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Methods The background electrolyte was 50 mmolL^(-1) sodium borate containing 5% acetonitrile. The voltage was 12 kV and the wavelength was set at 228 nm. The fingerprint, produced from electropherograms of ten different batches of samples, was established and 11 common peaks were confirmed.

以的50 mmolL^(-1)硼砂(含体积分数为5%的乙腈溶液)为背景电解质,运行电压12 kv,紫外检测波长228 nm,以10个不同产地药材的电泳图谱建立了甜瓜蒂毛细管电泳指纹图谱。

With an effective length of 30 cm. The running buffer was a mixture of 25 mmol/L sodium borate and 100 mmol/L boric acid (pH 8.6). Effective mobilities of the two medicines changed with altering the concentration of β-cyclodextrin.

所用未涂层熔融石英毛细管的规格为内径50 μm,总长37 cm,有效长度30 cm,电泳缓冲液为25 mmol/L硼砂+100 mmol/L硼酸(pH 8.6),并加入不同浓度的β-CD。

The rice bran protein can be separated by GP-HPLC with AUC buffer solution. 40 gliadin components and 20 low-molecular weight glutenin subunit could be separated by HPCE with the buffer solution of alkaline sodium borate from wheat. Therefore the differences between varieties can be identified.

用AUC缓冲液和排阻色谱能有效分离米糠蛋白;用毛细管电泳和碱性硼酸钠缓冲液分离小麦蛋白,可得到40多个醇溶蛋白组分和20多个低分子量谷蛋白亚基,以此可鉴别品种差异。

The optimal separation for capillary electrophoresis is 20% methanol, and 0.13mM of β-cyclodextrin in 25mM sodium tetraborate buffer solution(pH 9.1), and 20℃of temperature.

实验结果显示最佳化的毛细管电泳分离条件为25mM四硼酸钠溶液(pH= 9.1),添加0.13mM β-cyclodextrin 及20%甲醇溶液。

Results: The satisfactory separation was achieved on optimization of electrophoretic condition: 0.08 mol·L-1 heptane-10% isopropanol - 0.01 mol·L-1 sodium tetraborate buffer - 0.12 mol·L-1 SDS (pH 9.0) as microemulsion with on - column UV monitoring at 214 nm,25 kV applied voltage, 30 ℃ column temperature.

微乳毛细管电泳在吉他霉素组分分离方面的成功应用,为结构相似的中性物质的分离提供了一种新方法,也为日后的定量测定提供了依据。

The spectrograph system will be used to detect the XUV emission from capillary discharge plasma.

最后,利用标定后的平场谱仪对毛细管放电不同气体等离子体辐射进行了初步的测谱实验。

The spectrograph system will be used to detect the XUV emission from capillary di...

最后,利用标定后的平场谱仪对毛细管放电不同气体等离子体辐射进行了初步的测谱实验。

This paper established a method of analysis of taurine by spectrophotometry and discussed the factors that affected spectrophotometry.

本文研究了毛细管电泳测定牛磺酸的方法,采用萘-2,3-二甲醛和牛磺酸反应,衍尘为电化学活性的物质,进行电泳测定,并对衍生反应条件和电泳分析条件进行了优化,建立了一种测定牛磺酸的新方法。

The interactions of Strychnos alkaloids, fangchinoline,tetrandrine and carbamazepine with serum albumin were studied by fluorescencequenching spectra, synchronous fluorescence spectra, three-dimensional fluorescencespectra and ultra-v...

在系统查阅有关文献资料的基础上,进行了以下研究工作:(1)采用在线推扫预富集—胶束毛细管电泳法建立了测定中草药中马钱子生物碱的新方法。

In the thesis, CE was combined with on-line sweeping and hollow fiber-basedliquid-phase microextraction technique. Efficient and sensitive methods were developedfor the determination of Strychnos alkaloids, carbamazepine in Chinese herbal medicinesand biological samples. The interactions of Strychnos alkaloids, fangchinoline,tetrandrine and carbamazepine with serum albumin were studied by fluorescencequenching spectra, synchronous fluorescence spectra, three-dimensional fluorescencespectra and ultra-violet spectra.

本论文将毛细管电泳分离技术与在线推扫富集技术、中空纤维液相微萃取技术相结合,建立了中草药和生物样品中的马钱子生物碱、卡马西平的高效、灵敏和选择性好的CE分离检测方法。

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