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Both CaCN2 and urea inhibited the chlamydospore germination, mycelial growth and sporulation of the pathogen, but CaCN2 by using at the rates of 0.5 and 1.0%, had two inhibition zones for chlamydospore germination with time while urea had only one. Calcium cyanamide was also more effective on reducing mycelial growth and sporulation of the pathogen than urea did. Therefore, the suppression of pea wilt might be due to fungicidal effect of the intermediate products including hydrogen cyanamide and urea from calcium cyanamide.

由氰氮化钙(0.5及1.0%处理者)之抑制曲线在不同的时间出现两个抑制区,而尿素则仅有一个,及氰氮化钙对萎凋病菌菌丝生长及产胞的影响远较尿素为甚,显示氰氮化钙之所以能有效抑制萎凋病的主要因子,或许是来自其中间产物,包括尿素及氟酸的杀菌作用。

Due to large amount impurity in ammonium fluoaluminate which is used as raw material for the production of fluoride salt ,the smooth operation and the quality of cryolite are affected.

用氟化盐生产的原料氟铝酸铵中机械杂质多,影响了车间正常生产和冰晶石产品质量的现状,提出使用弧形筛过滤料浆,除去其中的机械杂质,来解决上述问题的方案,经生产试用,效果良好,取得了很好的经济效益。

To evaluate the bioactivity of the glass-ceramics,the specimens were soaked in the simulated body fluid. The results indicate that fluorapatite shows needle-like microstructure, which is similar to that in human bone and teeth. The formation of needle-like fluorapatite is related to the heat treatment procedure, which results in needle-like fluorapatite crystals by accelerating one-dimension growth along the c-axis through the screw dislocation growth mechanism. The mechanical properties of the glass-ceramics are close to those of the human bone and teeth. The bioactivity test results show that apatite layer is precipitated on the materials surface after 3 d immersion in SBF, which indicates the glass-ceramics have a good bioactivity.

研究结果表明:氟磷灰石相呈针状,与人体骨和牙齿的磷灰石形貌相似,有利于提高材料的生物活性和生物相容性;氟磷灰石的形成是材料被迅速加热至高温进行热处理,使磷灰石以螺旋位错生长机制沿c轴晶化长大所致;经热处理获得的材料具有优良的力学性能,基本满足骨科和齿科用生物材料的性能要求;材料在体外模拟体液中浸泡3 d后,样品表面已有磷灰石层生成,表明该材料具有较高的生物活性。

In this dissertation, traditional phase-transfer fluorination and solid-solid-liquid triphase-transfer esterification were studied, respectively.

本论文对传统相转移催化氟化和固一固一液三相相转移催化酯化反应进行了系统的研究。

So it has made the great progress. The method studied in this research from o-Dichlorobenzene is a ideal route to synthesize 2,4- dichlorofluorobenzene, which has temperate condition easy to control,safe process,low cost and good quality of products; The method of Phase transfer catalysis fluorination without solvent is better than present technology in presence of DMSO as solvent in many aspects; In a word,it is worth being promoted by the domestic correlative factories.

本课题所研究的以邻二氯苯为原料的2,4-二氯氟苯合成路线反应条件温和,工艺容易控制,生产安全,而且产品质量好,是比较理想的合成路线;以季胺盐为催化剂的无溶剂相转移催化氟化法与溶剂法相比具有明显的优势;通过实验确定的工艺条件对工业化生产有重要的指导意义,可提高以邻二氯苯为原料的工艺路线的市场竞争力。

The crosslinked PEG-20M glass capillary column was prepared by dynamic coating method with boron trifluoride as catalyst,3-glvcidyl-oxypropyl-trimethoxysilane as crosslinking agent.

以PEG-20M为固定相,三氟化硼为催化剂,3-缩甘油氧丙基三甲氧基硅烷(简称KH-560)为交联剂,二氯甲烷为溶剂,对预先用氯化钠沉积法粗糙化的玻璃毛细管柱进行动态涂渍。

The methods of preserving eleostearic acid were studied, adopting content of eleostearic acid as index. Eleostearic acid was esterificated with BF3 in methanol. The content of eleostearic acid was determined by gas chromatography, and the structure is studied by infrared spectroscopy.

初步研究了桐油酸的保存方法,以α-桐油酸含量为指标,将桐油酸与三氟化硼-甲醇溶液进行甲醋化,采用气相色语法检测桐油酸含量,并用红外光语扫描结构。

Using pentaerythritol as initiator, boron trifluoride diethyl etherate as catalyst.dichloroethane as dispersion agent, the chloride polyether polyol is synthesized based on the mechanism of cationic ring-opening polymerization of epiclilnrohyclrin.The azide polyether polyol is synthesized, in DMF through A and sodium azide, and the non-reported azide energetic curing agent is synthesized through the adduction of B and IIDI.

以季戊四醇为起始剂,三氟化硼乙醚为催化剂,1,2—二氯乙烷为分散剂,环氧氯丙烷经阳离子开环聚合反应制成氯化聚醚多元醇,A在N,N—二甲基甲酰胺中与叠氮化钠反应制得叠氮聚醚多元醇,B与六亚甲基二异氰酸酯加成反应制得未见文献报道的叠氮固化剂。

At the same time, we also reviewed the application of NaF as mineralier on the process of molecular sieves synthesis.

同时考察了氟化钠作为矿化剂在分子筛合成过程中的应用。

The titrant is a mixture of EDTA and sodium fluoride, both mercury film electrode and fluorinion selective electrode are inserted in the titration solution. In a process of titration, both the added volume of titrant and the concentration of mercury ion at each titration point can be obtained simultaneously from the potentials of two electrodes, and then the concentration of each component in the alloy can be obtained from the titration curves by multivariate calibration.

用ED-TA与氟化钠的混合溶液作为滴定剂,被滴定液中同时插入了汞膜电极和氟离子选择电极,在滴定过程中的任一滴定点,溶液中汞离子的浓度和滴定剂的加入体积可由两个电极的电位测定值同时获得,从而可应用多元校正法由相应的滴定曲线求得混合金属中每一种组分的含量。

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Lugalbanda was a god and shepherd king of Uruk where he was worshipped for over a thousand years.

Lugalbanda 是神和被崇拜了一千年多 Uruk古埃及喜克索王朝国王。

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