槲皮苷

Objective To establish the HPLC method for determination of geniposide, quercetin and gallic acid in Mongolian medicine Sendeng-4 decoction.

目的 建立测定蒙药森登－4汤中栀子苷、槲皮素和没食子酸的高效液相色谱方法。

Their structures were identified by physico-chemical properties and spectral analysis. RESULTS Seven compounds were isolated as kaempferol,quercetin,astragalin,isoquercitrin,kaempferol-3-O-β-D-glucuronic acid methyl ester,4-hydroxybenzonic acid,hentriacontane.

结果分离得到7个已知化合物，分别为山柰酚、槲皮素、山柰酚-3-O-β-D-吡喃葡萄糖苷、槲皮素-3-O-β-D-吡喃葡萄糖苷、山柰酚-3-O-β-D-吡喃葡萄糖醛酸甲酯、对羟基苯甲酸、三十一烷。

This method is highly sensitive and highly selective and was can be applied to the rutin、quercitrin、quercitrin-3-O-giucoside and quercitrin-3-O-galactose determination in yacon leaves with satisfactory result and also can be used to determine these flavonoids in Chinese herbal medicine and Chinese herbal and crude drugs preparations containing flavonoids.

该方法也可用于含芦丁型黄酮中草药及其制剂中芦丁、槲皮素、槲皮素-3-O-葡萄糖苷和槲皮素-3-O-半乳糖苷的检测。

On a ZORBAX Stable Bound (2.150 mm, 1.8 m), the rutin、quercitrin、quercitrin-3-O-giucoside and quercitrin-3-O-galactose could be separated completely with 0.05 mol/L potassium dihydrogen phosphate and methanol as mobile phase (40:60,V/V) at a flow rate of 0.3 ml/min and detected with a photodiode array detector .

在色谱柱为ZORBAX Stable Bound (2.150 mm， 1.8 m)，流动相为0.05 mol/L的磷酸二氢钾缓冲溶液-甲醇(40：60，V/V)，流速为0.3 ml/min，在检测波长为360 nm的色谱条件下，芦丁、槲皮素、槲皮素-3-O-葡萄糖苷和槲皮素-3-O-半乳糖苷分离效果好，方法灵敏度高，重现性好，用于测定雪莲果叶中的上述几种黄酮芦丁型黄酮，效果满意。

RESULTS β-sitosterol(1),2,6-dihydroxyhumlan-9-3(12),7(13),9-triene(2),quercetin-7-methyl ester(3),protocatecheuic acid(4),shikimic acid(5),shikimic acid methyl ester(6) and daucosterol(7) were isolated from Ill...

结果从厚皮香八角果皮中分离得到了7个化合物，分别是β-谷甾醇(1)2、，6-dihydroxyhumulan-9-3(12)，7(13)，9-triene(2)、槲皮素-7-甲基醚(3)、原儿茶酸(4)、莽草酸(5)、莽草酸甲酯(6)和胡萝卜苷(7)。

Sixteen compounds were separated from 80% ethanol extract of Plant A, they were:-lariciresinol,-isolariciresinol,-isolariciresinol 9-O-β-D-glucopyranoside, tanegoside B, apiginin, apigenin 7-O-β-D-glucoside, apigenin 7-O-β-neospheroside, quercetin 3-O-β-D-glucopyranoside, 1, 7-dihydroxy-3, 4-dimethoxyxanthone, 3-O- [α-L-rhamnopyranosyl (1-4 ] -β-D-glucopyranoside-(25S)-5β-spirostan-3β-ol , 3β-O-D-glucopyranoside quinovic acid, mangiferin , 3'-p-hydroxybenzoyl-mangiferin, physcion, benzenyl methanol β-D-glucopyranoside and Vanillic acid.

