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Aqua, Aloe Barbadensis Leaf Juice(1), Helianthus Annuus Seed Oil(2), Glycerin, Glyceryl Stearate, Octyl Palmitate, Potassium Stearate, Panthenol (Vit. B5), Tocopherol Acetate, Tocopherol, Beta-Glucan, Arginine, Allantoin, Geranium Maculatum Oil, Citrus Grandis Peel Oil, Citrus Aurantium Dulcis Peel Oil, Cocos Nucifera Oil(3), Linum Usitatissimum Seed Oil(4), Barosma Betulina Leaf Oil, Cetyl Alcohol, Xanthan Gum, Algin, Benzyl Alcohol, Ethylhexylglycerin, Phenoxyethanol

成分:纯净水、库拉索芦荟汁、葵花籽油、天然植物甘油、硬脂酸甘油酯(乳化剂,含有钠与钾之脂肪酸,作为柔软、润滑效果)、棕榈酸盐、硬脂酸钾、维生素 B5、维生素 E 、燕麦酵素葡聚糖、精氨酸、尿囊素、天竺葵精油、葡萄柚精油、橙花精油、椰子油、亚麻籽油、南非香叶精华、棕榈醇、黄原胶、褐藻胶、苯甲醇、乙基己基甘油、苯氧乙醇。

Water,c12-20 acid peg-8 ester,octyldodecanol,propylene glycol,coco-caprylate/caprate,cetearyl isononanoate,prunus amygdalus dulcisoil,biosaccharide gum-1,phenoxyethanol,ethylhexyl methoxycinnamate,potassium cetyl phosphate,simmondsia chinensisseed oil,carbomer,glyceryl polymethacrylate,malva sylvestrisextract,glyceryl stearate,cetearyl alcohol,cetyl palmitate,cocoglycerides,c12-13 alkyl lactate,methylparaben,sorbic acid,disodium edta,sodium hydroxide,tocopheryl acetate,benzophenone-3,iris germanica root extract,retinyl palmitate,butylparaben,peg-8,propylparaben,ethylparaben,sodium hyaluronate,chlorhexidine digluconate,tocopherol,ascorbyl palmitate,citric acid,ascorbic acid

水, c12-20 acid peg-8 ester,辛基十二烷醇,丙二醇,coco-caprylate/caprate,鲸蜡硬脂醇异壬酸酯,甜杏仁油,多醣物质,苯氧乙醇,4-甲氧基肉桂酸-2-乙基己基酯,十六烷基磷酸钾,西蒙得木籽油,卡波姆,甘油聚甲基丙烯酸酯,锦葵萃取,甘油硬脂酸,棕榈醇,十六烷基棕榈酸酯,椰油脂酸甘油酯类,c12-13烷醇乳酸酯,对羟基苯甲酸甲酯,山梨酸,乙二胺四乙酸二钠,氢氧化钠,维生素E醋酸酯,二苯甲酮-3,鸢尾花萃取,维他命A酯,对羟基苯甲酸丁酯,聚乙二醇-8,羟苯丙酯,羟苯乙酯,透明质酸钠,洗必泰葡萄糖酸盐,维生素E ,维生素C棕榈酸酯,柠檬酸,抗坏血酸

Water,dimethicone,propylene glycol,glycerin,cyclomethicone,ppg-15 stearyl ether,sorbitan oleate,stearic acid,cetyl alcohol,glyceryl stearate,ethylhexyl methoxycinnamate,peg-100 stearate,panthenol,phenoxyethanol,phospholipids,triethanolamine,methylparaben,oenothera biennis oil,imidazolidinyl urea,carbomer,c12-13 alkyl lactate,glycyrrhetinic acid,citrus aurantium dulcisoil,propylparaben,tocopheryl acetate,benzophenone-3,triclosan,disodium edta,ethylparaben,pentadecalactone,iris germanica root extract,retinyl palmitate,bisabolol,butylparaben,sodium hyaluronate,aesculus hippocastanumseed extract,ruscus aculeatus root extract,chlorhexidine digluconate,biosaccharide gum-1,citrus aurantium amaraoil,tocopherol,lecithin,ascorbyl palmitate,glyceryl oleate,BHT,citric acid,limonene,linalool

