比色温度

A series homopolyme of ethylene synthesised by metallocene catalyst was analyzed by the high temperature gelatin permeation chromatography. The results showed that the molecular weight distribution changed not too much when the ratio of Al/Ti ranging between 1000 and 4000, while the molecular weight distributed increased from 2.48 to 2.81 when the ratio ranging between 4000 and 7000; catalyst D had the lowest activity to be used as asymmetric metallocene catalyst; the curve of molecular weight moved much to the left with the increases of temperature and two active centres appeared when the temperature is 70℃.

通过高温凝胶渗透色谱对茂金属催化合成的一系列乙烯均聚物进行了分析，可以看出Al/Ti比从1000变到4000时，分子量分布曲线图变化不大，而从4000变到7000时，变化相当大，分布宽度从2.48增至2.81；催化剂D的活性最小，可作为非对称性茂系金属催化剂；该聚合体系分子量的大小受聚合温度的影响很明显，随温度的升高，分子量分布曲线图向左发生很大位移，在聚合温度为70℃时存在两个活性相当的活性中心。

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First of all, this study will be multi-walled carbon nanotubes by chemical oxidation process purified so it can be modified to deal with than the purification of purity before the modified 5 wt%, more than 1.89 times the surface area to increase the surface potential decrease of about 10 ~ 20 mV and the surface functional base (-COOH and-OH) to increase 1.45 times, and then the control technology of electroless preparation parameters include: analysis of plating time, plating analysis of temperature, metal ions in solution than the (Fe2+/ Ni2+), bath pH and the added value of dispersion Agent and other research towards Fe-Ni particles to increase the iron content and Fe-Ni particles spread in the MWCNT upper fixed targets,the results found that when the parameters for the preparation of 50 ℃, pH10, do not add dispersant, metal ions than the solution (Fe2 +/ Ni2 +) 7, the highest iron content can be Fe = 40.55 at%(flat iron content 111.17 mg / g) of nanocomposites Fe-Ni/CNT, then for a series of the nature of its analysis, the final evaluation Fe-Ni/CNT nanocomposites were processed on the effectiveness of the application of mixed pollutants, the results showed that in 120 minutes at the same time when Adsorption of heavy metal ions lead nitrate 10 ppm, selenium heavy metal ion degradation of 1 ppm and orange azo dye AO7 50 ppm standard of effluents, and after a total Fe-Ni nano-particles to SEM / EDS analysis of more than 50% still remaining.

本研究首先将多壁奈米碳管以化学氧化法做纯化改质处理能使其纯度较纯化改质前提高5 wt％、比表面积提高1.89倍、表面电位下降约10~20 mV以及表面官能基提高1.45倍，再控制无电镀技术之制备参数包括：析镀时间、析镀温度，镀液中金属离子比(Fe2+/Ni2+)、镀液pH值及是否添加分散剂等，研究朝提高Fe-Ni粒子的含铁量与Fe-Ni粒子散布固定在MWCNT上等目标进行，研究结果发现当制备参数为50 ℃、pH10、不添加分散剂、镀液金属离子比(Fe2+/Ni2+)7时，可得到最高铁含量Fe = 40.55 at％(单位铁含量111.17 mg/g)之奈米复合材料Fe-Ni/CNT，接著对其作一系列性质分析，最后评估奈米复合材料Fe-Ni/CNT对共处理混合污染物之应用效益，结果显示其在120分钟时能够同时吸附重金属硝酸铅离子10 ppm、重金属硒酸根离子1 ppm及降解偶氮橘色染料AO7 50 ppm达放流水标准，且共处理后奈米Fe-Ni粒子以SEM/EDS分析仍剩余50 %以上。

A method for the determination of residual pentane content in de-oiled asphalt of Liaohe heavy crude vacuum residuum was studied by using static headspace gas chromatography. The effects of gas-liquid phase ratio, equilibrium time and equilibrium temperature on headspace analysis were investigated.

采用静态顶空气相色谱法测定辽河稠油减压渣油高软化点脱油沥青中戊烷的含量，确定了色谱的测定条件，研究了气液相比、平衡时间、平衡温度等因素对定量分析的影响。

And on the basis of mono-factor test, using COD decreasing rate and decolour rate as targets, six factors affecting catalytic effect were selected to proceed L9(34) orthogonal experiments. The conclusion of primary and secondary factors was drawn and the turn was : kind of catalyst-amount of catalyst-pH value-temperature-amount of H2O2-amount of air . The optimization were determined to be : initial pH value : 5.5 ; temperatare : 90 C; amount of H2O2: lml/400ml waste water ; kind of catalyst: AC3 ; inciting small amount of air ; amount of catalyst: 125g activated carbon to 500g stone .

