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The feasibility of constructing a partial least squares model with a parsimonious calibration set for NIR spectral analysis was discussed. Waveband selection was also investigated for improving the predictive ability of the model.

通过标准样品和复杂基质样品共同构建的偏最小二乘模型,考察了波段筛选和建模参数对预测结果的影响。

Calibration models were established by the spectral measurement of a set of hydrolyzed standard sugar solutions by treating with concentrated sulfuric acid and a chemometrical software.

其原理是基于样品中的糖经浓硫酸处理后生成有紫外吸收的糠醛和羟甲基糠醛,进行紫外波长吸收测定;通过化学计量学软件,根据一组已知糖浓度标准样品的多波长光谱和所对应组成浓度之间的数学关系,建立校正模型。

Technique details were optimized about steps from sample treatment to gel staining, and 2 - DE gels are lampros and aequalis distributed , the method of sample treatment suitable for mass spectrography analysis.

优化从样品处理到凝胶染色几个过程的技术细节,蛋白表达谱清晰且分布均匀,样品处理方法适合后期的质谱测试分析。

In order to establish relative analysis methods and find out transfer rules and vertical distribution characteristics of heavy metals in sediments of Poyang lake,column form sampler designed by us was used in the experiments,the sediments samples from Wucheng section of the Ganjiang River in Poyang lake area were collected using adjacent water vertical spile method.

为建立鄱阳湖水域沉积物中重金属的相关研究方法,了解重金属污染物的迁移规律,并探讨底泥中重金属的垂直分布特征,采用底质柱状采样器通过临水垂直插管法采集鄱阳湖流域赣江吴城段的底质样品,利用微波消解—AS-990型原子吸收分析体系对柱状样中不同深度的样品进行重金属Cu含量的测定。

In Co42Ag58 and Co80Ag20 samples,spin wave resonancehas beenobserved.

在Co42Ag58和Co80Ag20样品中,观察到自旋波共振,但是两样品的SWR谱明显不同。

6Combining with several SEM pictures of different samples, cement-soilmicrostructure characteristics are described. Test results show that the cement-soil,whose stock-still time is longer, is a little worse of its strength than the one withoutstock-still time, because of its discontinuous microstructure and some micro-cracksbetween inter-particles.

6结合不同样品的SEM图片,描述了不同样品的微结构特征,试验结果表明,静置时间较长的水泥土由于微结构的不太致密、颗粒间存在较多的微裂缝,故其强度性能稍差。

The shelf life of cold storage sample and indoor storage sample can reach 6 months or longer.

冷藏样品与室内贮藏样品的货架期均可达6个月或者更长。

A stumper with required structures is pressed into the surface of polymeric foil and heated to a temperature above its glass transition temperature under suitable pressure until the temperature droped below the glass transition temperature of the polymer, followed by removal of the stumper and left the structures of the stamper in the polymeric foil.

将聚合物加热到其玻璃转化温度以上,利用预先制备好的模板在适当的压力下压向聚合物样品,保持压力直到聚合物温度降到玻璃转化温度以下,将模板移去后,模板上图形便转移到样品表面。

By scanning electron microscopy observation,distribution of pores was found to be ordered and pores were precisely vertical to their substratum.

采用阳极氧化方法制备了多孔氧化铝有序孔洞阵列,通过场发射扫描电镜和X射线衍射观测了样品的表面、截面的形貌和晶态结构,分析了样品的透射光谱性质。

Samples of animal manure were collected in Jiangsu Province in 2005 to 2006, the residues of sulfagidine, sulfanilamide, sulfadiazine, sulfamerazine(SM1), sulfadimidin(SM2), sulfamonomethoxine, sulfachloropyridazine, sulfamethoxazole were determined by HPLC with fluorimetric detector after pre-column derivatization.

2005—2006年采集了江苏省各市不同种类的集约化畜禽养殖场共178个畜禽粪便样品,用柱前衍生法高效液相色谱荧光检测器,检测了样品中8种磺胺类药物(磺胺胍、磺胺、磺胺嘧啶、磺胺甲嘧啶、磺胺二甲嘧啶、磺胺间甲氧嘧啶、磺胺氯哒嗪、磺胺甲恶唑)残留情况。

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