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槲皮素

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A rapid capillary electrophoresismethod has been developed for the determination of eleven bioactive flavonoids in bee propolis:acacetin,apigenin,cinnamic acid,galangin,ferulic acid,hesperidin,luteolin,naringenin,quercetin,resveratrol,and rutin.

使用毛细管电泳法检测蜂胶中11种黄酮类化合物:金合欢素、芹菜配基、兰肉桂酸、黄良姜精、阿魏酸、橙皮甙、毛地黄黄酮、柑桔黄素、槲皮素、白藜芦醇、芦丁。

A high-performance liquid chromatographic method for the simultaneous separation and determination of aryltetralin lignans and flavonoids in Podophyllum emodi Wall.var. chinesis Sprague was developed. The separation was performed on a Kromasil-C 18 column by gradient elution with phosphate buffer-methanol (0-13min, 50∶50, 33min, 30∶70) as mobile phase at a flow-rate of 0.8 ml/min, with detection 270nm.

首次建立了桃儿七中苦鬼臼葡萄糖甙、4-去甲基鬼臼脂素、表鬼臼脂素、苦鬼臼脂素、苦鬼臼酯酮、鬼臼脂素、鬼臼酯酮、去氧鬼臼脂素、去氢鬼臼脂素等9种木脂素以及山柰酚、槲皮素等2种黄酮类组分同时分离测定的高效液相方法。

RESULTS: Sixteen compounds, ursolic acid (1), indole-3-carboxaldehyde (2), indole-3-carboxylic acid (3), p-coumaric acid (4), azelaic acid (5), N-trans-feruloyl tyramine (6), blumenol A (7), 2-hydroxy-3-methylanthraquinone (8), rubiadin l-methyl ether (9), rubiadin (10), quercetin (11), luteolin (12), chrysoeriol 6-C-β-boivinopyranosyl-7-O-β-glucopyranoside (13), alternanthin (14), stigmasta-5, 22-dien-3β-ol (15), and α-spinasterol (16) were obtained from the EtOAc extract of Alternanthera philoxeroides.

结果:得到并鉴定了16个化合物,分别为乌苏酸(1)、吲哚-3-甲醛(2)、吲哚-3-甲酸(3)、对-香豆酸(4)、壬二酸(5)、N-反式阿魏酰基酪胺(6)、布卢姆醇A(7)、2-羟基-3-甲基蒽醌(8)、甲基异茜草素-1-甲醚(9)、甲基异茜草素(10)、槲皮素(11)、木犀草素(12)、柯伊利素-6-C-β-波伊文糖基-7-O-β-吡喃葡萄糖苷(13)、莲子草素(14)、豆甾醇(15)和α-菠甾醇(16)。

The method was successfully applied to separate and determine isoquercitrin, chlorogenic acid and quercetin in Inula britamica L.

将此方法应用于分离测定欧亚旋覆花中的异槲皮甙、绿原酸和槲皮素,取得良好结果。

By the quantitative analysis of flavonoids from the extract under acid hydrolysis condition, it is demonstrated that the level of isoquercitrin degrades along with the content of hydrochloric acid elevating and the level of kaempferol is reverse. Those reveal that there exist flavonoid conjugates whose aglycone is kaempferol in the leaves.

对青钱柳酸水解液中成分的测定表明,随着酸浓度的提高,异槲皮苷的含量下降,槲皮素的含量上升,山奈酚的含量也随酸浓度上升而增高,表明青钱柳中尚有以山奈酚为苷元的黄酮苷存在。

The results from statistical analysis of variance indicated that Bt toxin in Bt transgenic cotton had no negative effect on synthesis of flavonoids (mainly rutin, isoquercitrin and quercetin ).

显著性分析发现,外源Bt杀虫蛋白表达对棉花原有的芸香苷、槲皮素和异槲皮苷等抗虫黄酮类化合物不存在不利的影响。

Three flavonoids compounds: kaempferol *!, quercetin *, and isoquercitrin *# were isolated from the leaves of Cyclocarya paliurus Batal.

采用溶剂萃取及多种色谱技术分离纯化,根据理化性质和光谱分析方法鉴定其结构,确定从青钱柳中分离得到山柰酚、槲皮素和异槲皮苷 3个黄酮单体化合物,并用反相高效液相色谱法对其含量进行了测定,测得各自在甲醇和水提取物中的含量:山柰酚 0 。

An ionic liquid (1-ethyl-3-methylimidazolium tetrafluoroborate, 1E-3MI-TFB) modified micellar electrokinetic capillary chromatographic method was developed to separate and determine isoquercitrin, chlorogenic acid and quercetin.

建立了一种离子液体(1-乙基-3-甲基咪唑四氟硼酸盐,1E-3MI-TFB)修饰毛细管胶束电动色谱法分离测定异槲皮甙、绿原酸和槲皮素的方法。

Results showed a close relationship existed among the three flavonoid compounds with kaempferol content greater than quercetin and isoquercetin.

结果表明:青钱柳叶中3种黄酮类化合物质量分数紧密相关,其中山奈酚质量分数高于槲皮素和异槲皮苷。

objective in order to exploit the natural resources of chinese herbs,the inhibitive effects of the compositions of28chinese herbs on the growth of8common bacteria in oral cavity were determined.methods sen-sitive test of these bacteria were carried out by mtt method.at the same time,chessboard dilution method was used for combined sensitive test.results the compositions of28chinese herbs can inhibit the growth of5bacteria in dif-ferent levels,but the effects on other3bacteria are not obvious.quercetin and usnic acid have better effects on5bacteria than other26herbs compositions,with mic0.03125~0.125mg/ml and0.0156~0.0625mg/ml.conclu-sion quercetin and usnic acid can inhibit the5bacteria growth more effectively than other26herbs compositions.

目的 测试28种中药有效成分抑制8种口腔常见致病菌的作用,为抗菌中药有效成分用于口腔感染性疾病的防治做一些探讨。方法选择28种有抗菌作用的中药的有效成分,采用噻唑蓝法对8种口腔常见致病菌作药物敏感实验,同时采用液体棋盘稀释法进行联合药敏实验。结果 28种中药有效成分对3种牙周细菌抑制作用不明显,对另5种口腔常见细菌有一定的抑制作用,其中松萝酸和槲皮素有较强的抑菌作用,mic值分别在0.0156~0.0625mg/ml和0.3125~0.125mg/ml之间。结论所选28种中药成份中,松萝酸和槲皮素具有较强的抑菌作用。

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