水, 地美司康,丙二醇,甘油,环甲硅脂, PPG-15 硬脂基醚,油酸己六酯,硬脂酸,十六醇,甘油硬脂酸, 4-甲氧基肉桂酸-2-乙基己基酯,聚乙二醇硬脂酸酯,维生素B5,苯氧乙醇,磷脂质,三乙醇胺,羟苯甲酯,月见草油,尿素醛,卡波姆, c12-13烷醇乳酸酯,甘草亭酸,甜橙油,羟苯丙酯,醋酸盐维他命E,二苯酮-3,玉洁新,乙酸乙二胺二钠,羟苯乙酯,环十五内酯,鸢尾花根萃取,维他命A酯,没药醇,羟苯丁酯,透明质酸钠,欧洲七叶树籽萃取,假叶树根萃取,洗必泰葡萄糖酸盐,多醣物质,苦橙油,维生素E,卵燐脂,抗坏血酸棕榈酸酯,甘油油酸酯,二丁基羟基甲苯,柠檬酸,柠檬精油,芳樟醇水:几乎所有护肤品成分第一位都是水。地美司康:即silicon,矽灵,一般添加于霜剂中,使用后皮肤手感光滑。该成分不可吸收。

Water,c12-20 acid peg-8 ester,octyldodecanol,cetearyl isononanoate,butylene glycol,biosaccaride gum-1,peg-40 hydrogenated caster oil,ethylhexyl menthoxycinnamate,phenoxyethanol,potassium cetyl phosphate,macadamia ternifolia seed oil,dimethicone,carbomer,propylene glycol,glyceryl stearate,cocoglycerides,butyrospermum parkii,c12-13 alkyl lactate,methylparaben,benzophenone-3,pentadecalactone,sorbic acid,citrus aurantium dulcis oil,sodium hydroxyde,tocopheryl acetate,disodium edta,iris germanica root extract,retinyl palmitate,equisetum arvense extract,butylparaben,peg-8,propylparaben,ethylparaben,sodium hyaluronate,chlorhexidine digluconate,citrus aurantium amaraoil,tocopherol,ascorbyl palmitate,citric acid,ascorbic acid,limonene,linalool

水,c12-20 acid peg-8 ester,辛基十二烷醇,鲸蜡硬脂醇异壬酸酯,丁烯二醇,多醣物质,PEG-40氢化蓖麻油,4-甲氧基肉桂酸-2-乙基己基酯,苯氧乙醇,十六烷基磷酸钾,澳洲胡桃子油,地美司康,卡波姆,丙烯乙二醇,甘油硬脂酸,椰油脂酸甘油酯类,牛油果,c12-13烷醇乳酸酯,对羟基苯甲酸甲酯,二苯甲酮-3 ,环十五内酯,山梨酸,甜橙油,氢氧化钠,维生素E醋酸酯,乙二胺四乙酸二钠,鸢尾花萃取,维他命A酯,问荆萃取,对羟基苯甲酸丁酯,聚乙二醇- 8,羟苯丙酯,羟苯乙酯,透明质酸钠,洗必泰葡萄糖酸盐,苦橙油,维生素E ,维生素C棕榈酸酯,柠檬酸,抗坏血酸,柠檬精油,沉香醇水:几乎所有护肤品成分第一位都是水。辛基十二烷醇:界面活性剂、乳化剂、稠化剂,有一定刺激性

