根据实验的

Two representative compounds have been determined by X-ray crystallography. The best ratio of reactants, the adequate reaction temperature and solvent have been found by contrast experiments.4. The better photoreaction conditions and irridation times have been confirmed through the different photoreaction results. It is the first time that fifty quinazoline derivatives with biological activity and four photooxidation products with urea functional groups have been obtained by photochemistry method. Two representative compounds, quinazoline derivatives and photooxidation products, have been determined by X-ray crystallography, respectively.

通过实验对比我们找到了较佳的反应物的投料比、反应温度和反应所用的溶剂。4、根据不同条件下的光反应结果，确定了硫脲衍生物的相对较好的光反应条件和光照时间，首次利用光化学手段成功得到50个具有生物活性的喹唑啉衍生物和4个具有脲基官能团的光氧化的产物，测定了两个具有代表性的喹唑啉和光氧化的产物的晶体结构。

By synthetically analysizing the physical and chemical properties of all components and particle size, the content of F2641 in the JOB-iC is determined by gravimetric analysis after F2641 is seperated from HMX,TATB and PNP through ? alkali reflux. Determination conditions is set as follows the sample is boilingly refluxed for six hour in a constant temperature bath after adding lOOm! 8.0 ?? 0.1% NaOH. The solvent DMF saturated by TATB is used for extracting HMX,F21 and PNP from the sample and TATB is seperated by crucible filter G4. The mass precent of TATB is determined by extraction fractionation. The mass percent of PNP is measured by multiwavlength linear regression ultraviolet spectrophotometry. The testing conditions are set as follows:multiwavlength constitution: X=267nxn, 275nm, 283nm, 29mm, 299nm,the application scope of the Lambert-Beer law: the concentration of PNP is O.005?0.O25mgIml, the concentration of HMX is 0.060.3Omg/ml,absorption coefficents of PNP and HMX are solved by the slope of linear regression curve of absorbency- concentration of standard solution of PNP and HMIX for measuring wavelengthes,on the basis of the Lanibert-Beer law and absorbancy additivity principle, the slope of linear regression curve of A/E(1) and E1 of PNP and HMX solution is regarded as the concentration of PNP in the solution.

根据传爆药中各组分的物理、化学性质及主体炸药的粒度大小，进行综合分析，确定了采用碱回流重量法测定JOB-1C 中F_(2641)的含量，测定条件：加入100ml浓度为8.0±0.1％的氢氧化钠，在恒温水浴中煮沸回流6h；采用溶剂萃取法测定JOB-1C中TATB的含量，选择TATB饱和的二甲基甲酰胺为萃取溶剂，用G4坩埚式过虑器进行萃取分离；采用多波长线性回归紫外分光光度法测定JOB-1C中PNP的含量，通过实验确定了多波长组合：λ=267nm，275nm，283nm，291nm，299nm；朗波—比耳定律的适用范围为PNP浓度：0.005～0.025mg/ml，HMX浓度：0.06～0.30mg/ml；在测定波长下，对PNP、HMX标准溶液的吸光度—浓度进行线性回归，由回归曲线的斜率得出PNP、HMX的吸收系数；根据朗波—比耳定律和吸光度加和性原理，在测定波长下，对PNP、HMX 两组分混合溶液A_i/E_HMX(i与E_PNP(i/E_HMX(i进行线性回归，回归曲线的斜率即为混合溶液中PNP的浓度。

Pass to count to Wisterch parameter , and the steel wire is different from the molding tool get in touch with the length, and settle the path the research taking the length work the stabber angle to get under differently pull to stir the term, mold core adoption of best severally why size, combine the best work stabber of research the Cape, and settle the path to take the length nextly steel wire is in the molding tool of have fever to measure, air inside dispel-heat calories, winding dispel-heat on the coil-canister , and its molding tool dispel-heat calories of, and cause the steel wire the temperature difference pass in and outing the molding tool to influence steel wire machine function, under the experiment inside pull to stir the term according to the same race different work stabber Cape half of adoption the Cape(7 degree,10 degree,12 degrees, the best mold Cape, experience mold Cape) settle the path to take the length(2-3 mm,3-4 mm,4-5 mms, theories length, experience length) to proceed to experiment, and get the conclusion, work stabber the Cape then is more big the steel wire get in touch with the length with

