极性的

The Diels-Alder cycloadditions of [60] fullerene for preparation of optical limitingmaterials are discussed in chapter 3 and 6. Soluble cycloaddition derivatives of 〓aresynthesized by the reaction of 〓 with indene,1,1'-biindene andcyclopentadiene derivatives.〓Particular, the Diels-Alder cycloaddition of 〓 with1,1'-biindene under controlled conditions affords the stable monoadduct 〓〓of novel structure, which was confirmed by HPLC, FTIR, FD-MS,〓NMR,〓 NMR, HMQC and HMBC spectra, Its two bridgehead cage carbons resonate at70.91ppm, The 〓 NMR spectra showed 38 lines consistent with the 〓 symmetryassociated with [6,6] addition. The 〓 shows similar optical limitingproperties to that of 〓 in toluene for 8ns laser at wave length 532nm. Moreover, thehigh solubility of this adduct in polar solvents such as THF, acetone enables itsincorporation into sol-gel glass matrix. The thin films prepared via the sol-gel methodshow improved OL behaviour compared to those of 〓. The langmuir-Blodgett filmformation and uv-visible absorption of 〓 are also investigated. LBmonolayer of this compound is prepared on the air-water interface at 〓 mol/l. In chapter 4, three water-soluble derivatives of [60] fullerene: fullerol(1), theaddition product (2)of fullerol (1)with polyvinylpyrrolidone and fumaric acidderivative of 〓(3) are synthesized and characterized.

通过Diels-Alder环加成反应，用茚〓和1，1'-联茚〓及取代茂合成了一系列可溶性的〓环加成衍生物，发现可控制反应条件，使1，1'-联茚与〓反应，并高产率地得到具有新颖结构的单加成物，用HPLC、FTIR、FD-MS 及〓、HMQC、HMBC等多种波谱技术对其结构进行表征，测得它的两个〓杂化的桥头碳的化学位移为〓ppm，证明生成的衍生物为6∶6闭式环加成，〓NMR谱中共给出38个信号，表明〓联茚衍生物分子具有〓对称性；在波长532nm，脉冲宽度8ns的激光下，〓联茚衍生物的甲苯溶液的光限幅性能与〓的甲苯溶液相近，由于〓联茚单加成衍生物熱稳定性好，在四氢呋喃，丙酮等极性溶剂中溶解性好，能分别均匀地掺入溶胶-凝胶中，已发现它的溶胶(so1)光限幅性能优于纯〓的光限幅性能；使用Langmuir-Blodgett技术将〓联茚衍生物在空气和水的界面进行了LB单层膜和多层膜实验以及UV-Vis吸收谱研究，通过等温压缩曲线测试，证明浓度为〓〓时，〓联茚衍生物能够形成单层膜。

From the calculations, it can be found that the van der Waals interactions, the hydrophobic interactions, as well as the H-bonding interactions are crucial for the ligand binding. The 4-phenylamino group can produce strong van der Waals adn hydrophobic interactions with the nonpolar side chains of the residues deep in the binding cleft. The R^1 and R^2 substituents on the bicyclic chromophore can also produce strong van der Waals and hydrophobic interactions with the residues located at the exterior part of the binding pocket. Moreover, the two N atoms of the quinazoline can form H-bonds with EGFR, which will produce significant contribution to biological activities. The calculated nonbonded interactions between anilinoquinazolines and EGFR, as well as the information obtained from the predicted complexes, can interpret the structure-activities of the inhibitors well, which can afford us important information for structure-based drug design.