Water,caprylic/capric triglyceride,mineral oil,butylene glycol,stearic acid,acetylated lanolin,glycerin,ethylhexyl methoxycinnamate,dimethicone,polyisoprene,triethanolamine,cyclopentasiloxane,butyl methoxydibenzoylmethane,titanium dioxide,persea gratissima oil unsaponifiables,sodium DNA,borago officinalis seed oil,oenothera biennis oil,simmondsia chinensisseed oil,hydrolyzed RNA,tocopheryl acetate,urea,hydrolyzed extensin,retinyl palmitate,sodium hyaluronate,helianthus annuusseed oil,tocopherol,ascorbyl palmitate,ascorbic acid,lanolin alcohol,c12-20 acid peg-8 ester,cyclotetrasiloxane,glyceryl stearate,dimethiconol,ceteareth-20,carbomer,magnesium aluminum silicate,propylene glycol,peg-8,silica,BHT,citric acid,phenoxyethanol,methylparaben,butylparaben,ethylparaben,isobutylparaben,propylparaben,chlorhexidine digluconate

水,辛酸/癸酸三酸甘油酯,矿物油,丁二醇,硬脂酸,乙醯化羊毛脂,甘油,4-甲氧基肉桂酸-2-乙基己基酯,地美司康,聚异戊烯,三乙醇胺,环戊硅氧烷,丁基甲氧基二苯甲醯基甲烷,二氧化钛,酪梨油,DNA 钠盐,琉璃苣種子植物油,月见草油,荷荷巴籽油,水解RNA,醋酸盐维他命E,尿素,水解伸展蛋白,维他命A酯,透明质酸钠,葵花籽油,维生素E,抗坏血酸棕榈酸酯,维生素C衍生物,羊毛脂醇,C12-20 酸 PEG-8酯,环四硅氧烷,甘油硬脂酸,聚二甲基硅氧烷醇,鲸蜡硬脂醇醚-20,卡波姆,硅酸镁铝,丙二醇,聚乙二醇-8,二氧化硅,二丁基羟基甲苯,柠檬酸,苯氧乙醇,羟苯甲酯,羟苯丁酯,羟苯乙酯,羟苯甲酸异丁酯,羟苯丙酯,洗必泰葡萄糖酸盐

Purified water, octyl palmitate, castor oil phosphate, triethoxycaprylylsilane, glyceryl stearate, peg-100 stearate, isopropyl palmitate, cetearyl alcohol, vegetable glycerin, phenoxyethanol, benzyl alcohol, potassium sorbate, tocopherol, stearic acid, certified organic aloe barbadensis extract, certified organic lavandula angustifolia extract, avena sativa kernal flour, certified organic helianthus annuus seed oil, panthenol (vitamin B5), certified organic simmondsia chinensis seed oil, polysorbate 60, allantoin, certified organic chamomilla recutita flower extract, potassium cetyl phosphate, and xanthan gum.

纯水、辛基棕榈酸酯、蓖麻油磷酸盐、triethoxycaprylylsilane、硬脂酸锌,异丙酯、peg-100棕榈酸、cetearyl酒精、蔬菜甘油、萃取物、苯甲醇、山梨酸钾、生育酚、硬脂酸、有机认证索芦荟精华、有机认证此提取物、淡紫色沙枣阿韦纳处理(燕麦粉、有机认证的核心annuus的向日葵籽油、维他命原B5、泛醇经认证的有机simmondsia羊(霍霍巴籽油、polysorbate 60、尿囊素、有机认证chamomilla recutita洋甘菊三叶草萃取物、钾cetyl磷酸盐、黄原胶。

Trisodium salt of N,N,N'-ethylenediamine triacetic acid was prepared by hydrolyzing 2-oxo-1, 4-piperazine diacetic acid(3-KP) in the strong base solution. Then it was combined with lauroyl chloride, hexadecanoyl chloride and benzoyl chloride respectively. N-lauroyl-ED3A and N-hexadecanoyl-ED3A were prepared in succsess. The molecular structure of N-lauroyl-ED3A was characterized by ~1HNMR and ~(13)CNMR. The molecular structure of N-hexadecanoyl-ED3A was characterized by 1HNMR.

