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We investigated constituent of triterpenoid saponins ofAlbizzia, two new compounds together with two known compounds were isolated from Albizzia julibrissin Durazz. by using column chromatography (macroreticular resin, silica gel, Sephadex gel, reverse phase silica gel),preparative HPLC methods et al.On the basis of spectroscopic analysis, including IR,ESI-MS,~1H-NMR,~(13)C-NMR,HMBC,HMQC,~1H-~1HCOSY and chemical methods, the structure of two new compounds were identified as 3 - O -[β-D-xylopyranosyl(1→2)-β-D-fucopyranosyl (1→6)-β- D -2- deoxy - 2 - acetoamidoglucopyranosyl] -21-O-[(6S)-2- trans- 2,6-dimethyl - 6 - O-β- D - quinovopyranosyl -2,7- octadienoyl] - acacic acid- 28 - O-β-D-glucopyranosyl(1→3)[α-L-arabinofuranosyl(1→4)]-α-L-rhamnopyranosyl(1→2)-β-D-glucopyranoside acacic acid 3- O -β- D- glucopyranosy(1→3)-β- D- fucopyranosl(1→6) [β-D- xylopyranosyl (1→2)]-β-D-glucopyranoside ;two known compounds were acacic acid lactone 3- O -β-D- xylopyranosyl-(1→2)-β-D-fucopyranosl (1→6)- 2-deoxy -2 -acetoamido -β-D- glucopyranoside ; acacic acid lactone 3- O-β-D-xylopyranosyl(1→2)-α-L- arabinopyranosl (1→6)- 2- deoxy - 2- acetoamido -β-D-glucopyranoside . The study lays chemical foundation and chemical reference substance for enhancing quality standard of Albizzia julibrissin Durazz.

本研究论文在综述国内外对合欢属Albizzia三萜皂苷化学成分和药理作用研究进展的基础上,利用传统植化分离手段和现代分离技术,包括大孔树脂、硅胶、葡聚糖凝胶、反相硅胶等柱色谱,制备高效液相色谱法等技术从中药合欢皮中分离得到了4个化合物,其中,2个新化合物和2个己知化合物,并进一步通过现代分析技术IR,ESI-MS,~1H-NMR,~(13C-NMR,HMBC,HMQC,~1H-~1HCOSY等和化学方法鉴定了2个新化合物的结构分别是:3-O-[β-D-吡喃木糖基(1→2)-β-D-吡喃夫糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖基]-21-O-[(6S)-2-反式-2,6-二甲基-6-O-β-D-吡喃鸡纳糖基-2,7-辛二烯酸基]-金合欢酸-28-O-α-L-呋喃阿拉伯糖基(1→4)[β-D-吡喃葡萄糖基(1→3)]-α-L-吡喃鼠糖基(1→2)-β-D-吡喃葡萄糖苷,金合欢酸3-O-β-D-吡喃葡萄糖基(1→3)-β-D-吡喃夫糖基(1→6)[β-D-吡喃木糖基(1→2)]-β-D-吡喃葡萄糖苷;2个已知化合物结构分别是:金和欢酸内酯3-O-β-D-吡喃木糖基(1→2)-β-D-吡喃夫糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖苷,金和欢酸内酯3-O-β-D-吡喃木糖基(1→2)-α-L-吡喃阿拉伯糖基(1→6)-β-D-2-去氧-2-乙酰氨基吡喃葡萄糖苷。

Classics commissioner can be chosen seriously, the Babaji in A is round Ma Yun of trustee bureau chairman, the Communist Party of China 17 big delegates, the Chinese People's Liberation Army major general of army of Gu Dan of 211 hospitals dean , hou Xiulan of president of elementary school of test of city of Benxi of province of the delegate of outstanding basic level that teachs battlefront, Liaoning , the times van that socialistic new rural area builds, Sichuan saves double Mao Jiawan drifting a county to press down alcalde Mao Guocong, have " northeast civilian tells an official the first person " praise Jiang Caiyi of director of office of Liaoning Jing Heng's attorney, and Niu Shuhai, Li Chunyou, Ji Shengjun, Chen Gang, Zheng Yuanzhong be elected for times of the 6th China character of 10 big news.

经评委会认真评选,阿里巴巴集团董事局主席马云,中共17大代表、中国人民解放军211医院院长贾丹兵少将,教育战线的优秀基层代表、辽宁省本溪市实验小学校长侯秀兰,社会主义新农村建设的时代先锋、四川省双流县毛家湾镇镇长毛国聪,有"东北民告官第一人"之誉的辽宁敬恒律师事务所主任姜彩熠,以及牛树海、春友、季胜军、陈刚、郑元忠等当选为第6届中国时代十大新闻人物。

Based on the filtered Lie algebra of the universal enveloping algebra, the algebraic structure of projected subsystems are studied. It is proved that they have simple decompositions, and the construction of the representations is given as well as the corresponding criterion for project limit controllability.

基于泛包络代数的滤代数结构,研究了投影子系统的代数结构,证明它们具有简单的分解形式,并给出了它们的表示的构造方法和投影极限能控性的判别定理。

In the recent years, due to there being intrinsic relationships between tilting theory and quantum group, Lie algebra and other algebraic branch, tilting theory has been one of the international hot topics.

现在,由于倾斜理论与量子群,代数等其它代数学科的本质联系,倾斜理论成为国际研究热点之一。1998年,I。

Buildings and Classical Groups provides essential background material for specialists in several fields, particularly mathematicians interested in automorphic forms, representation theory, p-adic groups, number theory, algebraic groups, and Lie theory.

建筑物和古典组在多个领域提供必要的背景材料的专家,尤其是数学家在自守形式,表象理论,p进组,数论,代数群感兴趣,theor

Dear alice green, I feel truly grateful for all what you've done for my mother.on the morning of nov.28, my mother broke her legs in an accident while riding to workplace.she was so painful that she couldnt walk.fortunately she met u who was so kind and warm-heartd to sent her to hospital and home.Without you i can not imagine how could my mom live through that horrible time. its comforting that my mom gets much better now ,and we want to visit you to express our appreciation in person. SO could you please tell me the time you are convenient? you know we cant thank you enough. yours

假如你是华,11月28日上午,你母亲骑车上班摔坏了腿,无法行走,一名外国学生将你母亲送到医院治疗,然后又送她回家,你后来得知她叫ALICE GREEN,请你给她写一封80词左右的感谢信,并告诉她你母亲已经好多了,你准备和母亲一起去看她高一水平的,句型不要太难,简单的最好超级感谢你~!!!

Saw in hospital the tip Ang Lee alizarin red some are not cruel enough ......

看到住院的小费安茜有些不忍心了。。。。。。

Ang Lee the alizarin red will give up him once more for the tip elder brother?

安茜会为了小费再次放弃他的哥哥吗?

The etude is played at a brisk pace and studies right hand jumping between intervals larger than one octave, sometimes even stretching for two whole octaves within the time of a sixteenth note, at Allegretto tempo.

斯特是炫技派的代表,很多作品的演奏难度都很高,这首《钟》里揉合了同音轮指、长串的半音阶、单手的颤音、连续的八度进行和左手远距离的八度大跳等等高难度技巧。

Lines in recognition of Eric Lamarque, the Canadian truck driver who this past week caused extensive damage to the Mass Pike's brand-new Allston U-turn.

线路识别家祥lamarque ,加拿大卡车司机的人,这在过去一周造成广泛损害群众派克的崭新allston区掉头的。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。