毛细管

It was found that the time taken to establish equilibrium values of the capillary constant depends on the level of the meniscus of the liquid phase of the ROS with respect to the level of the liquid in the experimental cell and, as mentioned above, on the temperature and

结果发现，所需要的时间来建立平衡的价值观毛细管常数，就看水平，半月板的液相中的活性氧与尊重级的液体在实验细胞，而正如上文所述，对温度及

Based on the previous literatures, the following major innovation works were carried out in this dissertation:(1) The derivatization reaction conditions of ephedrine and pseudoephedrine with sensitive derivation reagent in aqueous system were studied and two new methods were developed for the assay of them by microemulsion electrokinetic chromatography and micellar electrokinetic chromatography with LIF detection. The sensitivity and analysis times were greatly improved compared with the previous reports;(2) A new method of CZE with indirect LIF detection was developed for the simultaneous determination of six coumarin compounds (esculin, esculetin, isofraxidin, genistein, naringin and sophoricoside) with fluorescein as the probe. The proposed method enlarges the application range of LIF detector, and provides new approach for the analysis of certain compounds difficult to derivatize;(3) Based on the above research, an MEKC with indirect LIF detection method for the simultaneous determination of adenine and guanine in DNA extracts from fungus, maize and soybean was established;(4) A new method for the investigation of the complexes formed between human serum albumin and ampicillin sodium under the simulated physiology conditions using laser light scattering technique was developed.

该论文在综述前人工作的基础上，开展了如下未见文献报道的创新性的研究工作：(1)使用灵敏的衍生试剂对麻黄碱和伪麻黄碱在水体系中的衍生反应条件进行了系统研究，建立了微乳电动色谱-激光诱导荧光检测法和胶束电动色谱—激光诱导荧光检测法测定麻黄碱和伪麻黄碱的灵敏分析新方法，与以前的报道相比，灵敏度和分析时间均有很大改善；(2)使用荧光素钠作为背景荧光试剂，建立了同时分析测定六种黄酮类化合物(秦皮甲素、秦皮乙素、异秦皮定、染料木素、柚皮苷和槐角苷)的毛细管区带电泳—间接激光诱导荧光检测新方法，扩大了激光诱导荧光检测的应用范围，对难衍生化合物的分离分析提供了一种新思路和新途径；(3)以荧光素钠作为背景荧光试剂，建立了一种用于同时测定食品提取DNA中的腺嘌呤和鸟嘌呤含量的胶束电动色谱—间接激光诱导荧光检测新方法；(4)用动态和静态激光散射法研究了模拟生理条件下人血清白蛋白与氨比西林钠盐相互作用所形成的复合物，为药物分子与蛋白质的相互作用、药代动力学等的研究提供了一种新思路。

The proposed method surpassed other chromatographic alternatives in terms of limit of detection at least 10~3 folds with good reproducebility. Chapter 4 A capillary zone electrophoresis with indirect LIF detection method is developed for the simultaneous determination of six coumarin compounds (esculin, esculetin, isofraxidin, genistein, naringin and sophoricoside).

第四章建立了一种毛细管区带电泳—间接激光诱导荧光检测法同时测定6种黄酮类化合物(秦皮甲素、秦皮乙素、异秦皮定、染料木素、柚皮苷和槐角苷)的新方法，扩大了LIF检测的应用范围。

Capillary electrophoresis separation and determination of the sex hormones, estriol, 17βestradiol, estrone, corticosterone, testosterone and progesterone were examined, using SDS and βcyclodextrin as Trisboate running buffer additive.

本文采用加入表面活性剂SDS和β环糊精的Tris 硼酸作为电泳溶液体系，对毛细管电泳法分离测定雌三醇，雌二醇，雌酮，皮质酮，睾酮和孕酮等六种天然性激素的条件进行了探讨。

A capillary GC method with temperature program for determination of eugenol in essential balm wasestablished.

建立了毛细管气相色谱法测定清凉油中丁香酚的含量。

We found that luminescent CdTe/CdS QDs prepared in aqueous phase very facilely conjugated to antibodies based on their strong adsorption.

运用毛细管电泳-激光诱导荧光检测、荧光光谱法和荧光相关光谱法对量子点-抗体标记产物进行了分析。

Wheat gliadins composition can be regarded as finger-print for varietal identification. The method of isolation and identification for wheat gliadin are SPAGE, RP-HPLC and CE techniques, three of them are complementary, CE is the most powerful tool.

小麦醇溶蛋白组成可以作为小麦品种鉴定的指纹图谱，其分离方法有酸性电泳、反相高压液相色谱和毛细管电泳等手段，3种方法相互补充，而CE分辨率最高。

In the second chapter, a microchip capillary electrophoresis with laser-induced fluorescence detector was constructed for separation and detection of riboflavin and flavin mononucleotide.

在第二章中，研究建立芯片毛细管电泳-激光诱导荧光分离分析核黄素和黄素单核苷酸的方法。

In this paper, the contents of total flavone were determined in Tropaeolum majus by capillary electrochromatography.

本文采用毛细管电色谱法测定了旱莲中总黄酮的含量。

When a capillary tube, in whose inner hole an optical fiber has been fixed and whose axial deviation amount between an outer peripheral surface of the capillary tube and a core center of an end surface of the optical fiber is 1.5 mum or less, is inserted into the insertion portion of the thin tube and the end surface of the optical fiber is fixed at a position at which a distance of the end surface to a focal point position of the partially spherical lens becomes -40 mum or less, emission light has an emission light bend of 0.2 DEG or less with respect to the center axis of the thin tube.

当将光纤固定在内孔且外周面与光纤的端面的纤芯中心的轴偏移量在1.5μm以内的毛细管插入细管的插入部，并且将光纤的端面固定于部分球面透镜的焦点位置±40μm以内的距离的位置上时，出射光曲率为出射光相对细管中心轴在0.2°以内。

We are in a real jam.

我们的麻烦大了。

Hey, it's Ahmet from India, that foreign exchange guy.

看，那是印度的阿曼特，国际交换生