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Keywords: diketoreductase,isomeride,separation and purification,statins chiral side-chain expression, photoaffinity labeling probe

通过DEAE-Sepharose离子交换柱及Sephadex分子筛柱纯化后，酶的纯度达到电泳纯，并通过正相硅胶柱和反相C-18柱分离纯化其反应产物。

Test results reveal that with the same area of the column section, the punching shear strength of the connections with nonrectangular columns is greater than that of the connections with square columns, and shear reinforcement can significantly enhance the strength and ductility of the connections with nonrectangular columns.

试验结果表明，与方柱－板柱连接试件相比，在柱截面积相同的情况下，异形柱－板柱连接试件具有较高的抗冲切承载力。抗冲切钢筋可以有效地提高板的冲切承载力和延性。

With cross-shaped column as the representative of nonrectangnlar columns, one experimental program is conducted to study behavior of slab-column connection with nonrectangular column provided with shear reinforcement, the shear reinforcement include traditional stirrup and stud shear reinforcement .

2以十字形柱为代表，对配置抗冲切钢筋的异形柱－板柱连接的受冲切性能进行了试验研究，将其受冲切特性与文献中相应方柱－板柱连接试验进行了比较分析，研究了抗冲切钢筋对其受冲切特性的影响。

X-ray diffraction showed that the hydroxy-chromium oligocations can be used as a stable pillaring agent after aging at 70 ℃ for four days, and a pillared composite with high crystallinity can be obtain...

与原料2H-MoS2相比，柱撑材料的层间距增大，晶粒变小，比表面积增加并且热稳定性提高。对催化苯饱和加氢反应表明，柱撑材料Cr-MoS2的催化活性明显优于未柱撑的2H-MoS2和RaneyNi催化剂，且结晶度较好的柱撑材料更具有较高的催化活性和较好的可重复性。

First, organic pillared montmorillonite were prepared in which three kinds of organic quaternary ammonium salts were used as pillaring agent. Physiochemical properties of organic pillared montmorillonites were characterized by XRD, FT-IR, TG-DTA. Furthermore their characters that have been testified are excellence.

首先用三种有机季胺盐作为柱撑剂制各出有机柱撑蒙脱石，并通过XRD、FT-ZR、TG-DTA等测试手段对其进行了表征，并且对制备的有机柱撑蒙脱石进行了性能测试，证明其性能优良，说明利用干法制备有机柱撑蒙脱石是切实可行的。

Pillared montmorillonite, as a representative of Sandwich like pillared interlayered clays ,caught many scientist"s attention not only because of its special structure of two-dimensional sheets but also its excellent activity of catalysis and adsorption. It is well documented that the method to prepare PILM, ion-exchanging, needed a long periods and was affected by many factors, and that the product had low thermal stability especially hydro-thermal stability which was the primary obstruction of its using in large-scale production. At the same time, PILM was well documented prepared with Na-montmorillonite, while there were a few documents about PILM prepared with Ca-montmorillonite. The large cost of remodel of Ca-montmorillonite to Na-montmorillonite was another obstacle of the application of PILM, while Ca-montmorillonite was widely distributed in nature, as a result, to prepare PILM with Ca-montmorillonite has practical significance. What"s more, PILM was mainly studied as a catalyst in oil refining process till now, but rarely documented in other catalysis reactions, especially in coal liquification filed which also needed high activity catalyst.

以柱撑蒙脱石为代表的具有&三明治&结构的柱撑粘土矿物因其特殊的二维孔道结构和优良的催化和吸附性能近年来成为国内外广泛关注和研究的热点，但是目前国内外大量报道的PILM制备大多采用离子交换法，生产周期很长，影响因素很多，并且产物热稳定性不够高，特别是水热稳定性较差，这是其不能在实际中大规模生产和应用的主要障碍，因此制备一种高稳定性的PILM意义非常；文献中大量报道的都是钠基蒙脱石合成的柱撑粘土矿物，传统的离子交换法必须将钙基蒙脱石钠化改型，其成本相当高，而自然界中大量存在的却是钙基蒙脱石，直接用钙基蒙脱石合成柱撑粘土矿物有很现实的意义，但目前这方面的报道却很少见；另外，迄今为止，PILM作为催化剂的研究领域主要在石油的炼制中应用，而在煤炭的液化中却鲜有报道，如果能在煤炭转化领域应用这一成果，其影响也将是相当大的。

Pillared montmorillonite, as a representative of Sandwich like pillared interlayered clays ,caught many scientist's attention not only because of its special structure of two-dimensional sheets but also its excellent activity of catalysis and adsorption. It is well documented that the method to prepare PILM, ion-exchanging, needed a long periods and was affected by many factors, and that the product had low thermal stability especially hydro-thermal stability which was the primary obstruction of its using in large-scale production. At the same time, PILM was well documented prepared with Na-montmorillonite, while there were a few documents about PILM prepared with Ca-montmorillonite. The large cost of remodel of Ca-montmorillonite to Na-montmorillonite was another obstacle of the application of PILM, while Ca-montmorillonite was widely distributed in nature, as a result, to prepare PILM with Ca-montmorillonite has practical significance. What's more, PILM was mainly studied as a catalyst in oil refinin g process till now, but rarely documented in other catalysis reactions, especially in coal liquification filed which also needed high activity catalyst.

