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HPLC was coupled with both mass spectroscopy and ultraviolet absorption spectroscopy for simultaneous separation and characterization of the products from glow plasma reaction of chloroform.(3) Phosphorus pentachloride has been used to perchlorinate acenaphthene under moderate pressure and temperature in sealed reaction vessels.

在此基础上，以反相C〓柱为固定相，甲醇/乙醇/环己烷为流动相，采用梯度洗脱的方法，对氯仿辉光放电合成产物进行高效液相色谱-紫外光谱-质谱联用分离分析，成功的分离得到包括富勒烯C〓和全氯代碳簇在内的数十种产物，并得到了相应的质谱和光谱数据。

Objective To analysis the results of treating the bothcolumn fractures of acetabulum via ilioinguinal approach.

目的 分析经髂腹股沟入路治疗髋臼双柱骨折的疗效。

MethodsBy high perfomance liquid chromatography method, mobile phase was acetamide plus water solution of sodium heptansulfonic acid and sodium phosphate.

方法采用高效液相色谱法，用乙腈与庚烷磺酸钠磷酸钠的水溶液为流动相，流速 1 。0ml/min ，柱温 4 0℃，检测波长为 2 80nm ，进样量为 2 0 μl。

Methods Protein in blood and urine was precipitated directly by acetonitrile with acetanilide was used as the internal standard using Agilent Zorbax SB-Aq column (250 mm×4.6 mm, 5 μm). The mixed solvents of water (triethylamine 0.12%, acetic acid 0.12%) and acetonitrile were used as the mobile phase to separate cephalosporins using gradient elution method at 1 mL/min and 254 nm.

以乙酰苯胺为内标，血液和尿液用乙腈直接沉淀蛋白，采用Agilent Zorbax SB-Aq(250 mm×4.6 mm， 5 μm)色谱柱，流动相选用水（含0.12%三乙胺和0.12%乙酸）和乙腈的混合溶剂梯度洗脱，流速1 mL/min，检测波长254 nm。

It has the function of correctly controlling the pressure, flame resistance and acid mist filtering when valve open and close.

阀体采用阻燃ABS材料，阀芯为柱状结构(ZL 00 2 41118.0)，双过滤酸雾滤片，具有准确控制开、闭阀压力、阻燃、过滤酸雾功能。

After acidify with hydrochloric acid, the plasma was extracted with ethyl ether and then analyzed by Hypersil ODS2 (250×4.6 mm,5 μm) column with the mobile phase of methanol-water-triethylamine-acetic acid(2500∶1500∶15∶7), and at the detection wavelength of 355 nm.

血样经盐酸酸化后以乙醚提取，进行 HPL C分析，色谱柱为 Hypersil ODS2 (2 5 0× 4.6 m m，5 μm)，流动相为甲醇-水-三乙胺-冰醋酸(2 5 0 0∶15 0 0∶ 15∶ 7)检测波长为 35 5 nm，尼美舒利为内标。

The oily substances and the acidic components were characterized using elementary analysis, IR spectral analyses and acidimetry.

采用石油醚和三氯甲烷分级萃取孤岛油田含聚污水中的油分，得到两个不同极性的组分F1和F2；用碱抽提法从酸值较高的F2组分中分离酸性物质并将其甲酯化，通过柱层析法将甲酯化物分成Ⅰ、Ⅱ和Ⅲ三个甲酯组分。

Between P14 and P21,CIAPIN1 immunoreaction in the brain,heart and liverbecame much lower. However,between P21 and P28,CIAPIN1 immunoreactionin the heart,brain,liver and skeletal muscle became much lower,while with thekidney development,CIAPIN1 immunoreaction in the kidney became higher. Invarious tissues from adult mouse,CIAPIN1 immunoreaction could be seen incardiac muscle cell,brain,hepatocyte,epithelium of renal tubule,skeletal muscle,lung tissue,gastric mucosa and gland,acinus lienalis.2. Distribution of CIAPIN1 in normal fetal and adult human tissuesTo reveal the possible physiological role of CIAPIN1,we examined theexpression and distribution of CIAPIN1 in fetal and adult human tissues usingimmunohistochemistry. We found that CIAPIN1 was ubiquitously distributed infetal and adult tissues,and was localized in both the cytoplasm and the nucleus.

然而，在3个月大的成年鼠中，CIAPIN1阳性反应物在心、脑、肝和肾小管中的表达强度要低于P28小鼠；但CIAPIN1阳性反应物在成年鼠骨骼肌中较P28小鼠高。2、CIAPIN1蛋白在人5个月胚胎及成人多器官组织内的表达在人5月胚胎多器官组织中，CIAPIN1阳性反应物见于心脏、胆囊单层柱状上皮和粘膜、结肠粘膜、小肠粘膜和绒毛、肝脏、直肠腺体、胃粘膜、肾上腺束状带、甲状腺滤泡、脾索、胸腺小叶间隔、皮肤真皮层和汗腺、睾丸白膜和间质、脑组织内神经元和神经胶质、肺小支气管和肺泡、骨骼肌、肾脏皮髓质和肾小管、子宫内膜、胰腺腺泡和胰岛、卵巢、输卵管粘膜等绝大多数组织细胞。

The mineral components are tremolite dominantly,with minor actinolite,diopside,epidote,clinozoisite,magnetite,pyrite and other impurities.

其结构主要为纤维状、柱纤状、粒纤状变晶结构、局部为放射状或帚状变晶结构等，以纤维状变晶结构最为常见。

The acute angle of the rear window and the elegant design of the C-pillar give the car a dynamic look, and make for a lower and more sporty appearance.

在后车窗锐角和典雅的设计的C柱都让汽车动态，并作出了更低，更运动的外观。

The absorption and distribution of chromium were studied in ryeusing nutrient culture technique and pot experiment.

采用不同浓度K2CrO4(0，0.4，0.8和1.2 mmol/L)的Hoagland营养液处理黑麦幼苗，测定铬在黑麦体内的亚细胞分布、铬化学形态及不同部位的积累。

By analyzing theory foundation of mathematical morphology in the digital image processing, researching morphology arithmetic of the binary Image, discussing two basic forms for the least structure element: dilation and erosion.

通过分析数学形态学在图像中的理论基础，研究二值图像的形态分析算法，探讨最小结构元素的两种基本形态：膨胀和腐蚀；分析了数学形态学复杂算法的基本原理，把数学形态学的部分并行处理理念引入到家实际应用中。