毛细管

Respectively, glutamic acid derivatized β-CD has been synthesized with epoxy chloropropane as the intermediate, a water-insoluble yellow liquid was got after the acetylating of the by using acetic anhydride, which was used as a novel gas chromatographic CSP; A water-soluble β-CD polymer cross-linked with epoxy chloropropane has been synthesized, and the derivatives of β-CD polymer were synthesized by its alkylating and acetylating. The different β-CD derivatives were coated on silica capillary columns by dynamic method, the chromatographic properties and retention behaviors of the fused silica capillary columns were studied, the results showed that the β-CD derivatives had good stereoselectivity and separation results to some compounds, especially to various positional isomers and enantiomers.

本文还分别以环氧氯丙烷为中间体，合成了七{2，6-二-O-[3-(1，3-二羟基丙氨酸)]}-β-环糊精，再用醋酸酐将其乙酰化，得到了一种淡黄色粘稠液体，合成了一种新型的环糊精衍生物；以环氧氯丙烷作交联剂合成了一种水溶性的β-环糊精聚合物，再将其烷基化和酰基化，合成了β-环糊精聚合物的不同衍生物，用动态法将不同类型的β-环糊精衍生物涂渍在石英毛细管柱上，通过对所制备柱柱性能的测试和对一系列化合物的分离和保留行为的研究，结果表明所合成的β-环糊精衍生物对各类化合物，特别是对位置异构体和对映异构体具有较好的分离效果，显示了很强的立体选择性。

This paper gives a brief review of two methods of soft lithogra phy-microcontact printing and micromolding in capillaries.

本文介绍了较早出现的软刻印术的两种方法———微接触印刷法和毛细管微模制法。

The concentration distribution of polymer solution prior to gelling has been numerically studied with self-consistent field theory.

采用连续自洽场理论分析了毛细管中发生凝胶化之前的聚合物溶液浓度分布的影响因素及其规律。

The design was optimized for maximum signal intensity by simulation and experiments. The size of focal spot in the micro-channel capillary was optimized. Fluorescence signal was enhanced 2～3 times when increasing the diameter of focal spot from 10μm to 50μm (full of the inner wall of capillary), through which the sensitivity and signal-noise ratio were also improved. A technique of using refractive matching liquid was presented. The fluorescence signals were boosted up and the signal collection efficiency was also meliorated when using this method.

通过理论分析和实验优化本系统的设计：优化聚焦于微通道中的激发光斑大小，增大聚焦到毛细管内径中的激发光斑尺寸，使光斑尺寸由最小的10μm增大到50μm，光电倍增管接收到的荧光信号提高了2-3倍，从而提高系统的信噪比和灵敏度；提出在聚焦物镜处加折射率匹配液的方法，加匹配液后的荧光信号得到了增强，因而提高了荧光收集效率和灵敏度。

Capillary electrophoresis was employed to quantitating the intercellular organic acids. The acquired data were subjected to multivariate analysis.

利用毛细管电泳技术对2种菌在不同抗生素作用下细胞内的主要有机酸进行检测，然后通过多变量统计分析对数据进行处理。

The capillary electrophoresis using non-gel sieving matrices is one of the most important techniques for DNA separation.

使用无胶筛分介质的毛细管电泳是最重要的DNA分离技术之一，通常使用无交联的高分子溶液作为无胶筛分介质。

The factors that affect the sample stacking process have been analyzed in detail by using a 1-D mathematic model.

本文在已有数学模型的基础上，对影响毛细管电堆积富集过程的因素进行了分析。

Crude petroleum and liquid or solid petroleum products - Determination of density or relative density - Capillary- stoppered pyknometer and graduated bicapillary pyknometer methods (ISO 3838:1983); German version EN ISO

