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The grafting effect and mechanism was charac- terized by FTIR,The heat stability of unvulcanized and dynamical mechanical proper- ty of vulc- lcanizates of SBR and SBR-g- were tested by TG and DMA respectively. medium-resistance properties of SBR and SBR-g- vulcan- izates were also investigated.The results showed that addition of St accelerated GMA grafting onto SBR and control the decomposition of SBR. When the conditions were GMA/St/DCP was 8/4/0.3 and grafting temperature was 160℃.

结果表明,St对提高接枝率、抑制SBR的降解起到了积极的作用;SBR中聚丁二烯的α-H和双键共同参与了GMA/St熔融接枝反应;当SBR/GMA/St/DCP=100/8/4/0.3、接枝温度为160℃时,SBR的接枝率较高(23.78%),SBR–g–硫化胶的拉伸强度和撕裂强度比SBR硫化胶的分别提高了119%和27.4%;SBR–(GMA--co-St)未硫化胶的Tg比SBR未硫化胶的高,而耐热分解性能优于SBR未硫化胶;SBR–g–硫化胶在低温条件下的刚性增大、弹性降低、具有较低的内耗,在常温下的阻尼性能较高,但弹性性能保持较好;SBR–g–硫化胶的耐热稳定性以及耐非极性有机溶剂的性能优于SBR硫化胶。

MAX1999EEI Pinout: 8- to 32-bit and 16- to 32-bit word packing options Programmable wait state options: 2 to 31 CCLK Digital audio interface includes six serial ports, two pre- cision clock generators, an input data port, three programmable timers and a signal routing unit Serial ports provide: Six dual data line serial ports that operate at up to 50 Mbits/s for a 200 MHz core on each data line each has a clock, frame sync, and two data lines that can be configured as either a receiver or transmitter pair Left-justified sample pair and I2S support, programmable direction for up to 24 simultaneous receive or transmit channels using two I2S compatible stereo devices per serial port TDM support for telecommunications interfaces including 128 TDM channel support for telephony interfaces such as H.100/H.110 Up to 12 TDM stream support, each with 128 channels per frame Companding selection on a per channel basis in TDM mode Input data port provides an additional input path to the DSP core configurable as either eight channels of I2S or serial data or as seven channels plus a single 20-bit wide syn- chronous parallel data acquisition port Supports receive audio channel data in I2S, left-justified sample pair, or right-justified mode Signal routing unit provides configurable and flexible connections between all DAI components, six serial ports, an input data port, two precision clock generators, three timers, 10 interrupts, six flag inputs, six flag outputs, and 20 SRU I/O pins Serial peripheral interface Master or slave serial boot through SPI Full-duplex operation Master-slave mode multimaster support Open drain outputs Programmable baud rates, clock polarities, and phases 3 Muxed Flag/IRQ lines 1 Muxed Flag/Timer expired line ROM based security features: JTAG access to memory permitted with a 64-bit key Protected memory regions that can be assigned to limit access under program control to sensitive code PLL has a wide variety of software and hardware multi- plier/divider ratios JTAG background telemetry for enhanced emulation features IEEE 1149.1 JTAG standard test access port and on-chip emulation Dual voltage: 3.3 V I/O, 1.2 V core Available in 136-ball BGA and 144-lead LQFP packages Lead free packages are also available