并在单因素试验的基础上，以废液COD去除率和脱色率为指标，选择废液初始pH值、反应温度、启动剂用量、催化剂类型、鼓空气量、催化剂加入量为因素，进行L_9(3~4)正交试验，确定影响因素因素的主次关系为：催化剂类型→催化剂加入量→废液初始pH值→反应温度→启动剂量→鼓空气量；最佳处理技术条件为：废液初始pH5.5；反应温度90℃；启动剂量1ml／400ml废液；AC3型催化剂；鼓小流量空气；炭石比125g／500g。

Different samples' absorbent was determined in the condition of different colorimetric time ,different samples' temperature and different freshness,it prove that the result was relative to different experiment conditions in order to master the key point and ensuer the accuracy of the result in experiment.

啤酒双乙酰的含量是啤酒质量评价中的一项非常重要的指标，通过对不同样品在不同的比色时间、不同的样品温度及新鲜程度条件下测定其吸光度，得出不同实验条件对测定结果的影响，以求在实验中掌握好其关键点，确保测定结果的准确性。

Methods by using a broad pH range column(Gemini NX C18,4.6mm×150mm,5μm),basic mobile phase which was[H_2O-ammonia-glacial acetic acid] (96:3.6:0.4)-methanol,the related substances in etimicinsulfate were separated and detected by electrospray ionization and positive ion monitoring,the ESI ion source condition was following: temperature is 350℃,nebulizing pressure is 50 psi,dry gas flow is 10 L /min.some related substances in etimicinsulfate were identified by comparing the retention time in chromatography,~+ spectrum and MS~2 spectrum with reference substances\',the others which haven\'t reference substances were identified or speculated by analyzing their MS~2 fragmentation with the help of a rule summarized from the MS~2 fragmentation of gentamicin C1a,micronomicin and etimicin.Results nineteen related substances in etimicinsulfate were separated and detected.

方法利用宽pH范围的Gemini NX C18(4.6mm×150mm，5μm)色谱柱，在碱性条件下，以[水-氨水-冰醋酸(96：3.6：0.4)]-甲醇(70：30)为流动相，直接分离各组分；并用HPLC-ESI-MS~2检测样品中各组分，质谱条件：ESI离子源，离子源温度350□，雾化室压力50 psi，干燥气流速10 L/min，正离子检测方式；对有对照品的有关物质采用比对有关物质与对照品的色谱保留时间、准分子离子的质荷比及二级质谱方法进行鉴定，无对照品的有关物质，则是先通过解析庆大霉素Cla、小诺霉素、依替米星的二级质谱，对该类化合物的二级质谱裂解规律进行归纳，并以此推测未知新化合物进行结构，再用推测的结构对二级质谱进行解析，如所有的碎片离子均合理解释，表明推测合理。

The methods of ultrasonic decolor ization for corn gluten meal and low velocity electric distilling extraction were studied in the tests.

研究超声波处理法对玉米蛋白粉进行脱色的工艺条件和电动搅拌方式提取玉米醇溶蛋白的最佳提取条件，确定最佳脱色条件是：以无水乙醇为溶剂，萃取温度50℃，料液比1：12，超声波处理25min；最佳提取条件是：料液比1：8，50℃水浴加热，低速搅拌提取3h，乙醇的浓度是75%。

The optimum conditions of extracting cystine were confirmed, as follows: the waste wool pretreatment conditions are pH10, alkali solution temperature 50 ℃ and dry temperature 80 ℃; the waste wool hydrolysis conditions are hydrochloric acid concentration 32%, acid to hairs ratio 1.8:1, hydrolysis temperature 120 ℃, and hydrolys...

研究了预处理、酸解条件、脱色对羊毛胱氨酸提取量的影响，得出了最佳提取胱氨酸的条件，即在pH值为10、碱液温度50℃、烘干温度80℃预处理后的羊毛，在质量分数32%的盐酸、酸毛比1.8：1、水解温度120℃的条件下水解8h。经检测，按所优化工艺提取的胱氨酸符合标准。

The other was a soft filter method. At the aspect of improving measurement range, this paper advanced using different wavelength at the same camera electron shutter.

在扩展温度测量区间方面，提出了一种在利用CCD摄像机不同电子快门分区测量的情况下，用CCD摄像机同一电子快门下改变比色波长来扩大测量温区的方法。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。