从模拟结果得到的抑制剂和靶酶之间的相互作用模式表明范德华相互作用、疏水相互作用以及氢键相互作用对抑制剂的活性都有重要的影响，抑制剂的苯胺部分位于活性口袋的底部，能够与受体残基的非极性侧链产生很强的范德华和疏水相互作用，抑制剂双环上的取代基团也能和活性口袋外部的部分残基形成一定的范德华和疏水性相互作用，而抑制剂喹唑啉环上的氮原子能和周围的残基形成较强的氢键相互作用，对抑制剂的活性有较大的影响，计算得到抑制剂和靶酶之间的非键相互作用能以及抑制剂和靶酶之间的相互作用信息能够很好地解释抑制剂活性和结构的关系，为全新抑制剂的设计提供了重要的结构信息。

At the BCL of 500ms, 1000ms and 2000ms,the VWtimes increased markedly with the BCL prolonging, and the degree of increasing was even obviously when heart rate was slow (BCL=2000ms or 1000ms). The enlargement of VWs was a most important reason to increase the incidence of ventricular arrhythmias; 2）At the BCL of 500ms, 1000ms or 2000ms,the VWtimes of the premature stimulates S2 was at endomembrane were wider than at the outermembrane. We supposed that premature stimulates come from endomembrane was easier inducing VF compared with outermembrane;3The VWtime of unidirectional block was wider than reentry's, we can see that reporlarization dispersion changed dynamicly. 4The QRS polar of the premature stimulates was opposite the primary beats ,which suggesting that excitation of inducing premature beats was coming from epicardial. That is to say electrotonic potential take part in the creation of reentry;5With the ratio of the Tp-e/QT increasing the occurrence of VF was upgrading. So the ratio was an effective method to estimate the event of SCD.6 The VWtimes of S3 were broaden than S2's. But we can not study penetratingly, which is the contents of our future studies.

在BCL为500ms、 1000ms和2000ms刺激条件下，随着刺激周长的增加单向传导阻滞时间易损窗呈增大趋势；并且在心率较慢时(BCL为2000ms和1000ms)增大最明显，是LQTS患者室性心律失常发生率增加的原因之一；2）在BCL为500ms、 1000ms和2000ms刺激条件下，S2位于内膜侧时时间易损窗大于在外膜侧时的，推测来自于内膜侧的期前刺激易于诱发室性心律失常；3）折返激动时间易损窗小于在单向传导阻滞时间易损窗，折返易发生于S2刚进入单向传导阻滞区间时，这说明复极梯度的不均一是动态变化的；4心电图上倒置QRS波与正常S1刺激所引起QRS波极性相反，提示不同位置S2刺激引发的室性早搏的兴奋均来自于外膜侧，说明了电紧张电位扩布参与了折返的产生；5）Tp－e/QT可以反应跨膜复极离散度，随着Tp－e/QT比值的增加PVT的发生增多，其可以用来预测室性心律失常的发生。6）随着期前刺激数目的增加时间易损窗增大。

Skill-mental dominated event-group has characteristics what are polarizing frighten goal and fluctuating variation course. 6 Coaches and athletes must insist on the principles that is comminuting of judging accurately and intervening in good time, perspective with getting practical to combine together, timeliness and synchronous combine together, controllability and principle that substantial results combine together.

影响竞赛过程中运动员竞技能力变异的众多因素可聚合为以下四个相对独立又相互联系的子系统，即：运动员的竞技状态与相对竞技实力、参赛认知水平与比赛经验、可逆转环境和中立环境。4运动员竞技能力的参赛变异具有变异成因的多元性和多变性、变异内容体能的先导性、变异过程的可控性与非可控性、变异结果的两极性和层次性和参赛行为的心态易变性等五个方面的一般训练学特征。5体能主导类项群具有变异结果直观性、变异过程连续性和对手制约两重性等特征；技能主导类项群具有单项贡献制约性、个体变异传递性和裁判评定诱导性等特征；技战能主导类项群具有群体整合共生性、核心技战术制导性、攻防转换制约性和局盘赛点突增性等特征；技心能主导类项群具有目标恐惧极化性和变异过程波动性等特征。6教练员、运动员必须坚持准确判断和适时干预相结合、前瞻性与务实性相结合、适时性与同步性相结合、可控性与实效性相结合的原则。

In the second study, interpersonal and social rhythm therapy was 1 of 3 intense psychotherapies that resulted in better outcomes than collaborative care, in a 1-year randomized study that was part of the Systematic Treatment Enhancement Program for Bipolar Disorder trial (Miklowitz DJ et al. Arch Gen Psychiatry 2007;64:419-426). A total of 293 outpatients with bipolar I or II disorder and depression treated with protocol pharmacotherapy were randomized to up to 30 sessions of intensive psychotherapy with 1 of 3 methods — interpersonal and social rhythm therapy, family-focused therapy, or cognitive behavior therapy — or to 3 sessions of collaborative care treatment. Compared with patients treated with brief collaborative care, patients receiving intensive psychotherapy attained remission of depression within a shorter time.