MAX1999EEI引脚说明: 8 - 32位和16 - 32位字包装选择可编程等待状态的选择:2至31个CCLK数字音频接口包括6个串行端口,两个前643时钟发生器,输入数据端口, 3可编程定时器和一个信号路由单元串行端口提供:六双串口数据线,在高达50 Mbps的操作/为200兆赫的每个数据行每个人都有一个时钟,帧同步的核心秒,和两个数据可以作为任何一个接收器或发射器对左对齐和I2S配对样本的支持下,最多可同时接收或传送24个频道,每使用两个系列的I2S兼容立体声设备配置可编程方向线;港口的TDM通信接口,包括支持128个电话接口的TDM的渠道,如H.100/H.110支持多达12个的TDM流的支持下,每帧128个频道每个压缩扩展每通道的基础上选择在TDM模式输入数据端口提供了一个额外的输入路径的DSP核心配置为I2S或串行数据或7加一个20位宽的SYN -异步的并行数据采集接口通道或8通道;支持接收通道I2S音频数据,左对齐样本对,或右对齐模式信号路由单元组件之间提供所有戴配置和灵活的连接,6个串行端口,一个输入数据端口,两个精密时钟发生器,3个定时器,10个中断,六旗投入,产出6个旗,20曼谷南南区域股的I / O管脚串行外设接口的硕士或奴隶通过SPI串行启动全双工运作主从模式多主机支持开漏输出可编程波特率,时钟极性和第三期合并调制旗/ IRQ线路1合并调制旗/定时器过期线光盘的防伪特征:JTAG的访问与64位受保护的关键允许内存内存可分配给程序访问控制的限制下对敏感地区有一个代码锁相环/遥测分比率为背景的JTAG仿真功能增强的IEEE 1149.1 JTAG标准测试访问端口的软件和硬件多钳各种各样和片上仿真双电压:3.3六/输出,可在1.2 V核心136球BGA封装和144引脚LQFP封装无铅封装,也可

TDA4864 Pinout: 8- to 32-bit and 16- to 32-bit word packing options Programmable wait state options: 2 to 31 CCLK Digital audio interface includes six serial ports, two pre- cision clock generators, an input data port, three programmable timers and a signal routing unit Serial ports provide: Six dual data line serial ports that operate at up to 50 Mbits/s for a 200 MHz core on each data line each has a clock, frame sync, and two data lines that can be configured as either a receiver or transmitter pair Left-justified sample pair and I2S support, programmable direction for up to 24 simultaneous receive or transmit channels using two I2S compatible stereo devices per serial port TDM support for telecommunications interfaces including 128 TDM channel support for telephony interfaces such as H.100/H.110 Up to 12 TDM stream support, each with 128 channels per frame Companding selection on a per channel basis in TDM mode Input data port provides an additional input path to the DSP core configurable as either eight channels of I2S or serial data or as seven channels plus a single 20-bit wide syn- chronous parallel data acquisition port Supports receive audio channel data in I2S, left-justified sample pair, or right-justified mode Signal routing unit provides configurable and flexible connections between all DAI components, six serial ports, an input data port, two precision clock generators, three timers, 10 interrupts, six flag inputs, six flag outputs, and 20 SRU I/O pins Serial peripheral interface Master or slave serial boot through SPI Full-duplex operation Master-slave mode multimaster support Open drain outputs Programmable baud rates, clock polarities, and phases 3 Muxed Flag/IRQ lines 1 Muxed Flag/Timer expired line ROM based security features: JTAG access to memory permitted with a 64-bit key Protected memory regions that can be assigned to limit access under program control to sensitive code PLL has a wide variety of software and hardware multi- plier/divider ratios JTAG background telemetry for enhanced emulation features IEEE 1149.1 JTAG standard test access port and on-chip emulation Dual voltage: 3.3 V I/O, 1.2 V core Available in 136-ball BGA and 144-lead LQFP packages Lead free packages are also available

TDA4864引脚说明: 8 - 32位和16 - 32位字包装选择可编程等待状态的选择:2至31个CCLK数字音频接口包括6个串行端口,两个前643时钟发生器,输入数据端口, 3可编程定时器和一个信号路由单元串行端口提供:六双串口数据线,在高达50 Mbps的操作/为200兆赫的每个数据行每个人都有一个时钟,帧同步的核心秒,和两个数据可以作为任何一个接收器或发射器对左对齐和I2S样本对支持,最多可同时接收或传送24个频道,每使用两个系列的I2S兼容立体声设备配置可编程方向线;港口的TDM通信接口,包括支持128个电话接口的TDM的渠道,如H.100/H.110支持多达12个的TDM流的支持下,每帧128个频道每个压缩扩展每通道的基础上选择在TDM模式输入数据端口提供了一个额外的输入路径的DSP核心配置为I2S或串行数据或7加一个20位宽的SYN -异步的并行数据采集接口通道或8通道;支持接收通道I2S音频数据,左对齐样本对,或右对齐模式信号路由单元组件之间提供所有戴配置和灵活的连接,6个串行端口,一个输入数据端口,两个精密时钟发生器,3个定时器,10个中断,六旗投入,产出6个旗,20曼谷南南区域股的I / O管脚串行外设接口的硕士或奴隶通过SPI串行启动全双工运作主从模式多主机支持开漏输出可编程波特率,时钟极性和第三期合并调制旗/ IRQ线路1合并调制旗/定时器过期线光盘的防伪特征:JTAG的访问与64位受保护的关键允许内存内存可分配给程序访问控制的限制下对敏感地区有一个代码锁相环/分比率背景遥测的JTAG仿真功能增强的IEEE 1149.1 JTAG标准测试访问端口软件和硬件多钳各种各样和片上仿真双电压:3.3六/输出,可在1.2 V核心136球BGA封装和144引脚LQFP封装无铅封装,也可