通过对Wisterch参数，钢丝与模具接触长度、定径带长度、工作锥角度的研究得到了在不同拉拨条件下模芯采用的最佳几何尺寸，并研究最佳工作锥角、定径带长度下钢丝在模具中的发热量、空气中散热量、卷筒上的散热量及其模具散热量的不同，导致钢丝进出模具的温度差别对钢丝机械性能的影响，在实验中根据同种拉拨条件下采用不同工作锥角半角、定径带长度进行试验，得出结论，工作锥角越大则钢丝与模具接触长度越短，钢丝变形越剧烈，在模具中发热量就越高，导致钢丝出模温度高，使钢丝强度、硬度升高，弯曲、扭转次数降低，并且降低模具使用寿命。在其它条件相同的情况下，定径带越长则钢丝与定径带简壁磨擦增大，使钢丝发热量加大，从而使钢丝强度、硬度略升高，弯曲扭转次数略降低但定径带的增大减小了钢丝变形产生的弹性后效使钢丝出模直径比较稳定。

In chapter three, various theories and experience on the dispersion of nano-powders proposed by former researchers were generalized and reviewed. Technical standards and experimental process for determining technological parameters were suggested for the dispersion of nano-scaled metal oxides in aqueous medium according to their surface wettability, surface charge, the dependence of surface charge on pH and the compatibility of surfactants with pH and pH adjusting agents. Based on these suggested standards and experimental method, highly stable and dispersive aqueous suspensoid of nm-ZnO, nm-TiO〓, nm-Co〓O〓 and nm-MnO powders were prepared successfully and surface modification on these nano-powders was also achieved.

本文第三章通过大量的文献调研，归纳总结了前人在纳米粒子分散技术方面的理论和经验，并在此基础上根据纳米氧化物粉体的表面润湿性、表面电性及其与分散介质pH值的关系、表面活性剂及其与pH调节剂的配伍关系设计了纳米氧化物水分散体系的工艺规范以及确定工艺参数的通用实验步骤，成功地制备了纳米氧化锌、纳米二氧化钛、纳米氧化钴和纳米氧化锰的高稳定分散悬浮液并实现了干粉体的表面改性，为纳米材料在氧化锌压敏电阻中的应用创造了第二个前提条件。

In this paper, the sorting of wear, the mechanics of wear particle formed and the characteristics of wear particles are introduced, and morphology characteristics parameter of wear particle are determined, which is particle brim digital feature. Based on image characters, after pre-process, section and extracting of contour parameter of wear particle using image process technique, four shape character parameters are extracted by fourier series expansion. After analyzing fundamental principle and shortcomings of neural network, current BP algorithm is improved in output optimization, network linearization implication optimization and adding momentum, and then astringe speed of BP algorithm.

本文介绍了磨损的分类以及磨粒的生成机理、磨粒的形态特征，应用摩擦学系统分析的观点，确定磨粒边缘数字特征为磨粒的识别特征参数；根据磨粒图像的特征，利用计算机图像处理技术对磨粒图像进行预处理、分割、轮廓参数的提取，采用傅立叶级数展开式提取磨粒四个形状特征参数：圆形度、散射度、凹度、细长度；针对 BP(Back-Propagation)神经网络收敛速度慢的特点，对现行的 BP 算法进行改进，并通过实验验证改进后的网络收敛速度快；研究设计了磨粒图像采集系统；利用 BP 算法建立磨损磨粒自动识别算法模型 AWPRM(Auto Wear Particle Recognition Model)。

The thermal decomposition yielded unsaturated compound and dithiobenzoic acid, leading to some loss of living character of the polymerization, such as retarded reaction rate and broadened molecular weight distribution.

我们根据合成双硫酯的经验和实验中的观察发现，双硫酯的热稳定性对RAFT聚合影响很大，在较高的温度下双硫酯会发生一定程度的热分解，生成的双硫酸会对聚合有一定的阻聚和延迟作用。

The phase tracking principle of source-contained homodyne detection is researched, the frame diagram for phase detection and experimental results are given.

介绍了一种新型的光纤电压传感器结构和工作原理，分析了系统中椭圆芯双模光纤的传输模式和模间相干光斑的变化，采用熔接的方式进行相干光接收来获得正交相位漂移信号，根据模间群折射率差与光程差的关系设计调整光纤的长度，依据石英晶体和空气的绝缘强度进行传感光纤匝数设计，讨论了含源零差探测法的相位跟踪原理，给出了相位检测框架图及实验结果，分析表明该设计方案能达到相位跟踪的目的。

Needle taking place is commonly used the rescue that changes cure and danger to weigh a patient at patient of children, tumour, in infusion, because secure not firm outside can bringing about syringe needle slippery haemorrhage to be in charge of, cause local strut, aching, serious person can send infiltration of the certain pharmaceuticals that change cure to cause subcutaneous tissue hypodermically necrotic or the liquid cannot be defeated in time note and illness of incur loss through delay, new puncture increases the patient's anguish not only, also increased economic burden to also can be affected at the same time to the patient nurse working quality, the course relapses clinical experiment, my division adopts vein to accept the annular and fixed method of buy needle, obtained better result, introduce as follows now. 1 method is taken fixed stick (needle taking place is deployed) together, the disinfection that wide 10cm controls wraps cloth, two paragraphs of end are seamed on after sticking glue to buckle vein to leave buy needle puncture to succeed, convention is secured with adhesive plaster, next the ground degree of tightness will take stalk of handle of buy pinhead, needle, needle to be in firmly aptly fixed and fixed stick , next annular in blood-vessel twine stick on stick buckle. 2 experience apply this method to secure vein to left buy needle method to reduce the patient's anguish, reduced cost, provided mobile space for the patient, also avoid heparin cap prolapse, still facilitate observation puncture is nodded, do not affect hematic use, gauze pad can alleviate heparin cap is oppressive and unwell, reduce infusion pollution.

