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样品分布

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The natural distributing populations of the indigenous timber species--Cordia africana that grew in and around the area of Mizan Teferi in Ethiopia were investigated. Bulk seed samples were selected from ten phenotypically superior trees in different natural populations. They were evaluated through the performance of their half-sibs and especially examined for variability in seed morphometrics, seed germination, and seedling growth at nursery stage.

通过对埃塞俄比亚Mizan Teferi及周边地区生长的乡土用材树种--非洲破布木自然种群分布情况调查,筛选了10株生长表现型较好的优良母树,采集了大量的供试种子样品,并对其种子外部特征和在苗圃中的发芽率和种苗生长表现进行了观察和分析对比。

In an attempt to provide a better understanding of the diversity, evolution and spread of geminiviruses in China, 32 samples showing typical geminivirus symptoms were collected from papaya, tomato, tobacco, Euphorbia pulcherrima, Sonchus oleraceus Linn and Ageratum conyzoides in Guangxi province.

为了明确双生病毒的发生、分布与传播,我们从广西番木瓜、番茄、烟草、一品红、苦苣菜及胜红蓟上采集了32个具有双生病毒典型症状的样品并对病毒进行了分子检测与鉴定。

Benzene hexachloride, dichlorodiphenyltrichoroethane and organophosphorus pesticides in 103 soil samples collected from Wutongqiao district of Sichuan were detected by gas chromatography. Spatial distribution characteristics of residual pesticide in soils of transitional zone from mountain to plain was evaluated by employing the methods of GIS and geostatistical techniques.

以四川省五通桥区为例,利用气相色谱法检测丘陵平原过渡区103个样点的土壤样品中六六六、滴滴涕和10种有机磷农药残留量,利用地统计方法和GIS技术,评价研究区域内的土壤农药残留空间分布特征。

The model of heat and mass transfer of a biological sample in cryopreservation was solved by perturbation and integral methods.

用摄动法和积分法求解了生物样品的传热传质模型,在模型简化时比较了积分解和精确解,探讨了低温保存中细胞的损伤机理,对冷却介质温度随时间线性变化时相变界面的移动作了实验研究,用自己设计和制作的实验台架和测试装置测量了相变界面的移动和温场的分布。

The recovery of low, medium and high concentration, relative standard deviations of precision and stability experiments are consistent with the requirements of biological sample analysis.

结果表明,低、中、高三个浓度的回收率,精密度和稳定性试验结果均符合生物样品的测定要求,为君-使对药体内动力学和组织分布研究奠定了方法学基础。

Collecting water and soil samples from Tainan brine pan of Lianyungang, taking salt as the sole growth limiting factor, we have investigated the numerical distribution of halophilic bacteria with the media containing 4%, 12% and 25% mass-concentration of NaCl.

在连云港台南盐田中取卤水和底泥样品,以盐为限制性生长因子,采用含4%、12%和25%的NaCl平板对嗜盐菌的分布状况进行调查,表明盐田中嗜盐菌数量在夏季最多,每毫升卤水中最高为1。

In addition nC〓, nC〓, two isomers of C〓 sterene and three isomers of C〓 isoprenoid hydrocarbons were also identified from aliphatic fraction of pyrolyzed product at 200℃. After pyrolyzed at 300℃, the main aliphatic hydrocarbons were normal alkanes ranged from C〓 to C〓, with C〓 as the main peak and C〓 as the second main peak. Meanwhile, pristane, phytane and C〓 sterane were also detected. In the pyrolysates at 400℃ and 500℃, the content of saturated hydrocarbons decreased, the range of normal alkanes distribution became narrow and the main peak was nC〓. Low concentration of C〓-C〓 steranes was detected and the content of C〓-C〓 increased more.

在200℃热模拟产物饱和烃馏分中除检测出两种长链烯烃外,还检测到正十九碳单烯烃、正三十五碳双烯烃、两个碳二十八甾烯的同分异构体和三个C〓类异戊二烯烷烃化合物同分异构体。300℃模拟产物饱和烃主要为正烷烃,正烷烃的碳数分布范围为C〓-C〓,以C〓为主峰、C〓为次主峰;另外,样品中还检出姥鲛烷、植烷和C〓甾烷等化合物。400和500℃热模拟产物中的饱和烃含量下降,正烷烃系列碳数分布范围变窄,主峰碳后移至C〓,检测到低浓度的C〓-C〓甾烷系列化合物,另外,C〓-C〓藿烷系列化合物含量进一步增加。

Secondly, we provide a two-level model to depict the one-, two-and three-photon fluorescent process and with it to calculate the one-, two-and three-photon fluorescence intensity dependence of the incident excitation intensity and time. We study the fluorescence intensity when excitation light's time distribution are square pulse、Gaussian pulse and sech pulse. We find that the influence of excitation light's time distribution on the two- and three- photon fluorescence peak intensity is larger than the one-photon fluorescence peak intensity. Two-level model can account for the behavior of saturation fluorescence.