In the present dissertation, a surfactant-templated mesoporous silica molecular sieve with high pore volume, high porosity and narrow bimodal mesopore size distribution was synthesized for the first time in a reaction system, which was used usually in the synthesis of mesoporous MCM-41 molecular sieves, by a judiciously controlled two-phase sol-gel processing under basic conditions.

在本论文中,我们通过对一个通常用于制备介孔MCM-41分子筛的反应体系中正硅酸乙酯水解与缩合反应相对速率的精确调控,首次在弱碱性体系中合成了一种具有高孔隙率、大孔体积和双介孔孔分布特征的新型二氧化硅分子筛材料,简记为BMS,并对BMS二氧化硅分子筛中双介孔结构形成的原因及各种可能对其结构和性质产生影响的合成因素如Ammonia/silica摩尔比、组分浓度的变化、表面活性剂烷基链长度的调节、辅助有机物均三甲苯的引入、催化剂的结构和性质、溶剂和助溶剂的极性和用量、老化和干燥条件的变化及合成后水热处理等,利用不同的测试手段如XRD,SEM,TEM,〓Si MAS NMR,TG-DTA,N〓吸附测试等进行了系统的表征研究。

Therefore, the EL spectra of (Znq_2)_4 is wider than that of Znq_2. 4._2 was synthesized. The analysis of molecular spatial structure and the characterization of material performance of_2 and Liq showed that two Liq molecules and two Naq molecules were connected by Na-O-Na bond bridges to form_2. Compared with Liq,_2 exhibits stronger rigidity in planar molecular structure, larger steric hindrance and intermolecular distance, and much smaller molecular polarity, thus resulting in much longer fluorescence lifetime, much higher fluorescence quantum efficiency, wider energy bandgap and better film formability. When used as light-emitting layer in OLED,_2 shows lower formation probability of excited dimmer and exciplex formation than Liq, thus emits bluer light with higher current efficiency than Liq. When_2 ultrathin film is used as electron injection layer in OLED, it exhibits higher current density, higher luminance, lower turn-on voltage and higher current efficiency than Liq ultrathin film for the existence of sodium ions in_2 ultrathin film. 5. The summarization the relationship between molecular spatial structure and material performance of Alq_3,(Znq_2) and Liq, lead the conclusion that the molecular spatial structure of Mq_n affects its material performance in such aspects as the rigidity of planar molecular structure, intermolecular interaction, molecule stacking mode and intermolecular distance.

制备了_2,通过对_2和Liq的分子空间结构与性能进行分析与讨论,发现_2是通过两个Na-O-Na键桥将两个Liq和两个Naq连接构成的,其分子平面结构的刚性程度强于Liq,空间位阻大于Liq,分子之间的距离大于Liq,分子极性远远小于Liq;_2的荧光寿命长于Liq,荧光量子效率高于Liq,成膜性优于Liq;_2的禁带宽度比Liq大,光致发光光谱中_2的最大发射峰较Liq发生蓝移;当_2在OLED中作为发光层时,激发二聚体与激基复合物的生成几率远远小于Liq,发的光比Liq更蓝,电流效率大于Liq;_2超薄膜中有Na离子的存在,与Liq超薄膜相比,当其在OLED中作为电子注入层时,具有更大的电流密度,更高的发光强度,更低的阈值电压和更高的电流效率 5、对上述Alq_3、Znq_2和Liq的分子空间结构与材料性能之间的关系进行了归纳总结,认为Mq_n的分子空间结构主要在分子平面结构的刚性程度,相邻分子之间的相互作用,分子堆叠的方式和分子之间的距离这四个方面影响其性能。

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