毛细管

A very large sample plug was introduced hydrostatically into the capillary (65 cm×50 μm i.d., effective length of 35 cm) over 80 s at a height difference of 11 cm. The working conditions for CE-FA separation are as follows: operating voltage, 10 kV; running buffer, 67 mmol/L phosphate, pH 7.4. The unbound ketoprofen concentration was directly measured from the height of the frontal peak.

一大体积样品虹吸进样至未涂层毛细管(65 cm×50 μm i.d。，有效长度35 cm)，进样时间80 s，毛细管两端高度差11 cm，工作电压10 kV，运行缓冲液为67 mmol/L磷酸盐缓冲液(pH 7.4)，游离酮洛芬浓度由前沿峰的高度直接测定。

Adsorption isotherms of propane, butane, propane and liquified petroleum gas on the quartz beads were determined respectively by means of the method of vacuum weighing , and the relationship between the isosteric adsorption enthalpy change and adsorbance was also reported.

用石英玻璃微珠模拟了HP－1，HP－20M，HP－17毛细管色谱柱内壁，用真空重量法测定了丙烷、丁烷、丙烯、液化石油气样品在3种模拟毛细管内壁表面的吸附等温线，并计算了等量吸附热随吸附量的变化关系。

In the first part, the development of researches in TCM with CE and NACE was reviewed. In the second part, the content of two kinds of TCM was analyzed by CE and NACE, respectively.

然后将毛细管电泳技术用于中药厚朴和吴茱萸的成分分析中，建立了两种不同的毛细管电泳方法。

The content of naphthalin in circulating wash oil was determined by capillary column gas chromatography with DB-1 capillary column and FID detector.

采用DB-1毛细管柱和FID检测器，以毛细管柱气相色谱法测定循环洗油中的萘含量。

Based on noncontinuous spray for each sprayer, the multiplex low flow system was achieved by applying ESI potential sequentially to the four low flow sprayers, resulting in only one sprayer being sprayed at any given time.

为了使低流速鞘流界面可被应用在多通道毛细管电泳质谱，我们利用非连续电喷洒的概念，使此四根毛细管电泳产生序列式喷洒，再与质谱仪同步化。

A pCEC instrument to study the separation behavior of solutes on 320μm CEC column was established, and the separation of neutral solutes with low concentration organic salt as the mobile phase was realized. Furthermore, nine compounds with similar structure were separated in a saltless system.

采用搭建的加压毛细管电色谱仪探讨了溶质在320μm内径毛细管柱上的分离行为，并且在低浓度的有机盐溶液作流动相条件下实现了中性溶质的分离。

A pCEC instrument to study the separation behavior of solutes on 320 um CEC column was established, and the separation of neutral solutes with low concentration organic salt as the mobile phase was realized. Furthermore, nine compounds with similar structure were separated in a saltless system.

采用搭建的加压毛细管电色谱仪探讨了溶质在320 μm内径毛细管柱上的分离行为，并且在低浓度的有机盐溶液作流动相条件下实现了中性溶质的分离。

In this thesis, a pulled bare capillary tip was proposed to be used as the ESI emitter. The outside surface of the tip was neither coated with electric-conductivity materials nor subjected to an external high voltage. Thus, there is no concern such as short lifetime that generally observed in conventional sheathless tips.

本论文尝试直接利用高温拉制及氢氟酸处理过的毛细管尖端做为电喷洒尖端，此设计不需要涂布导电材料及施加第二组电压於毛细管尖端处，此无鞘流界面因此能够避免因导电材料涂布不密合稳定而造成的易脱落及寿命短等问题。

CD was added into running buffer in above electrophoresis system, and the separation efficiency of polycarboxylic acids was improved further by the supramolecular interaction. Based on that, the method for separation and determination of several di- and tricarboxylic acids, including oxalic, malic, tartaric and citric acids, found in fruit juices was developed, which supplied a fast, convenient and sensitive method for the food analysis, the quality control of foods and various drinks.

果汁中多元有机酸的毛细管区带电泳/Cu电极安培检测在上述分析体系的电泳介质中添加β-CD，利用CPB与β-CD的协同超分子作用，进一步提高了多元有机酸的分离效率，成功实现了水果中四种常见多元有机酸草酸、柠檬酸、苹果酸、酒石酸的基线分离，建立了几种果汁中上述有机酸毛细管区带电泳/Cu电极安培检测定量测定方法，为食品分析、食品饮料质量控制以至辨别酒类商品真伪等提供了一种方便、快速、灵敏度高的分析方法。

The microheterogeneity and tryptic fragments of glycoprotein recombinant human erythropoietin were analyzed by high performance capillary electrophoresis.

用高效毛细管电泳测定了重组人促红细胞生成素的微多相性、肽图，同时采用毛细管电泳质谱联用技术鉴定了部分非糖基化胰酶消解片段和O－126糖基化肽的结构。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失