以柱撑蒙脱石为代表的具有&三明治&结构的柱撑粘土矿物因其特殊的二维孔道结构和优良的催化和吸附性能近年来成为国内外广泛关注和研究的热点，但是目前国内外大量报道的PILM制备大多采用离子交换法，生产周期很长，影响因素很多，并且产物热稳定性不够高，特别是水热稳定性较差，这是其不能在实际中大规模生产和应用的主要障碍，因此制备一种高稳定性的PILM意义非常；文献中大量报道的都是钠基蒙脱石合成的柱撑粘土矿物，传统的离子交换法必须将钙基蒙脱石钠化改型，其成本相当高，而自然界中大量存在的却是钙基蒙脱石，直接用钙基蒙脱石合成柱撑粘土矿物有很现实的意义，但目前这方面的报道却很少见；另外，迄今为止，PILM作为催化剂的研究领域主要在石油的炼制中应用，而在煤炭的液化中却鲜有报道，如果能在煤炭转化领域应用这一成果，其影响也将是相当大的。

This paper studies the correlation between the maximum height s of the Plinian volcanic eruption columns and mass flux of the volcanic eruptions according to measurement data acquired from active volcanoes around the world.

Plinian式火山喷发柱最大高度是研究火山喷发对环境、气候影响时空范围的重要物理学参数，在分析了影响Plinian式火山喷发柱最大高度诸因素的基础上认为，火山喷发的质量通量是反映火山喷发柱最大高度最有效并且在实际中可以进行测量的参数之一，以此为基础，利用目前实测的火山喷发柱最大高度的数值与火山喷发质量通量的结果，建立两者的相关方程为：H＝0。

Previous studies indicate two possibilities of the formation of the greigite: 1 the seepage of seawater during the postglacial transgression provides sulfate and makes the reducing diagenetic conditions; 2 it may be precipitated as the authengenic mineral in marine or lacustrine sediments during the low sea-level stand of the Late Pleistocene.

本研究在前期工作基础上，针对已发现的硫复铁矿富集区选择典型柱状样6根(深约1.5-2.5m，长柱样；B436、B437、B439、B459、B483、B484)，同时于扬子浅滩前缘新获取柱状样4根(深约0.3-0.5m，短柱样；ST9、ST13、ST15、ST23)，进行了U系测年，粒度分析、磁性测量、X—射线衍射分析、微体古生物鉴定分析、粘土矿物和化学元素含量测试，试图揭示东海外陆架浅部地层结构、揭露硫复铁矿在地层中的分布规律及成因机制，从而探讨该区晚更新世以来海平面波动模式及其控制下的地层发育。

Joint behavior of beam and column is the key of entire structure.This paper uses finite elemnt analyzing software ANSYS to analyze the bearing mechanics of joint under monotonic load and periodic load,and gets load-displacement curves,viscosity curves and frame curves.The paper mainly analyzes how axis-push ratio,gradation of concrete,plate layout and steel type to affect tensibility performance and viscosity feature of joint.The results indicate that concrete-filled squar tube column has good tensibility performance and dissipative ability.

梁柱节点的性能是影响结构整体性能的关键，而目前对方钢管混凝土柱—钢梁节点抗震性能的研究工作尚不完善，本文通过有限元软件ANSYS来分析方钢管混凝土柱—钢梁节点，研究节点区在单调荷载和低周反复荷载作用下的受力机理，得节点区的荷载位移曲线、滞回曲线及骨架线；着重分析方钢管混凝土柱的轴压比、混凝土等级，隔板形式和钢材型号在低周反复荷载作用下对节点延性和耗能等抗震性能指标的影响。

The absorption and distribution of chromium were studied in ryeusing nutrient culture technique and pot experiment.

采用不同浓度K2CrO4(0，0.4，0.8和1.2 mmol/L)的Hoagland营养液处理黑麦幼苗，测定铬在黑麦体内的亚细胞分布、铬化学形态及不同部位的积累。

By analyzing theory foundation of mathematical morphology in the digital image processing, researching morphology arithmetic of the binary Image, discussing two basic forms for the least structure element: dilation and erosion.

通过分析数学形态学在图像中的理论基础，研究二值图像的形态分析算法，探讨最小结构元素的两种基本形态：膨胀和腐蚀；分析了数学形态学复杂算法的基本原理，把数学形态学的部分并行处理理念引入到家实际应用中。