步甲

Trituberculatus, China's coastal areas are production, back on both sides have developed a sharp protrusion, fifth right pereiopod bian wide, suitable for swimming.

三疣梭子蟹，中国沿海均产，背甲两侧有发达的尖突，第五对步足扁宽，适于游泳。

A new method for synthesizing rosin allyl alcohol ester was studied. p-Toluenesulfonic acid allyl alcohol ester was first synthesized by O-acylation of allyl alcohol with p-toluene sulfonyl chloride, using NaOH as catalyst. Then rosin allyl alcohol ester was synthesized from sodium resinate and p-toluenesulfonic acid allyl alcohol ester.

探索了一种两步合成松香烯丙醇酯的新方法，即先以烯丙醇和时甲苯磺酰氯为原料，以NaOH为催化剂，通过O-酰化反应合成中间体对甲笨磺酸烯丙醇酯，再与松香钠皂发生亲核取代反应合成目标产物松香烯丙醇酯。

To an asymmetric synthesis of (1), we applied a type of Roush addition in the first step to introduce the C4 stereocenter, and then the chair substance -122 are readily transformed into the title compound -aphanorphine using the same route as to the racemic target molecular.

aphanorphine分子的不对称合成是在第一步通过对甲氧基苯乙醛（119）发生Roush反应引入手性，得到手性高烯丙醇-122，然后利用与合成外消旋目标分子相同的方法，光学纯化合物-122经一系列转化可得到光学纯中间体化合物139；化合物139发生分子内傅—克反应的过程中，由C4位手性立体特异地控制C1位手性的生成，从而解决-aphanorphine分子中的手性问题。

By using the a device being similar to water segregator and by controlling the temperature, cyclization of the intermediate product in chloroform reduced carbonization and gave 2-dodecaneanthraquinane in 68.1% yielding.

以十二烷基苯和苯酐为起始原料，经酰基化、关环和磺化三步反应合成了3-十二烷基蒽醌磺酸；并进一步改进和优化了合成工艺条件：即在催化剂三氯化铝过量50%并有三乙胺存在的条件下，中间体2-（4-十二烷基苯甲酰基）苯甲酸收率为72.45%；关环反应采用氯仿作溶剂，利用类似分水器的装置有效控制反应温度以减少碳化，2-十二烷基蒽醌的收率为68.1%。

Nitro-4-methylsulfonylbenzoic acid was prepared from 4-toluene sulfonyl chloride by the reaction of Alkylation (in the condition of sodium sulfite and baking soda), Nitrification (in the condition of nitric acid and vitriol) and Oxidation reaction (in the condition of nitric acid and catalyzer).

研究了以对甲苯磺酰氯为起始原料，首先通过亚硫酸钠和碳酸氢钠的水溶液进行烷基化、其次在浓硝酸和浓硫酸加热回流的条件下峭化、最后在浓硝酸和催化剂的条件下进行氧化，3步反应合成了玉米田高效除草剂甲基磺草酮的重要中间体2-硝基－4-甲磺酰基苯甲酸。

That when the sound of the horn, pipe, harp, trigon, psaltery, bagpipe, and all sorts of instruments, comes to your ears, you are to go down on your faces in worship before the image of gold which Nebuchadnezzar the king has put up

你们一听见号角、箫笛、琵琶、琴、瑟、风笛、和各样乐器的声音，就当俯伏、向尼布甲尼撒王所立的金像下拜；你们几时听到角、笙、琴、瑟、筝、箫及各种乐器齐奏，就当俯伏朝拜拿步高王立的金像。

Compound 9 is glycosylated in the presence of TMSOTf with rhamose-derived trichloroacetimidates to provide target trisaccharide Saponin 1, oleanolic acid 3-yl-2,4-di-O-a-L-rhamnopyranosyl -p-D-glucopyranosideCoumpond 18 is prepared with oleanic acid and Bromide 11 through phase-thansfer catalysis glycosylation manner.

三糖皂苷Saponin 1是以葡萄糖齐墩果酸皂苷为起始原料，用BBTZ(1-苯甲酰苯并噻唑)选择性保护葡萄糖3′，6′-羟基得到化合物9，然后以化合物9为糖基受体，进行一步糖苷化可以在化合物9的2′，4′-羟基上同时引入两分子鼠李糖，最后脱掉所有的保护基得到目标化合物Saponin1。

In which the buffer's pH was adjusted, pfu Taq DNA polymerase and Klenow fragment were combined, the organic reagent methylamine was added to uncoil the secondary structure.

本研究通过调整反应体系缓冲液pH值、采用高保真pfu DNA聚合酶和Klenow酶组合、加缓解二级结构的有机试剂甲胺、换引物多步扩增而成功实现了重复区片段R02一R11的扩增。

2-Substituted-3,4-dihydro-1(2H)-isoquinolinones were synthesized from methyl 3-hydroxy-ben- zoates via allyl etherification, Claisen rearrangement, oxidation, reductive amination and aminolysis for the first time.

以3-羟基-4-甲氧基苯甲酸甲酯等为原料，通过烯丙基醚化、Claisen重排、氧化、与伯胺反应、还原、分子内酯的胺解六步反应合成了一系列2-取代-3，4-二氢-1-异喹啉酮类化合物。

The hydrogenation and methyl esterification of furoic acid over Pd/γ-Al2O3 catalysts was investigated in fixed bed micro-reactor by one-step method.

采用连续流动固定床微反应器，以糠酸、甲醇、氢气为原料，Pd/γ-Al2O3为催化剂，使糠酸一步加氢甲醋化生成α-四氢糠酸甲酯。

I didn't watch TV last night, because it .

昨晚我没有看电视，因为电视机坏了。

Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

今年以来，在北京的很多小区里，电梯液晶电视被撤了下来。