原油和液体或固体石油产品。密度或相对密度的测定。毛细管塞阻比重瓶法和带刻度双毛细菅比重瓶法

Common transparent quartz tube SiO2 more than 99.9% purity, geometry, chemical stability, thermal stability, resistance to thermal denaturation and anti-crystallization properties of the fine, optical transmittance above 93%; from hydroxyl in hydroxyl tube below 10ppm, after vacuum from hydroxyl, hydroxy-up to 5ppm below apply to high-pressure mercury lamp, sodium lamp, metal halide lamp, such as low-hydroxy products; white pipe, used mainly for heating tube, heating tube, far infrared control the manufacture, milky quartz pearl quartz tube possession of new technology, the management side as if the surface of pearls, all aspects of performance than ordinary white tube better; filter tube to filter out ultraviolet UV band in the harmful wavelengths of 190-320nm ultraviolet light source applied to environmental protection manufacturing; no ozone UV filter tube and pipe the contrary, through the ultraviolet wavelength around 253.7nm, there is no ozone UV lamp main material, widely used in medical equipment, water treatment, food hygiene, such as sterilization; quartz casing diameter 8-120mm in between, has a single opening, double opening round, flat-top shape and widen the mouth of necking, flanging, sanding and other processing, high temperature resistance, corrosion resistance, good light transmission and moisture-proof, explosion-proof characteristics such as widely used in aquarium thermostat, disinfection equipment, heating pipes, water treatment, metal halide lamp, such as product manufacturing and environmental protection, health, chemical and other fields; quartz Clamshell specifications 8-180mm, the shape according to the customer requirements, the bubble shell can take capillary has to carry out the exhaust, high temperature, light transmission is good, mainly for JC, JD, H1-H7, the stage lights and high-pressure mercury lamp, sodium lamp, metal halide lamp, such as product manufacturing; quartz water jacket mainly used in printing and packaging processing industry ---- UV light-curing, UV light curing is a very reliable and can be used to replace hot air dryers and other drying technique of curing technology, which in the printing and packaging of the processing industry has been widely.

普通透明石英管SiO2纯度达99.9%以上，几何尺寸、化学稳定性、热稳定性、抗热变性和抗析晶性能优良，光学透过率达93%以上；脱羟管羟基在10ppm以下，经过真空脱羟，羟基可达5ppm以下，适用于高压汞灯、钠灯、金卤灯等低羟基产品；乳白管，主要用于发热管、加热管、远红外管的制造，珠光石英管乳白石英管之新工艺，管面好象珍珠的表面，各方面性能比普通乳白管更优；滤紫外线管能够滤除紫外光谱波段中对人体有害的190-320nm波长的紫外线，适用于环保光源的制造；无臭氧管与滤紫外线管相反，可透过253.7nm左右波长的紫外线，是无臭氧紫外线杀菌灯的主要材料，广泛用于医疗器械、水处理、食品卫生等杀菌；石英套管直径范围在8-120mm之间，有单开口、双开口、圆头、平头等外形和扩口、缩口、翻边、磨砂等加工，具有耐高温、耐腐蚀、透光性好及防潮、防爆等特点，广泛使用于水族恒温器、消毒设备、加热管、水处理、金卤灯等产品的制造和环保、卫生、化工等领域；石英泡壳规格Φ8-180mm，形状根据客户要求，泡壳上可以接有毛细管，可进行排气，耐高温，透光性好，主要用于JC、JD、H1-H7、舞台灯和高压汞灯、钠灯、金卤灯等产品的制造；石英水套主要用于印刷和包装加工工业---- UV光固化， UV光固化是一种十分可靠的、可取代热空气干燥机和其他干燥技术的固化技术，它在印刷和包装加工工业已经得到广泛应用。

Preparation of quasi-interpenetrating network/functionalized gold nanoparticle composite matrix and its performance for DNA sequencingA new matrix additive,PDMA-functionalized gold nanoparticle, was prepared by "grafting-to" approach to avoid GNP aggregation at high concentration of salt in buffer solution,and then incorporated into quasi-IPN composed of LPA(3.3 MDa) and PDMA to form novel polymer/metal composite sieving matrix(quasi-IPN/GNP-PDMA) for DNA sequencing by CE.

准互穿聚合物网络/官能化的金纳米粒子复合介质的制备及其用于DNA测序性能的研究为了解决GNPs在高盐浓度下易附聚的问题，由&grafting-to&法制备了一种新型介质添加剂，即PDMA官能化的GNPs，并将其加入到由LPA(3.3 MDa)和PDMA所组成的quasi-IPN中得到了用于毛细管电泳DNA测序的聚合物/金属复合筛分介质(quasi-IPN/GNP-PDMA)。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失