锡、氯化锡(香水的稳定剂以及其它锡盐的原料)以及氧化锡(催化剂以及钢材的拋光粉)。

It was shown from the results that emulsifier TP-Ⅴ which was prepared by PEG 4000 reacted with TME, in the molar ratio of TME to PEG 2:1, at about 110℃ for 1 h, catalyzed by boron trifluoride diethyl etherate, has a very good emulsifying impact for TME. Particle size distribution of the emulsion was homo-geneous and viscosity of the emulsion was small.

实验结果表明，以M相对适中的PEG4000与TME按物质的量比2： 1、在催化剂三氟化硼乙醚作用下、110℃左右反应1h合成的乳化剂TP-Ⅴ，对萜烯基环氧树脂具有很好的乳化效果，制备的乳液粒子粒径均一度较高，乳液表观黏度较小。

The novel vacuum furnace is employed in laboratory study. Compared with atmosphere magnesium carbothermic reduction furnace, this new one has the merits of high automation, easy manipulation and fine safety. Vacuum coking, vacuum carbothermic reduction process and magnesium vapory condensation process can be carried out in a furnace.

小型实验结果证明：还原温度升高，还原时间延长，氧化镁还原率增大，添加适量的氟化物对还原反应有促进作用；还原过程中真空度随时间的变化具有规律性，由此可以判断还原反应进行的速度与程度；真空中煤还原氧化镁的条件是：配料时保证C：MgO=3：1，并加入占总料重10％的氟化钙作为催化剂，尽可能的提高反应温度至1500℃以上，保温30～40分钟。

The results show that the originated materials for electrolyte aluminium is Al2O3 and AlF3 has good property to absorb vapour. After the water contained in the originated materials goes into electrolyte, AlF3 reacts with water hydrolyzed and the rest of water is electrolyzed into hydrogen and oxygen. Hydrogen enteres aluminum liquid by diffusing and autoecious in Al2O3, which is the main source of hydrogen in electrolyte aluminum liquid.

研究结果表明：电解铝所用的原材料(Al2O3和AlF3等)有良好的吸水性能，所携带的水分进入电解液后，或与氟化盐发生水解反应，或被电解成氢和氧，析出的氢通过扩散和Al2O3寄生机制进入铝液，这是电解铝液中氢的主要来源。

On the basis of stripping principle, the mathematical model of removal of tiny moisture in the complexing agent was established, and the solution of this model was carried on by using the software of Matlab.

针对在硼同位素的分离过程中，由于三氟化硼的特殊性质，必须对整个系统的水质量浓度进行控制，而系统中的微量水主要由络合剂引入的问题，根据汽提原理，对络合剂中的微量水份脱除建立数学模型，并利用Matlab软件对此模型进行求解。

In fact, we had obtained polythiophene films with high quality in BF3 ethyl ether, a kind of solvated Lewis acid. The electric conductivity of the polythiophene film is a bout 100 Scm-1. and the tensile strength is as high as 140 MPa, which is forty percent higher than that of aluminum.

事实上，我们已经从一种Lewis酸催化下的低电位聚合体系—噻吩/三氟化硼乙醚溶液中得到了高质量的聚噻吩薄膜，在降低了的聚合电位下得到的聚合物具有优异的力学及电学性能：拉伸强度达140MPa(比金属铝高40%)，电导率则可达100Scm-1。

In fact, we had obtained polythiophene films with high quality in BF〓-ethyl ether, a kind of solvated Lewis acid. The electric conductivity of the polythiophene film is about 100Scm〓, and the tensile strength is as high as 140Mpa, which is forty percent higher than that of aluminum.

事实上，我们已经从一种Lewis酸催化下的低电位聚合体系-噻吩/三氟化硼乙醚溶液中得到了高质量的聚噻吩薄膜，在降低了的聚合电位下得到的聚合物具有优异的力学及电学性能：拉伸强度达140MPa（比金属铝高40％），电导率则可达100Scm〓。

I am accused of being overreligious," she said in her quiet, frank manner,"but that does not prevent me thinking the children very cruel who obstinately commit such suicide.""

客人们在卡罗利娜·埃凯家里，举止就文雅一些，因为卡罗利娜的母亲治家很严厉。

Designed by French fashion house Herm è s, this elegant uniform was manufactured in our home, Hong Kong, and was the first without a hat.

由著名品牌 Herm è s 设计，这件高贵的制服是香港本土制造，是我们第一套不配帽子的制服。