在第二项研究中，个体间与社会节律疗法是三种密集精神治疗中的一环，这些治疗的预后比联合照护好，这项研究是一项为期一年的随机分派研究，且是Systematic Treatment Enhancement Program for Bipolar Disorder试验的一部份（Miklowitz，等人Arch Gen Psychiatry 2007；64：419-426），总共有293位罹患第一或第二型双极性异常与忧郁症，且正在接受药物治疗疗程的门诊病患，他们被随机分派接受高达30次的密集精神治疗，分别是个体间与社会节律疗法、家庭疗法或是认知行为治疗，或是接受三次的联合照护治疗；相较於接受行为治疗照护的病患，接受密集精神治疗的病患达到忧郁症状消退的时间较快。

Because a part of hydroxyl group in methyl cellulose were substituted by trimethylsilyl group , the product could be dissolved in amounts of common organic solvents, such as chloroform, xylene and so on.

通过甲基纤维素与六甲基二硅亚胺的反应，成功地实现了对水溶性物质甲基纤维素醚三甲基硅化的改性；红外光谱验证了反应的发生，核磁共振氢谱确定了三甲基硅甲基纤维素的取代度；纤维素醚上的部分羟基被三甲基硅化后取得了在普通溶剂中的良好的溶解性，且随着取代度的增加，在非极性溶剂中的溶解性逐渐变好；通过热失重实验，对其热稳定性进行了测试。

Wheares under buffer pH5.2, there is no strong static electricity and instead being a longer wavelength movement; SDS\'s participation just restricts the relative movement of heme\'s ethylene; a new fluorescent peak forms and the reduction of enzymatic activity is due to the packing of micella\'s formation.

强变性的阴离子表活剂SDS与带净正电荷和弱负电荷的SBP(处于pH2.6和4.2缓冲液中)有强烈的静电力作用，酶活力丧失，二级结构变化，荧光强度增加，特征Soret发生蓝移，卟啉环的π-π*共轭的分裂能增大；而当SBP带净负电荷(pH5.2)时，没有静电吸引力，Soret带发生红移；SDS的引入只是限制了血红素上乙烯取代基的运动，使其与卟啉环共轭：极性环境的变化导致产生新的荧光峰；酶活力因胶团包裹作用而有下降。

Cable .Make use of this principle, we can quickly locate the target cable or break point from large amount of cables, under carpet, the inner of decoration wall and over ceiling1 operation is simple , reliable , the interface is nimble , use is broad , bionic form , carry-over are convenient, since our link tester has two signal output port, it can work when switch is running, this is very convenient. 2 applies to all metal cable such as network cable , tele phone line cable , video cable , automobile circuit .it can not be work with high voltage(above 80V),if you want to locate it ,please turn off the cable power supply3 can test the telephone line polarity, connectedness, rough position of breaking point.4 uses the two crocodile clamp to avoid getting rid of the job of make network cable. Use the RJ45/RJ11 interface can connect to the network and the telephone line directly.5 link tester can find out that pair of circuit line cable from large mount of cables. 6 high amplitude ranks 200 times amplification circuit is sui table to locate long distance cable.7 two-sided network lines sequence indicator is easy to examine the network line cable whether or not correctly conveniently. 8 portable types multifunctional bag can encase most of your engineering tools; remit your messy carry-over of implement bothering. 9 adopt two 9V batteries.

