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A filter of capillary electrophoresis signals with online wavelet transform was developed. The online wavelet transform with fixed time window was used and how to select the hest length of time window was discussed.

将在线小波变换用于毛细管电泳信号的滤噪处理,满足了毛细管电泳信号采集过程中实时处理和监控的需求。

Methods: The cyclodextrin, concentration, pH, organic solvent were studied, and the results indicated that the enantiomer of ephedrin and ephedrine levorotatory were baseline separated under the following experimental conditions: uncoated fused silica capillary (75 μm× 68 cm), 25 mmol/L Tris, 2% HP-β-CD and 1% SBE-β-CD, pH was adjusted at 3.0 by phosphoric acid, and 15 kV separation voltage.

以SBE-β-CD和HP-β-CD二元环糊精为手性添加剂,探讨了环糊精种类及浓度、pH、有机溶剂种类等因素对麻黄碱及伪麻黄碱对映体拆分的影响,结果表明:毛细管:未涂渍熔融石英毛细管75μm×68 cm(有效长度60 cm)。分离用缓冲液为25 mmol/L的Tris缓冲液,含2.0% HP-β-CD和1.0% SBE-β-CD,用磷酸调节pH至3.0。

Capillary Electrophoresis as a Method for Determining Hydrolysis Rate Constant of Raffinose Capillary electrophoresis was first employed for the determination of hydrolysis rate constant of trisaccharide raffinose.

测定棉子糖水解速率常数的毛细管电泳方法毛细管电泳首次用于测定三糖的水解速率常数。

And the content of capillary ion chromatography instrument includes micro-flow pump, injector, suppressors, conductometric detectors, UV-Vis detectors and fluorescence detectors with small volumes.

对毛细管离子色谱仪的总结包括微流量泵、小体积进样器、适合毛细管离子色谱系统的小体积抑制器、电导和光学检测器等。

Under the same buffer circumstance, the signals were collected by the amperometric detector and the conductometric detector at the same time using the same Pt wire working electrode and the same counter electrode.

首次采用本实验室自行研制的毛细管电泳多通道电化学检测系统将电导仪和伏安仪并联与同一毛细管电泳系统中,在同一缓冲溶液和同一工作电极下对无机离子和酚类化合物同时进行了检测取得了满意的结果。

And the content of capillary ion chromatography instrument includes micro-flow pump, injector, suppressors, conductometric detectors, UV-Vis detectors and fluorescence detectors with small volumes.

对毛细管离子色谱仪的总结包括微流量泵、体积进样器、合毛细管离子色谱系统的小体积抑制器、导和光学检测器等。

Adsorption isotherms of propane, butane, propane and liquified petroleum gas on the quartz beads were determined respectively by means of the method of vacuum weighing , and the relationship between the isosteric adsorption enthalpy change and adsorbance was also reported.

用石英玻璃微珠模拟了HP-1,HP-20M,HP-17毛细管色谱柱内壁,用真空重量法测定了丙烷、丁烷、丙烯、液化石油气样品在3种模拟毛细管内壁表面的吸附等温线,并计算了等量吸附热随吸附量的变化关系。

In the first part, the development of researches in TCM with CE and NACE was reviewed. In the second part, the content of two kinds of TCM was analyzed by CE and NACE, respectively.

然后将毛细管电泳技术用于中药厚朴和吴茱萸的成分分析中,建立了两种不同的毛细管电泳方法。

In this thesis, a pulled bare capillary tip was proposed to be used as the ESI emitter. The outside surface of the tip was neither coated with electric-conductivity materials nor subjected to an external high voltage. Thus, there is no concern such as short lifetime that generally observed in conventional sheathless tips.

本论文尝试直接利用高温拉制及氢氟酸处理过的毛细管尖端做为电喷洒尖端,此设计不需要涂布导电材料及施加第二组电压於毛细管尖端处,此无鞘流界面因此能够避免因导电材料涂布不密合稳定而造成的易脱落及寿命短等问题。

The microheterogeneity and tryptic fragments of glycoprotein recombinant human erythropoietin were analyzed by high performance capillary electrophoresis.

用高效毛细管电泳测定了重组人促红细胞生成素的微多相性、肽图,同时采用毛细管电泳质谱联用技术鉴定了部分非糖基化胰酶消解片段和O-126糖基化肽的结构。

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