结果： 1。从植物A的80％乙醇提取物中共分离得到16个化合物，分别为：-落叶松脂醇、-异落叶松脂醇、异落叶松脂醇9-O-β-D-吡喃葡萄糖苷、tanegoside B、芹菜素、芹菜素7-O-β-葡萄糖苷、芹菜素7-O-β-新橙皮糖苷、槲皮素3-O-β-D-吡喃葡萄糖苷、1，7-二羟基-3，4-二甲氧基-口山酮、菝葜皂苷元-3-O-[α-L-吡喃鼠李糖基（1-4）]-β-D-吡喃葡萄糖苷、喹诺酸3β-O-D-葡萄糖苷、知母宁、3′-对羟基苯甲酸-知母宁、大黄素甲醚、苯甲醇-β-D-吡喃葡萄糖苷、香草酸。

Their chemical structures were characterizd on the basis of spectral and chemical evidences to be: Sarracenin (1), 2-methyl-5-hydroxy-7-O-ethyl caffeate chromome (2), Naringenin(3), 2-methyl-5, 7-dihydroxychromome (4), 2-methyl-6-hydroxyl-cinnamic acid methyl ester (5), eriodictyol (6), quercetin (7), Naringenin-7-O-β-D-glucoside( 8 ), eriodictyol-7-O-α-D-glucoside (9), quercetin-3-O-β-D-glucoside(10). In addition, one compound was abtained from the n-butanol frationk, which was finally identified as Morrosiside(11) by spectral and chemical evidences.

以波谱数据及其理化性质鉴定为：Sarracenin(1)，2-甲基-5-羟基-7-O-咖啡酸乙酯色原酮(2)，柚皮素(3)，2-甲基-5，7-二羟基色原酮(4)，2-甲基-6-羟基苯丙烯酸甲酯(5)，圣草酚(6)，槲皮素(7)，柚皮素-7-O-β-D-葡萄糖苷(Naringenin-7-O-β-D-glucoside)(8)，圣草酚-7-O-α-D-葡萄糖苷(eriodictyol-7-O-α-D-glucoside)(9)，槲皮素-3-O-β-D-葡萄糖苷(quercetin--3-O-β-D-glucoside)(10)；另外从正丁醇萃取部位分离得到1个化合物，以波谱数据和文献对照鉴定为：Morroniside(11)。

There were no significant differences in contents of quercetin, isoquercitrin and kaempferol in the fronds, and also no significant differences in contents of rutin, quercetin, kaempferol and total flavonoids in the roots of the three plants studied under the same As treatment.

结果表明：在相同As浓度处理条件下，叶片中槲皮素、异槲皮甙和山奈酚的含量不存在显著差；根部芸香苷、槲皮素、山奈酚和总黄酮含量也不存在显著差异。

We can supply monomers, such as Rutin,Baicalin,Amygdalin,Ursolic acid,limonin,?Glycyrrhizic acid, Chlorogenic acid, Paeoniflorin, Gardenoside, Paeonol, Apigenin, Naringin, Naringenin, Astragalus P.E., Soybean Isoflavones, Epimedium Extract and so on.

产品主要有单体（含量90%~98%：苦杏仁苷、柠檬苦素、熊果酸、芍药苷、栀子苷、丹皮酚、芦丁、槲皮素、黄芩苷、黄芩素、芹菜素、绿原酸、甘草酸、柚皮苷、柚皮素；标准提取物：山楂总黄酮、葛根总黄酮、黄芪多糖、枸杞多糖、大豆异黄酮等。

Seven chemical constituents were identified on the basis of chemical methods and spectral evidences. ResultsFrom this plant, seven active compounds were isolated. They were determined as farrerol, myricetin ,quercetin, taxifolin, umbelliferone, hyperin and juniper camphor.

结果从满山红中分离得到了7种活性化合物，分别为杜鹃素，杨梅素，槲皮素，二氢槲皮素，伞形花内酯，金丝桃苷，杜松脑。

Plunder melds and run with this jewel!

掠夺melds和运行与此宝石！

My dream is to be a crazy growing tree and extend at the edge between the city and the forest.

此刻，也许正是在通往天国的路上，我体验着这白色的晕旋。