线路通产品特点：1 操作简单、性能可靠，接口灵活、用途广泛，仿生外形、携带方便，由于本设备采用了信号双路输出方式，可以解决交换机工作状态下使用，避免了关掉交换机影响其他线路的使用的麻烦。2 适用于查找网络电缆、电话线路、视频电缆、汽车电路、无强电状态下的所有金属电缆。3 可以测试电话线路极性、连通性，断点大概位置。4 两个鳄鱼嘴夹，避免了去做水晶头的麻烦，RJ45/RJ11接口线，可直接连接网络和电话线模块。5 寻线器快速地在众多紊乱的线路中找出需要查找的那一对线路线缆。6 高音频振幅级别200倍的放大电路，适合长距离电缆定位。7 双面网络线续灯可以更直观方便的检查校正网络线续线路连接是否正确。8 便携式多功能软包，可以把您工程施工、维护的基本工具装齐，免除您工具散乱携带的麻烦。9 本寻线器采用2节9V电池。

Be work with high voltage(above 80V),if you want to locate it ,please turn off the cable power supply3 can test the telephone line polarity, connectedness, rough position of breaking point.4 uses the two crocodile clamp to avoid getting rid of the job of make network cable. Use the RJ45/RJ11 interface can connect to the network and the telephone line directly.5 link tester can find out that pair of circuit line cable from large mount of cables. 6 high amplitude ranks 200 times amplification circuit is suitable to locate long distance cable.7 two-sided network lines sequence indicator is easy to examine the network line cable whether or not correctly conveniently. 8 portable types multifunctional bag can encase most of your engineering tools; remit your messy carry-over of implement bothering. 9 adopt two 9V batteries.

l线路通产品特点：1 操作简单、性能可靠，接口灵活、用途广泛，仿生外形、携带方便，由于本设备采用了信号双路输出方式，可以解决交换机工作状态下使用，避免了关掉交换机影响其他线路的使用的麻烦。2 适用于查找网络电缆、电话线路、视频电缆、汽车电路、无强电状态下的所有金属电缆。3 可以测试电话线路极性、连通性，断点大概位置。4 两个鳄鱼嘴夹，避免了去做水晶头的麻烦，RJ45/RJ11接口线，可直接连接网络和电话线模块。5 寻线器快速地在众多紊乱的线路中找出需要查找的那一对线路线缆。6 高音频振幅级别200倍的放大电路，适合长距离电缆定位。7 双面网络线续灯可以更直观方便的检查校正网络线续线路连接是否正确。8 便携式多功能软包，可以把您工程施工、维护的基本工具装齐，免除您工具散乱携带的麻烦。9 本寻线器采用2节9V电池。

The emulsion quartz stone material protective agent's solute has certain active multi-compositions and so on of functionality siloxanes and fluorine silicon hydride, this kind groups with the active ingredient carry alcoholysis reaction the ion condition water on quartz stone material surface, thus causes the siloxanes and the fluorine siloxanes has chemistry keying connection with the quartz stone surface, from outside to inside of the quartz stone surface and stone inside pore surface forms a kind of complex network structure, this kind of network structure is extremely dense, it may filter polar and carbon dioxide, slows down the speed that water molecules go in and out the quartz stone pore, so the quartz stone will not be soaked by the water molecules, meanwhile to be a barrier to stop alkaline compounds and salt to infiltrate from an interface to another, also can have the very good physical enhancement effect.

乳液型石材防护剂的溶质是具有一定活性的多官能度的硅氧烷和氟硅烷等组成，这种带有活性成份的基团与石材表层离子态水进行醇解反应，从而使硅氧烷和氟硅氧烷与石材表面进行化学键连接，由外向内在石材表面和石材内部毛的表层形成一种结构复杂的网状结构，此种网状结构极其密实，它可将极性水分子和二氧化碳进行过滤，减缓水分子进出石材毛孔的速度，不会被水分子浸湿，同时还有阻隔石材不同界面的碱性化合物和盐份向另外一个界面渗透，同时还能起到很好的物理增强效果。

However, as the name（read－only memory）implies, CD disks cannot be written onorchanged in any way.

然而，正如其名字所指出的那样，CD盘不能写，也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口，替代木托盘，免薰蒸，符合欧盟、北美各国对出口货物包装材料的法令要求；喷涂钢托盘适用于重载上货架之用，托盘表面根据需要制作成平板状、波纹状及间隔形式，满足不同的使用要求。