将3-KP 在强碱性条件下水解,生成ED3ANa3 的水溶液,然后分别与月桂酰氯、棕榈酰氯和苯甲酰氯反应,成功制得N—月桂酰基ED3A 和N—棕榈酰基ED3A,并用~1HNMR 和~(13)CNMR 对N—月桂酰基ED3A 的分子结构进行了表征,用1HNMR 对N—棕榈酰基ED3A 的分子结构进行了表征。

Secondly, organical composite thermal storage materials which takethe PNIPAAm gels as the carriers and the palmitic acid and the lauric acidmixture for phase change materials were Synthesized by radicalpolymerization ,and organical/inorganical composite materials which takeP(NIPAAm-co-AAm) gels as the carriers and the palmitic acid、thelauric acid and Na_2HPO_4·12H_2O mixture were also Synthesized byradical polymerization.

其次,本文采用自由基聚合法,合成了以PNIPAAm凝胶为载体,棕榈酸和月桂酸的混合物为相变材料有机复合相变蓄热材料;及P(NIPAAm-co-AAm)凝胶为载体,棕榈酸、月桂酸和Na_2HPO_4·12H_2O为相变材料的有机/无机复合相变蓄热材料,采用红外光谱、示差扫描量热法、热重分析、扫描电镜等手段对两种复合材料的结构及热性能进行了表征与分析,研究了有机酸和无机盐的百分含量对复合材料的相变温度和相变焓的影响。

These compounds were identified as follows:chrysophanol (FP-1),physcion(FP-2),eriosematin(FP-3),scoparone(FP-4),lupeol(FP-5),betulinic acid(FP-6),3\',4\'-Dihydroxy-trans-cinamic acid octacosyl ester(FP-7),β-sitosterol (FP-8),flemiphilippinone A(FP-9),monopalmitin(FP-10),emodin(FP-11),islandicin (FP-12),salicylic acid(FP-13),p-methoxyphenylpropionic acid(FP-14),trideca-1, 3-diene(FP-15),lupinifolin(FP-16),flemichin D(FP-17),flemiphilippinin A(FP-18), auriculasin(FP-19),erythrinin B(FP-20),6-C-prenylluteolin(FP-21), 8-(1,1-dimethylallyl) genistein(FP-22),flemiphilippinin E(FP-23),flemiphilippinin F (FP-24),5,7,3\',4\'-tetrahydroxy-6,8-diprenylisoflavone(FP-25),flemiphilippinin D (FP-26),dorsmaninsⅠ(FP-27),osajin(FP-28),6,8-diprenyleriodictyol(FP-29), lupinalbin A(FP-30),genistein(FP-31),3\'-O-methylorobol(FP-32),orobol(FP-33), 5,7,2\',3\',4\'-pentahrdroxyflavone(FP-34),the mixture of biochanin A and prunetin (FP-35 and 36),genistin(FP-37),sophororicoside(FP-38),3\'-O-methylorobol-7-glucoside(FP-39),the mixture of sissotrin and prunetin 4\'-O-β-D-glucoside(FP-40 and 41),adenosine(FP-42) and luteoloside(FP-43,mixture).

