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Nucleophilic opening of the terminalepoxide 57 by a lithium acetylide from 27 in the presence of BF3·EtO furnishedcompound 58, which had the skeleton of target molecule, subsequent conversionsinvolved the introduction of γlactone gave Annonacin.

然后以三氟化硼参与的炔负离子开环氧反应建立分子骨架,得到化合物58。随后经氢化,引入α,β不饱和丁内酯环、去保护等几步反应,就得到Annonacin。

A method of producing crystal sodium fluoride with sodium fluosilicate and sodium carbonate is introduced.

本文介绍了以氟硅酸钠、纯碱为原料生产晶体氟化钠的工艺,并对操作条件作了详细的说明。

The influence of excess anhydrous hydrogen fluoride, the amount of oleum and its trickling rate, t...

在此过程中,本文研究了无水氟化氢过量百分率、发烟硫酸用量及滴加速度、六氟磷酸的加热时间、加热温度以及冷凝介质等因素对五氟化磷产率和纯度的影响。

The influence of excess anhydrous hydrogen fluoride, the amount of oleum and its trickling rate, the time...

在此过程中,本文研究了无水氟化氢过量百分率、发烟硫酸用量及滴加速度、六氟磷酸的加热时间、加热温度以及冷凝介质等因素对五氟化磷产率和纯度的影响。

The influence of excess anhydrous hydrogen fluoride, the amount of oleum and its trickling rate, the time and temperature of heating hexafluorophosphoric acid, and refrigerants on the yield and the content of phosphorus pentafluoride was studied.

在此过程中,本文研究了无水氟化氢过量百分率、发烟硫酸用量及滴加速度、六氟磷酸的加热时间、加热温度以及冷凝介质等因素对五氟化磷产率和纯度的影响。

Optimal conditions for crystallizing have been investigated on a laboratory scale pellet reactor initially seeded with phosphorite.

在流化床诱导结晶法除氟研究中,确定了以磷灰石为结晶核的氟化钙结晶过程中的最佳工艺参数。

Fluoride bioavailability in fluoridated milk is still high and sufficient.

结论氟化牛奶中氟的生物利用率是足够高的。

The aims of our research are exploitation of fluorinated compounds and probing into new fluorinating technology.

本研究以含氟化合物的开发为目的和主线,并以此带动相应氟化反应理论与新技术的研究。

Historically, perfluoropolyethers are the first fluorinated polymers proposed for cosmetics1, and still the most important.

有史以来,全氟聚醚是最先用于化妆品的氟化聚合物,并且目前仍然是最重要的。

Optimum conditions are as follows: DMF is used as solvent, compound quaternary ammonium salt as catalyst, n(p-nitrochloro benzene):n=1: 1.2, m:m(p-nitrochloro benzene)=4%, m:m(p-nitrochloro benzene)1:1, and reacted under 155~160℃ for 18 h; reduction reaction is carried out in methanol with Raney nickel, which is used as catalyst; the raw product is added an antioxidant, and distilled simply under reduced pressure to obtain 4-fluoroaniline with excellence quality, purity is over 99.5%, total yield is 89.3%.

实验结果表明,氟化反应的最佳条件为:二甲基甲酰胺为溶剂、复合季铵盐为催化剂,n:n=1:1.2,m(催化剂:m=4%,m:m=1:1,于155~160℃下反应18h;还原反应在甲醇中进行,以阮内镍为催化剂;粗产品加入抗氧剂,减压条件下简单蒸馏得高品位的对氟苯胺。

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Lugalbanda was a god and shepherd king of Uruk where he was worshipped for over a thousand years.

Lugalbanda 是神和被崇拜了一千年多 Uruk古埃及喜克索王朝国王。

I am coming just now,' and went on perfuming himself with Hunut, then he came and sat.

我来只是现在,'歼灭战perfuming自己与胡努特,那麼,他来到和SAT 。

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三叶草是爱尔兰和圣特里克节的标志同时它的寓意是带来幸运。3片心形叶子围绕着一根断茎,深绿色。