槲皮醇

Molecularly imprinted polymer using quercetin as template molecules, methacrylic acid as functional monomers, ethylene glycol dimethacrylate as crosslinking agent were prepared, and the binding sites of MIP were selectively modified with diazomethane.The effects of template molecule concentration, solvent and diazomethane usage on modification were discussed.

以槲皮素为模板分子，甲基丙烯酸为功能单体，乙二醇二甲基丙烯酸酯为交联剂，制备了分子印迹聚合物，并以重氮甲烷为修饰剂，对MIP的结合点进行了选择性修饰，探讨了模板分子浓度、溶剂及重氮甲烷用量等对修饰效果的影响。

A rapid capillary electrophoresismethod has been developed for the determination of eleven bioactive flavonoids in bee propolis:acacetin,apigenin,cinnamic acid,galangin,ferulic acid,hesperidin,luteolin,naringenin,quercetin,resveratrol,and rutin.

使用毛细管电泳法检测蜂胶中11种黄酮类化合物：金合欢素、芹菜配基、兰肉桂酸、黄良姜精、阿魏酸、橙皮甙、毛地黄黄酮、柑桔黄素、槲皮素、白藜芦醇、芦丁。

Phenolics detected in C. incanus L. bee pollen belong to flavonol, flavanols (quercetin, kaempferol, galangin, and isorhamnetin), flavones and phenylpropanoids.

酚类物质检测长梅花湖蜂花粉属于黄酮，黄烷醇（槲皮素，山奈酚，高良姜素和异鼠），黄酮和苯丙。

Results: Seven compounds were isolated from the ethanol extract of the fruits and identified as oleanolic acid, luteolin-7-O-β-D-glucoside, quercitrin,β-sitosterol-3-O-β-D-glucoside, p-hydroxyphenethyl-β-D-glucoside, D-mannitol and hexitol.

结果：从女贞子的乙醇提取物中分离得到7个单体化合物，分别鉴定为齐墩果酸、木犀草素－7-O-β-D-葡萄糖苷、槲皮苷、β-胡萝卜苷、对羟基苯乙醇－β-D-葡萄糖苷、甘露醇及己六醇。

At week 4,animals received quercetin and rutin,as well as allopurinol.

第4周后分别口服给予大鼠槲皮素和芦丁，并以别嘌呤醇为阳性对照药。

RESULTS β-sitosterol(1),2,6-dihydroxyhumlan-9-3(12),7(13),9-triene(2),quercetin-7-methyl ester(3),protocatecheuic acid(4),shikimic acid(5),shikimic acid methyl ester(6) and daucosterol(7) were isolated from Ill...

结果从厚皮香八角果皮中分离得到了7个化合物，分别是β-谷甾醇(1)2、，6-dihydroxyhumulan-9-3(12)，7(13)，9-triene(2)、槲皮素-7-甲基醚(3)、原儿茶酸(4)、莽草酸(5)、莽草酸甲酯(6)和胡萝卜苷(7)。

Sixteen compounds were separated from 80% ethanol extract of Plant A, they were:-lariciresinol,-isolariciresinol,-isolariciresinol 9-O-β-D-glucopyranoside, tanegoside B, apiginin, apigenin 7-O-β-D-glucoside, apigenin 7-O-β-neospheroside, quercetin 3-O-β-D-glucopyranoside, 1, 7-dihydroxy-3, 4-dimethoxyxanthone, 3-O- [α-L-rhamnopyranosyl (1-4 ] -β-D-glucopyranoside-(25S)-5β-spirostan-3β-ol , 3β-O-D-glucopyranoside quinovic acid, mangiferin , 3'-p-hydroxybenzoyl-mangiferin, physcion, benzenyl methanol β-D-glucopyranoside and Vanillic acid.

结果： 1。从植物A的80％乙醇提取物中共分离得到16个化合物，分别为：-落叶松脂醇、-异落叶松脂醇、异落叶松脂醇9-O-β-D-吡喃葡萄糖苷、tanegoside B、芹菜素、芹菜素7-O-β-葡萄糖苷、芹菜素7-O-β-新橙皮糖苷、槲皮素3-O-β-D-吡喃葡萄糖苷、1，7-二羟基-3，4-二甲氧基-口山酮、菝葜皂苷元-3-O-[α-L-吡喃鼠李糖基（1-4）]-β-D-吡喃葡萄糖苷、喹诺酸3β-O-D-葡萄糖苷、知母宁、3′-对羟基苯甲酸-知母宁、大黄素甲醚、苯甲醇-β-D-吡喃葡萄糖苷、香草酸。