然后用二能级模型解释了单、双、三光子激发原理,在理论上推导出了单、双、三光子吸收诱导荧光强度与脉冲强度以及脉冲作用时间的关系,并进一步研究了入射光时间分布分别为矩形、高斯型、双曲正割型时激发溶解在氯仿溶液中的C22H22N4O样品所产生的荧光峰值光强,结果表明激发光的时间分布对双、三光子荧光峰值强度的影响比对单光子的影响要大。

This thesis has systematically studies the microstructure of the sinter bearing fluorine of different compositions and in different sintering condition.(1) The main units of the Low Fluorine Sinter are magnetite、hematite、 SFCA、larnite、glass and pore. The cuspidine doesn't form for the low content fluorine, and the fluorine is in glass; Sinter basicity dominates the forming of the larnite and SFCA, when basicity is between 1. 72 and 1. 96, there are more larnites in the binder phase, and when the basicity is biger than 1. 96, there are more SFCA in the binder phase; the hematite appears like magnetite and usually is around pore.

为此,本文对不同组成、不同烧结条件的烧结矿样品进行了系统的显微分析和研究,其主要内容包括:(1)构成低氟烧结矿的主要组元有磁铁矿、赤铁矿、铁酸钙、硅酸二钙、玻璃体和气孔,由于含氟量的降低,枪晶石等含氟矿物并未形成,氟分布在后期凝固的玻璃体中,其中硅酸二钙和铁酸钙受碱度影响较大,硅酸二钙在碱度为1.72~1.96范围内形成较多,铁酸钙在碱度大于1.96含量增多,赤铁矿呈磁铁矿假象,多分布在气孔周围,各组元的生成顺序为:磁铁矿—硅酸二钙—铁酸钙—玻璃体。

The following main results are obtained: The TiO_2 photocatalyst with small crystallite size, high surface area, narrow and uniform pore size distribution, and microporous frameworks could be prepared out by applying MW radiation in the preparation process. The microwave-induced fluorescence technique verified for the first time that microwave enhanced the formation rate of hydroxyl radical, leading to the increase in the photocatalytic efficiency. Compared with the conventional catalyst, TiO_2 prepared by MW dielectric heating owns a higher UV absorption ability, and its optical absorption edge and photovoltaic response are shifted toward the short wavelength region, resulting in increase of photooxidation efficiency. The photocatalytic conversion and the mineralization ratio of acetaldehyde are increased respectively by 30% and 40% over the TiO2 prepared by MW radiation when compared to the TiO2 prepared by the conventional heating. For the MW-assisted photocatalytic reaction over the MW-prepared TiO2, production of hydroxyl radicals is enhanced by 22.5%, and the photocatalytic conversion is accordingly increased by 20%. Similarlly, applying MW also increased the photocatalytic conversion and the mineralization ratio of acetaldehyde over TiO2/Al2O3 sample.

论文得到如下主要结果和结论:(1)微波介电加热TiO_2 溶胶可得到晶粒度小、光催化活性高、比表面积大和孔径分布窄而均一,且微孔发达的TiO_2光催化剂;在溶胶干燥处理过程中微波可使催化剂表面缺陷增加,进而导致光催化反应过程有更多的活性羟基自由基产生;(2)微波制备能显著增强TiO_2 样品的紫外光吸收率,并使其光吸收和光伏响应阈值发生蓝移,从而提高TiO_2的氧化还原能力;(3)与常规加热法所制TiO_2比较,微波法制备的TiO_2对乙醛的光催化降解转化率提高30%,CO_2生成率提高40%以上;(4)与未加微波辐射时相比,发现在光催化反应过程中施加微波,TiO_2 的羟基自由基生成速率提高了22.5%,相应CH_3CHO 光催化降解转化率提高了20%;对Al_2O_3/TiO_2催化剂,CH_3CHO 光催化降解转化率甚至提高了33%,同时CO_2 的生成率也都大幅度提高;(5)微波辐射可改变光催化降解乙醛的产物分布,推断施加微波时乙醛光催化降解按照羟基自由基引发的链式反应机理进行,微波&非热效应&起主要作用。

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