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氟化氧

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For developing an immunoassay for multiple residues of pyrethroid pesticides, the hapten N-2- carbanmoyl-(3"-phenoxyphenyl) methyl 3-(2"-Cldoro-3",3",3"-trifluoropropenyl)-2, 2-dimethylcyclopropane- carboxylate was synthesized from cyanohydrin and 3-(2"-Chloro-3",3",3- trifluoropropenyl)-2, 2-dimethylcyclopropanecarboxylic acid via hydrolysis and esterification. The synthesis of the hapten was foundation of preparaing anti- cyhalothrin polyclonal antibodies.

为了制备对单一拟除虫菊酯高特异性的抗体,以菊酸和氰醇为起始原料,通过水解、酯化反应合成了半抗原N-2-氨甲酰-(3-苯氧基苄基)甲基-3-(2-氯-3,3,3-三氟丙烯基)-2,2-二甲基环丙烷羧酸酯,为进一步制备抗三氟氰菊酯的特异性抗体奠定基础。

Large single crystals were also obtained by using pyrocatechol as additive. It was shown by 〓Si-NMR and IR that Sipyrocatechol complex was formed in the reaction system.

在F〓体系中,F〓对铝源和硅源起络合和矿化作用,形成可溶性氟硅酸盐AlF〓〓、SiF〓〓络合物,然后缓慢水解成含氧氟硅酸盐络合物,它们再发生定向缩聚,提供了分子筛晶体生长所需的可溶性结构单元。

This invention is directed to the-tartaric acid salt of 2-amino-N-{1-(2,4-difluoro-benzyloxymethyl)-2-oxo-2-3-oxo-3a-pyridin-2-ylmethyl-2-(2,2,2-trifluoroethyl-2,3,3a, 4,6,7-hexahydro-pyrazolo(4,3-c) pyridin-5-yl-ethyl}-2-methyl-propionamide which is a growth hormone secretagogue and as such is useful for increasing the level of endogenous growth hormone.

本发明涉及2-氨基-N-{1--(2,4-二氟-卞氧甲基)-2-氧代-2-3-氧代-3a-(R-吡啶-2-基甲基-2-(2,2,2-三氟-乙基)-2,3,3a,4,6,7-六氢化-吡唑子基(4,3-c)吡啶-5-基-乙基}-2-甲基-丙酰胺的--酒石酸盐,它是一种生长激素促分泌素,并且可用于提高内源性生长激素水平。

Six lateral difluorine substituted tolan -type liquid crystals were synthesized via Sonogashira cross-coupling of 4-alkylphenylacetylene and 4-iodo-2,3-difluoro-1-alkoxybenzene under the protection of argon.

用邻二氟苯为起始原料,在-78℃经过两次选择性"邻位金属化"反应、醚化反应、氧化反应制得2,3-二氟-4-碘-1-烷氧基苯,再与4-烷基苯乙炔在氩气保护下进行Sonogash ira偶联反应,制备出6种侧向二氟取代二苯乙炔类液晶。

Study on an efficient process for the preparation of trifloxystrobin starting from 2-methylacetophenone bypartial oxidation,esterification,reaction with methoxyamine,bromization and condensation with 3'- acetophenone oxime.

以邻甲基苯乙酮为原料,经过高锰酸钾的碱性氧化,甲醇酯化,再与甲氧基胺盐酸盐肟化后,用N-溴丁二酰亚胺溴化,最后和间三氟甲基苯乙酮肟缩合得到目标产物肟菌酯。

Benzene perfluorous nonene ether was prepared by the reaction of perfluo-rous nonene (C9F18) and phenol,and the molecular structure of which was identified by IR and NMR spectra.

以全氟壬烯、苯酚和氯磺酸为主要原料,经醚化、磺化和中和反应制备对全氟壬烯氧基苯磺酸表面活性剂,用红外光谱和19FNMR,1HNMR对分子结构进行了表征。

Bezaldehyde was used as protective agent in first method.S-Epichloeohydrin was aminated and acidulated to give(2S)-1-Amino-3-chloro-propanol Salts.The acetylation of (2S)-1-Amino-3-chloro-propanol by acetic anhydride produced the intermediate-N-[2--3-chloropropyl]acetamide.And then at 20℃,in the presence of lithium tert-butoxide,benzyl 3-fluoro-4-morpholinophenyl carbamate react with-N-[2--3-chloropropyl]acetamide to give linezolid in total yield of 43.6%.

路线一采用苯甲醛作保护剂,使S-环氧氯丙烷氨解、酸化生成S-1-氨基-3-氯-2-丙醇盐酸盐,然后经乙酰化反应后,生成中间体-N-[2-乙酰氧基-3-氯丙基]乙酰胺,再用N-(3-氟-4-吗啉苯基)氨基甲酸苄酯和中间体在催化剂叔丁醇锂存在下25℃反应生成利奈唑酮,总产率达到43.6%。

In the process, 2, 4-difluoroaniline is used to carry out ammoniated reaction. Then through a series of similar reactions, the important intermediate of temafloxacin, which is called 7-chloro-6-fluoro-1-(2, 4-difluorophenyl)-1, 4-dihydro-4-oxo-3-quinoline acid, is gained.

与环丙沙星和二氟沙星类似,用2,4-二氟苯胺进行胺化反应,再进行一系列类似的反应,制得合成替马沙星的关键中间体7-氯-6-氟-1-(2,4-二氟苯基)-1,4-二氢-4-氧代喹啉-3-羧酸。

A series of sulfonated poly(phthalazinone ether phosphine oxide)s were prepared via polycondensation of 4-(4-hydroxyphenyl) phthalazinone with sBFPPO and BFPPO.

通过将4-(4-羟基苯基)-2,3-二氮杂萘酮与二(4-氟苯)苯基氧膦和磺化二(4-氟苯)苯基氧膦单体共聚,制备了一系列磺化聚二氮杂萘酮醚三苯基氧膦。

Study on Nitrogen Forms in Chaohu Lake and Wabu Lake Sediments;2. Fluorine, one of the necessary trace elements of human beings is presented in the form s of inorganic and organic compounds in foods, such as sodium fluoride, silicon fluoride, and fluoroacetate etc.

文中阐述了食品中氟的赋存形态及其分析方法,研究了灰化、碱熔、微量扩散、氧瓶燃烧、酸浸提及高温燃烧水解等前处理方法提取氟的形态差异,并对食品中氟的分析提出了建议。

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