氟代苯

The effects of substituents on the nucleophilic reaction of benzyl halide and sodium azide were studied.

合成了叠氮苄、对氰基叠氮苄，对氟叠氮苄，对甲基叠氮苄和联苯二叠氮苄，研究了苯环上不同取代基对苄基卤代物与叠氮化钠经亲核取代反应生成苄基叠氮化物的反应的影响。

CH3OH could attack the phosphor atom in 1,3,2-dioxaphopholane of compiound (1) to give O-methyl O-hydroxyethyl-O-phthalimidoethyl thiophosphate in 85% yield; in the presence of potassium hydroxide aryl selenol could attack the carbon atom in 1,3,2-diox-aphopholane of the cyclic phospholipid conjugate of N^1-(2-furanidyl)-N^3--5-fluorouracil to give the corresponding product of ring-opening in high yields.

在室温下，以异丙醇作溶剂，苯硒酚与化合物2不反应。在氢氧化钾存在下，以异丙醇／水作溶剂（体积比20：1，在室温下，硒酚可以有效地进攻中化合物2中1，3，2-二氧磷杂环戊烷中的碳原子生成相应的开环产物。按照这一反应条件，顺利实现了硒酚对N^1-（2-呋喃基）-N^3-羟烷基-5-氟脲嘧啶硫代环甘油磷脂缀合物的亲核开环，生成甘油骨架的端碳原子上带有芳硒基新颖的磷脂核苷缀合物。

In medium of mixed sulphuric acid and phosphoric acid, with N-phenylated anthranilic acid as a tracer agent, the standard solution of ammonium ferrous sulphate is used to titrate chromium.

试样以硝酸、氢氟酸溶解，加高氯酸冒烟驱除硅和氟，并将铬氧化为六价，在硫磷混合酸介质中，以N-苯代邻氨基苯甲酸为指示剂，用硫酸亚铁铵标准溶液滴定铬。

The intermediates 2a～2f of cyclic (1-arylseleno)glycerol phosphate and tegafur conjugates were synthesized by one-pot reaction of hexaethyl phosphorous triamide, activated by a catalytic amount of iodine, with (N3-tegafur)alkanol, 1-arylselenoglycerol and sulphur successively in refluxing benzene.

以碘作催化剂，无水苯为溶剂，六乙基亚磷酰三胺依次与羟乙基替加氟、1-芳硒基甘油及硫反应，得中间体硒代环甘油磷脂替加氟缀合物2a～2f。

The labia have now been sutured together almost completely.The drains and the Foley catheter come out at the top.

此刻阴唇已经几乎完全的缝在一起了，排除多余淤血体液的管子和Foley导管从顶端冒出来。

To get the business done, I suggest we split the difference in price.

为了做成这笔生意，我建议我们在价格上大家各让一半。