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Both net fluxes and concentrations of phosphine had obviously positive correlation with temperature.

磷化氢的净通量和浓度与温度均呈显著正相关。

The optimum conditions for extraction was proved practicable by condition filtration and orthogonal design with supersonic wave method .The results showed that the optimum conditions for extraction to ultrasonic method is : methanol (φ=40,20ml),and 15℃ for 30 min ,this paper has determined nicotine contents that is 23.50mg/g at absorption peak (λ=262nm) by HPLC with an eluent consisting of methanol –potass Phosphate alleciate (pH=3) with the recovery and coefficient of variation are 101.52% and 0.91%.

通过超声波提取方法进行条件筛选和正交化实验,确定了烟草中尼古丁的最佳提取条件,结果表明,超声波最佳条件是:甲醇浓度40%,固液比1:20,提取时间30 分钟,超声温度15℃,用高效液相色谱方法在波长262nm 处测定尼古丁的含量,流动相组成为甲醇:磷酸二氢钾缓冲溶液=10:90,测得烟草中尼古丁的含量为23.50 mg/g,平均回收率为101.52%,相对偏差为0.91%。

Some research and analysis on the reaction of 2,4-difluoronitrobenzene and nucleophilic reagent alcohol sodium (methyl alcohol ,ethyl alcohol, propyl alcohol, n-butyl alcohol, t-butyl alcohol, et hl) and the reaction choice of opposite -F in different solvent and conditions have done in this paper.

论文以2,4-二氟硝基苯为主要原料,研究了其与亲核试剂醇钠(甲醇、乙醇、丙醇、正丁醇、叔丁醇等)在不同溶剂中的反应情况,讨论了在几种代表性的溶剂——醇、四氢呋喃、苯、N,N-二甲基甲酰胺中亲核取代反应的情况,研究了温度、反应时间、亲核试剂、溶剂等条件对亲核取代反应的影响。

In this paper the synthesis of propyl gallate from gallic acid and n-propyl alcohol as reactants and catalyzed by sodium bisulfate was studied; various influencing factors on the reaction were also investigated.

研究了以硫酸氢钠为催化剂,没食子酸和正丙醇为原料合成没食子酸丙酯,并考察影响反应的因素。

The quadratics rotary orthogonal combination design was used to conduct field experiment of integrated balanced of yard manure, urea, calcium superphosphate, potassium chloride and potassium dihydrogen phosphate fertilizer in order to increase the yield of Chinese chestnut.

为提高板栗的产量,对圈肥、尿素、过磷酸钙、氯化钾、磷酸二氢钾等肥料,运用二次旋转正交组合设计,开展综合配套的施肥田间试验。

The best method for isolation and purification of β-dihydroagarofuran sesquiterpene in Celastrus angulatus is alternate normal-phase and reserve-phase high performance liquid chromatography.

结果表明,对苦皮藤中富含二氢沉香呋喃倍半萜类化合物部分进行分离的过程中,采用正相、反相高压制备柱层析交替进行的方法最为有效。

Isolation and purification of dihydroagarofuran sesquiterpene in Celastrus angulatus was preformed with normal-phase and reserve-phase high performance liquid chromatography and detected with TLC and HPLC.

为了优化苦皮藤中二氢沉香呋喃倍半萜类化合物分离纯化的方法,应用正相及反相高压制备柱层析相结合的方法进行分离纯化,以TLC及HPLC确定制备流动相条件并跟踪检测其分离效果。

By using the silicomolybdic yellow colorimetric method, the paper determines not only the existing form of soluble glass in the newly made-up, being used, and discarded cooling liquid,but also the relation of the stability of cooling liquid to the concentration and standing time of monosilicic acid and total silicic acid. The relation of the concentration of polysil...

本文采用硅钼黄比色法测定新配制、使用中和报废冷却液中的水玻璃存在形态和研究冷却液的稳定性与单正硅酸、总硅酸的浓度和放置时间的相关性;用四氢呋哺萃取比色法测定冷却液中的高聚硅酸含量与放置时间的相关性;研究用超声波、磁场等物理方法处理废冷却液的再生可行性及水玻璃的形态变化。

By orthogonal design, the optimal fermentation medium for the cellulase production of the strain was 73% wheat bran, 10% soybean meal, 15% corn grain tegument, 2% ammonium sulfite, 0.15% urea, 0.05% potassium dihydrogen phosphate, 0.1% magnesium sulfate.

采用正交试验法,对该菌株生产纤维素酶的培养基配方进行了优化,确定了生产用最适培养基配方:麸皮73%,豆粕10%,玉米皮15%,硫酸氨2%,尿素0.15%,磷酸二氢钾0.05%,硫酸镁0.1%。

The hydrogen-transfer reaction of HC≡CF→C=H was taken as an example to calculate the microcanonical unimolecular rate constants with consideration of the tunneling correction and the curvature correction and the selection of the rotation states.

以氟代乙炔的氢迁移反应为例,计算了隧道效应、曲率因子和转动选态对微正则系综单分子反应速率常数的影响。

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