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Methods: Using proper sample treatment method, applying non-polar capillary column (HP-1) to replace packed column for the determination of sodium cyclamate in food.

采用适当的样品处理方法,应用弱极性的HP-1毛细管柱取代填充柱检测食品样品中的甜蜜素。

In this study,a simple and useful method,gas chromatography with FID detection,was employed to measure sodium cyclamate in food.

甜蜜素是我国食品行业中应用最多的一种甜味剂,介绍了一种毛细管柱气相色谱法在测定食品中甜蜜素的方法方面的应用,此法简便、快速、实用、成本低,线性范围0.01g/kg~5.0g/kg,检出限为0.01g/kg,RSD为2.1%~4.4%,回收率为94%~99%。

The method of determination of cyclamate in foods adopts Carrez reagents and ultrasonic extraction to eliminate the effect of protein and so on, use ultrasonic extraction and large caliber capillary. It is simple, rapid, with high precision and accuracy of the merits.

通过对样品采用Carrez试剂消除蛋白质等影响,超声波萃取,使用大口径弱极性毛细管具有简便、快速,精密度和准确度高的优点。

Polystyrene,polyethylene and their deuterated polymers are important fuel container materials of Z-pinch driven ICF experiment. To meet the shape demand of physical experiment,filaments with the diameter of 30~100 μm were prepared by melt spinning via high pressure capillary rheometer and its accessory section HAUL-OFF system.

聚苯乙烯,聚乙烯及其的氘代物是Z箍缩驱动惯性约束聚变实验中的重要固体燃料容器材料,针对物理实验对其形状的特殊要求,利用高压毛细管流变仪及HAUL-OFF熔体拉伸测试单元进行熔融纺丝,制备出直径为30~100 μm的聚合物丝样品。

A method for Pendimethalin quantitation was established by using diamyl phthalate as internal standard with GC. The chromatographic column was HP-5, and temperature program was used: 200℃ for 0.5 min, programmed to rise at 10℃ to 240℃, then isothermal for 2.5 min.

采用HP-5石英毛细管色谱柱和FID检测器,以邻苯二甲酸二戊酯为内标物,在适宜的色谱条件下对二甲戊灵原药进行定量分析。

The focused protein zones were eluted to the entrance of MS by combining cathodic mobilization with gravity.

已聚焦好的蛋白质区带通过结合阴极移动和重力移动的方法从毛细管中流出而进入质谱仪。

Sitafloxacin epimers were separated by capillary zone electrophoresis using γ-cyclodextrin and D-phenylalanine as chiral selector.

以γ-环糊精和D-苯丙氨酸为手性选择剂,采用毛细管区带电泳成功地分离了新型抗菌素西他沙星差向异构体。

A baseline separation of Sitafloxacin epimers was achieved with a background electrolyte of 10 mmol/L KH2PO4-K2HPO4 (pH 4.5), 10 mmol/L CuSO4, 20 mmol/L γ-CD and 10 mmol/L D-Phe. The linear range for Sitafloxacin was 32-400 mg/L (0.996). The relative standard deviations of migration time and peak area were less than 1.9% and 3.8% respectively.

实验结果表明,添加剂的种类和浓度是影响西他沙星手性分离的重要因素,只有当D-苯丙氨酸、铜离子和γ-环糊精同时存在并达到一定浓度时,西他沙星差向异构体在毛细管电泳中才具有良好的分离效果。

However, in contrast with the extensive employment of cyclodextrins and crown ethers, the application of calixarenes in CE was limited.

但与环糊精和冠醚的广泛应用相比,杯芳烃在毛细管电泳中的应用研究才刚刚开始,是一个有待开发的新领域。

The effects of the catalyst on the graft levels for different PP powder were experimented. The graft product was characterized by infrared spectrophotometer , melt flow viscosity and differential scanning calorimeter .

考察了在反应过程中加入催化剂对不同PP粉接枝率的影响,采用红外谱图、毛细管流变仪和差热分析等手段对接枝物进行表征。

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每逢看到沃林顿那刚毅的脸,那乌黑、忧郁的眼睛,她便会相信,他一定作过不幸的爱情的受害者。

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