步法

A kind of modified casting polyurethane by styrene and divinyl benzene with good adhesion with ethylene-propylene-diene monomerhas been prepared by one-step process, which can be cured at the room temperature.

采用苯乙烯、二乙烯基苯对聚氨酯进行了改性研究，利用一步法工艺，制备了与三元乙丙橡胶具有优良粘接性能的双组分室温固化的改性浇注胶。

Titanium ethoxide was directly prepared using titanium as sacrificial anode in absolute ethanol.

采用海绵钛为&牺牲&阳极，在无隔膜电解槽中，电化学一步法制备了纳米TiO2 前驱体钛酸乙酯Ti 4 。

In this chapter, not only Extensed ACD Model, which took higher-order moments、 strict stationarity、 geometric ergodicity and a-mixing property with exponential decay as its sufficient and included most of the present forms of ACD Models was expounded, Box-Cox transformation was carried out by figurate the parameter of ?

尽管关于ACD的实证研究已经十分丰富，却很少有人把注意力放在条件期间模型设定的测试上，本章探讨了关于ACD模型统计性质研究的最新成果，并研究采用两步法来测试条件期间模型的误差项的分布，第一步包括通过QML估计条件期间过程，以获得误差的一致估计；第二步衡量基准密度的参数和非参数估计与残差的风险率函数之间的紧密度。

Nanosized CPF(Conjugated Polymer of Furfuryl alcohol)/ZnO composite catalyst was prepared through in-situ polymerization and heat conversion. The thermal stability, morphologies, size, structure and optical absorption properties of the CPF/ZnO material were characterized by TG-DTA, TEM, XRD, XPS, IR and UV-Vis techniques.

通过原位聚合-热转化两步法，利用ZnO纳米微粒和糠醇制备出了具有大共轭结构的高分子和ZnO的纳米复合催化材料；用TG-DTA、TEM、XRD、XPS、IR和UV-Vis等技术对其热稳定性、形貌、尺寸、结构及吸光特性等进行了表征，以亚甲基蓝溶液的催化降解研究了该材料在自然光条件下的催化性能。

Methods Autologous cord blood serum was used to culture cord mesenchymal stem cells. An enzyme digesting method was used to isolate mesenchymal stem cells from the cord. Morphology, immunotyping and hepatogenic differentiation of these cells were assayed.

分离自体脐血清用于后续细胞培养，利用酶消化法从脐带组织中分离培养间充质干细胞，检测其形态和免疫表型，并采用两步法诱导其向肝细胞诱导分化。

The optimum synthetic conditions of hexadecanoic acid diethanolamide used two-step method are as follows:(1)reaction temperature was 140℃, reaction time was 4.5hours and molar ratio of hexadecanoic acid to diethanolamide was 1:1.15.(2)reaction temperature was 80℃, molar ratio of hexadecanoic acid to diethanolamide was 1:1.55 and mass concentration of the catalyst was 0.8%, reaction time was 3 hours.

二步法合成十六酸二乙醇酰胺最佳合成工艺为：(1)反应温度140℃、反应摩尔比n十六酸∶n二乙醇胺=1∶1.15、反应时间4.5h；(2)反应温度80℃、反应总摩尔比n十六酸∶n二乙醇胺=1∶1.55、催化剂用量0.8%、反应时间3h。

Based on this monomer, several novel polyimides bearing side chain s composed of cyano-biphenyl mesogenic end groups and hexylene spacer were prepared.

合成了一种含氰基联苯氧基侧链的二元胺单体，然后通过两步法热酰亚胺化工艺制备了新型的含氰基联苯基团侧链的聚酰亚胺。

Based on this monomer, several novel polyimides bearing side chains composed of cyano-biphenyl mesogenic end groups and hexylene spacer were prepared.

合成了一种含氰基联苯氧基侧链的二元胺单体，然后通过两步法热醯亚胺化工艺制备了新型的含氟基联苯基团侧链的聚醯亚胺。

In this paper, initiator is dissolved in 1-bromopropane which is solvent. Then the propene and hydrogen bromide that can be dissolved in 1-bromopropane are inlet in l-bromopropane when initiator is decomposing. The reaction occurs in fluid phase and high-purity 1-bromopropane is synthesized by one step method. In this paper, the material HBr is synthesized with NaBr and sulfuric acid at the presence of hydrobromic acid.

本论文以1-溴丙烷为溶剂，将引发剂溶于其中，加热到引发剂开始分解时再通入丙烯和HBr，使二者溶解于1-溴丙烷中，在液相中进行反应，实现丙烯&一步法&合成高纯1-溴丙烷利用NaBr与硫酸在氢溴酸存在下反应制备HBr气体，以作为合成1-溴丙烷的原料。

These conditions included original material source, reagent ratio, base solutions, power of the microwave, reaction time and so on.2, Chitosan obtained from above was modified by Schiff base type macrocycles, which was prepared by the reaction of the reagents of salicylaldehyde, glacial acetic acid, hydrobromic acid, chloroepoxy propane and the others.

反应的最优化条件为：物料比1：25；反应时间20min；NaOH溶液浓度为50%；微波功率为450w。 2、利用原料水杨醛、氢溴酸、冰醋酸等采用四步法合成了含羟基的Schiff碱型大环化合物，然后以取代方法将此Schiff碱型大环化合物负载到壳聚糖上，得到具有特殊结构与性能的壳聚糖衍生物，并得到各中间产物的红外光谱图。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。