Their chemical structures were characterizd on the basis of spectral and chemical evidences to be: Sarracenin (1), 2-methyl-5-hydroxy-7-O-ethyl caffeate chromome (2), Naringenin(3), 2-methyl-5, 7-dihydroxychromome (4), 2-methyl-6-hydroxyl-cinnamic acid methyl ester (5), eriodictyol (6), quercetin (7), Naringenin-7-O-β-D-glucoside( 8 ), eriodictyol-7-O-α-D-glucoside (9), quercetin-3-O-β-D-glucoside(10). In addition, one compound was abtained from the n-butanol frationk, which was finally identified as Morrosiside(11) by spectral and chemical evidences.

以波谱数据及其理化性质鉴定为：Sarracenin(1)，2-甲基-5-羟基-7-O-咖啡酸乙酯色原酮(2)，柚皮素(3)，2-甲基-5，7-二羟基色原酮(4)，2-甲基-6-羟基苯丙烯酸甲酯(5)，圣草酚(6)，槲皮素(7)，柚皮素-7-O-β-D-葡萄糖苷(Naringenin-7-O-β-D-glucoside)(8)，圣草酚-7-O-α-D-葡萄糖苷(eriodictyol-7-O-α-D-glucoside)(9)，槲皮素-3-O-β-D-葡萄糖苷(quercetin--3-O-β-D-glucoside)(10)；另外从正丁醇萃取部位分离得到1个化合物，以波谱数据和文献对照鉴定为：Morroniside(11)。

RESULTS: Sixteen compounds, ursolic acid (1), indole-3-carboxaldehyde (2), indole-3-carboxylic acid (3), p-coumaric acid (4), azelaic acid (5), N-trans-feruloyl tyramine (6), blumenol A (7), 2-hydroxy-3-methylanthraquinone (8), rubiadin l-methyl ether (9), rubiadin (10), quercetin (11), luteolin (12), chrysoeriol 6-C-β-boivinopyranosyl-7-O-β-glucopyranoside (13), alternanthin (14), stigmasta-5, 22-dien-3β-ol (15), and α-spinasterol (16) were obtained from the EtOAc extract of Alternanthera philoxeroides.

结果：得到并鉴定了16个化合物，分别为乌苏酸(1)、吲哚-3-甲醛(2)、吲哚-3-甲酸(3)、对-香豆酸(4)、壬二酸(5)、N-反式阿魏酰基酪胺(6)、布卢姆醇A(7)、2-羟基-3-甲基蒽醌(8)、甲基异茜草素-1-甲醚(9)、甲基异茜草素(10)、槲皮素(11)、木犀草素(12)、柯伊利素-6-C-β-波伊文糖基-7-O-β-吡喃葡萄糖苷(13)、莲子草素(14)、豆甾醇(15)和α-菠甾醇(16)。

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我公司主营产品：钩藤 Gouteng ·水飞蓟素·水飞蓟素·水飞蓟宾·白藜芦醇·大豆甙元·大黄素·大豆异黄酮·酸枣仁提取物·姜黄素，青蒿素松树皮提取物，连翘提取物，野菊花提取物，喜树碱，山楂提取物，熊果酸，玉米须提取物，麦冬提取物，大蒜提取物，人参总皂甙，枸杞提取物，问荆提取物，绿茶提取物，小白菊提取物，苦参提取物，缬草提取物，水杨甙，鬼臼毒素，红曲米提取物，葛根提取物，黄芪提取物，苦瓜提取物，刺蒺藜提取物，银杏叶提取物，枳实提取物，淫羊藿甙，葡萄籽提取物，丹参提取物，山药提取物，越橘提取物，穿心莲提取物，白柳皮提取物，五味子提起物，绞股蓝提取物，当归提取物，红车轴草提取物，红景天提取物，土贝母总皂甙，黄春菊提取物，黑升麻提取物，贯叶连翘提取物，虎杖甙，染料木素，利血平，辛弗林，青藤碱，刺五加甙，薯蓣皂素，葛根素，脱皮激素，卡瓦提取物，叶黄素，番茄红素，南瓜籽提取物，甘草提取物，荨麻提取物，黄芩提取物，蛇床子，细辛，锯叶棕提取物，水皂角提取物，芦丁提取物，紫甘蓝提取物，益母草提取物，延胡索提取物，啤酒花提取物，厚朴提取物，黄杨木提取物，板兰根提取物，生姜提取物，蒲公英提取物，番泻叶提取物，芦荟提取物，党参提取物，金银花提取物，槲皮素，等等

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Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。