概要： 留置针常用于小儿、肿瘤患者化疗及危重患者的抢救，在输液中，由于固定不牢可导致针头滑出血管外，引起局部肿胀，疼痛，严重者可致某些化疗药物渗入皮下造成皮下组织坏死或液体不能及时输注而延误病情，重新穿刺不仅增加病人的痛苦，也给病人增加了经济负担同时也会影响护理工作质量，经过反复临床实验，我科采取静脉留置针的环形固定方法，取得了较好的效果，现介绍如下。1方法取固定贴一块，宽10cm左右的消毒包布，两段端缝上粘胶扣静脉留置针穿刺成功后，常规用胶布固定，然后将根据松紧适宜将留置针头、针柄、针梗处牢牢固定固定贴，然后在血管中环形缠绕粘上粘扣。2心得应用此方法固定静脉留置针方法减少了患者的痛苦，降低了费用，为患者提供了活动的空间，也避免肝素帽脱垂，还便于观察穿刺点，不影响血运，纱布衬垫可缓解肝素帽压迫不适，减少输液污染。

At the one-cell stage, each embryo was injected with gradient doses of 2-8ng MO. The control morpholino, was purchased from Gene-Tools.To test the knockdown effectiveness of the morpholino, the tbx2-EGFP (enhanced green fluorescent protein) construct was generated. And coinjection of morpholino with mRNA tests its specificity of the morpholino. Overexpression of tbx2 via mRNA microinjection helps us understand gaining function of tbx2. Results The tbx2-EGFP construct tests the knockdown effectiveness of the morpholino. Zebrafish embryos lacking tbx2 function have defects in cardiac contractility, rhythm and morphology in a dose-dependent manner. The embryos with c-MO are normal in development. Coinjection of morpholino with mRNA rescue the phenotype of tbx2 knocking down. The phenotypes include pericardial edema, hypogenetic ventricle, dilation of atria, arrhythmia, bradycardia, asystole, abnormal atrioventricular canal, aberrant valve and blood regurgitation.

结果荧光蛋白融合标记实验验证了tbx2-MO可以很好得阻抑斑马鱼胚胎tbx2的表达，tbx2-MO组胚胎在心脏收缩性、节律和形态学发生上出现了异常，心脏畸形随着注射剂量的增加而出现比较一致的表型，而c-MO组胚胎没有出现明显的畸形；tbx2-mRNA和tbx2-MO的共注射减少了tbx2-MO胚胎心脏畸形的发生率及减轻了心脏畸形的程度，验证了所设计合成的tbx2-MO对tbx2基因的抑制作用具有特异性；tbx2-MO组胚胎心脏缺陷包括心室发育不良、心房扩张、房室管和瓣膜异常以及心率缓慢、心律不齐、心脏停搏、血液返流等，并根据心脏发育异常的程度分为轻、中、重度畸形组tbx2-mRNA基因过表达胚胎没有见到心腔的形成。

Methods: According to the mechanism of cough reflex, the c-fibres's role in the respiratory system, and the principle of isosterism. Here, a peripheral antitussive LD was regarded as a lead compound. Amino functional groups, as substituents at the 1-hydroxy group of the racemate of LD, were introduced into the structure of the molecule. These novel compounds were confirmed by 1H-NMR, MS spectrum. Their antitussive activities were studied on mice in sequential method. The EDT50, the stimulating time that caused cough by NH3 on half of mice, were measured. Then could caculated the ratio R between the EDT50 of the treated groups and control group.

根据咳嗽反射的机制及C-纤维在呼吸系统的作用，以外周镇咳药左羟丙哌嗪为先导化合物，依据电子等排原理，在其结构中引入氨基以取代羟丙哌嗪分子中1位的羟基，设计一系列未见报道的化合物（01-15）；并采用了一条适宜的路线进行合成，通过1H-NMR、MS确证结构；采用&序贯法&实验进行新化合物的镇咳活性研究，动物模型采用氨水引咳小鼠，获得引致半数小鼠咳嗽的氨水刺激时间（EDT50）及给药组EDT50与对照组的比值R。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。