这些化合物分别为大黄酚(FP-1)、大黄素甲醚(FP-2)、eriosematin(FP-3)、滨蒿内酯(FP-4)、羽扇豆醇(FP-5)、白桦酸(FP-6)、咖啡酸二十八烷酯(FP-7)、β-谷甾醇(FP-8)、蔓性千斤拔酮A(FP-9)、单棕榈酸甘油酯(FP-10)、大黄素(FP-11)、islandicin(FP-12)、水杨酸(FP-13)、对甲氧基苯丙酸(FP-14)、十三烷-1,4-二烯烃(FP-15)、lupinifolin(FP-16)、千斤拔素D(FP-17)、蔓性千斤拔素A(FP-18)、auriculasin(FP-19)、erythrinin B(FP-20)、6-C-异戊烯基木犀草素(FP-21)、8-(1,1-二甲烯丙基)-染料木黄酮(FP-22)、蔓性千斤拔素E(FP-23)、蔓性千斤拔素F(FP-24)、5,7,3′,4′-四羟基-6,8-双异戊烯基异黄酮(FP-25)、蔓性千斤拔素D(FP-26)、dorsmaninsⅠ(FP-27)、osajin(FP-28)、6,8-双异戊烯基圣草素(FP-29)、lupinalbin A(FP-30)、染料木黄酮(FP-31)、3\'-O-甲基香豌豆苷元(FP-32)、奥洛醇(FP-33)、5,7,2′,3′,4′-五羟基黄酮(FP-34)、鹰嘴豆素甲和樱黄素的混合物(FP-35和FP-36)、染料木苷(FP-37)、槐属苷(FP-38)、7-葡萄糖基-3\'-O-甲基香豌豆苷(FP-39)、印度黄檀苷和樱黄素4′-O-β-D-葡萄糖苷的混合物(FP-40和FP-41)、腺嘌呤核苷(FP-42)和木犀草苷(FP-43,混合物)。

In this paper, firstly using natural fatty acids including lauric acid, myristic acid, palmitic acid etc. and disproportionated rosin as starting materials, the acyl reaction of starting materials with SOCl_2 respectively, and then using Schotten-Baumann condensation: on the reaction conditions of alkalescence, condensation of acylchloride with amino acid (sarcosine, glycine, alanine etc.), and then acidification, saltation. A series of anionic surfactants of N-acyl amino: sodium N-fatty acyl sarcosinate (SFS-12, SFS-14, SFS-16); sodiun N-fatty acyl glycinate(SFG-12, SFG-14, SFG-16); sodium N-fatty acyl alaninate(SFA-12, SFA-14, SFA-16)and sodium N-disproportionated rosinoyl aminatewere prepared. During the preparation of N-acylamino acid, the reaction conditions of acylchloride with amino acid condensation were identified by optimizing the synthetic conditions of N-lauroyl sarcosine: mol ratio of amino acid to acylchloride 2:1, reaction taken place in a solvent composed by acetone/water 2:1, acylchloride and 20% NaOH were slowly added to the reaction mixture at the same time while maintaining the pH at 9~10, after completion of adding maintaining reacting for 2.5h at 25℃.

首先以月桂酸、肉豆蔻酸、棕榈酸等天然脂肪酸和歧化松香为原料,与氯化亚砜反应制得酰氯,然后采用Schotten-Baumann 缩合法路线,即在碱性条件下,酰氯和氨基酸(肌氨酸、甘氨酸、丙氨酸等)缩合,经过酸化、成盐,合成一系列氨基酸型阴离子表面活性剂:脂肪酰肌氨酸钠,即月桂酰肌氨酸钠(SFS-12)、肉豆蔻酰肌氨酸钠(SFS-14)、棕榈酰肌氨酸钠(SFS-16);脂肪酰甘氨酸钠,即月桂酰甘氨酸钠(SFG-12)、肉豆蔻酰甘氨酸钠(SFG-14)、棕榈酰甘氨酸钠(SFG-16);脂肪酰丙氨酸钠,即月桂酰丙氨酸钠(SFA-12)、肉豆蔻酰丙氨酸钠(SFA-14)、棕榈酰丙氨酸钠(SFA-16);N-歧化松香酰基氨基酸钠(sodium N-disproportionated rosinoyl aminate),即N-歧化松香酰基肌氨酸钠(sodium N-disproportionated rosinoyl sarcosinate ,简称SDRS)、N-歧化松香酰基甘氨酸钠(sodium N-disproportionated rosinoyl glycinate,简称SDRG)、N-歧化松香酰基丙氨酸钠(sodium N-disproportionated rosinoyl alaninate,简称SDRA)。

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