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Samples were saponified with 20 g/L sodium hydroxide. The sexual hormones were then extracted with dichloromethane-acetic acetate (40∶1, v/v) under acidic conditions (pH 3, adjusted with 1 mol/L HCl ). An XTerraTMRP18 column was employed and a mixture of water-methanol-acetonitrile (50∶32∶18, v/v) was used as mobile phase. The seven sexual hormones were detected at 230 nm. The average spiked recoveries for the seven sexual hormones ranged from 75.6% to 97.8% with relative standard deviations of 1.9% to 7.2%. The linear ranges of determination were from 5 to 50 mg/L with correlation coefficients of 0.9999, and the limits of detection were from 3.7 to 12 ng.

先在试样中加入20 g/L氢氧化钠溶液与油脂进行皂化反应,然后用二氯甲烷-乙酸乙酯(体积比为40∶1)混合液在酸性条件下(pH 3)萃取,选择XTerraTMRP18色谱柱,以水-甲醇-乙腈(体积比为50∶32∶18)混合液为流动相,在波长230 nm处检测。7种性激素分离良好并排除了样品中杂质峰的干扰,低、高浓度平均回收率范围为75.6%~97.8%;相对标准偏差为1.9%~7.2%;检出限为3.7~12 ng。

It is an effective way to use the appropriate narrow bandgap nanosize semiconductors that is stable in chemical and biochemical conditions and not pollute the surroundings in reaction, which sensitizes nanocrysalline titanium dioxide carriers synchronously to prompt the utilization of the solar spectra and the efficiency of photocatalysis.

利用染料分子作表面敏化半导体材料和利用杂质掺杂来实现宽禁带半导体吸收光谱的扩展有一定的局限性,采用化学和生物惰性且对环境不产生二次污染的窄禁带半导体敏化同时考虑团簇颗粒粒径对载体性能的影响,是提高纳米二氧化钛光催化剂对阳光的吸收利用率和量子效率的有效方法。

The results show that the residue mainly consists of high-carbon alkanes, esters, elemental sulfurs, copper sulfides and mechanical impurities.

结果表明:残留物主要由高碳烷烃、酯类、单质硫、硫化铜和机械杂质等组成。

The main process of metal wire drawing wastewater treatment is removing impurity and demulsification. This article took Saint Electrician production workshop waste wiredrawing fluid (in which, COD content is 11 233 mg/L, pH value is 8.4 and the content of wire drawing oil is 4%) as research object, used chemical demulsification method and through laboratory experiment, adopted electrolyte and coagulant separately to deal with the wastewater.

金属拉丝废水的处理工艺主要过程是去除杂质和破乳,以赛特电工生产车间的废拉丝液为研究对象(COD含量为11 233 mg/L,pH值8.4,拉丝油含量4%),选用化学破乳法,通过实验室实验,分别采用电解质和混凝剂处理废液。

The results show that magnesium and aluminum theoretically can be thoroughly dissolved from the blast furnace slag by diluted sulfuric acid pretreatment on the blast furnace slag even if the ended concentration of sulfuric acid is 0.001mol/L, while the titanium basically could not be dissolved. Therefore it is theoretically indicated that the separation of the magnesium and aluminum from the slag with the least titanium loss by diluted sulfuric acid pretreatment is possible.

结果表明,采用稀硫酸对高炉渣进行预处理,当终酸浓度即使为0.001mol·l~(-1)时,镁、铝理论上也能全部被酸浸出,而钛在0.001 mol·l~(-1)的酸浓度条件下基本不被浸出,从而从理论上可以说明对高炉渣采用稀酸预处理可以很好的将炉渣中的镁、铝等杂质分离出来,而钛极少被浸出。

Air-removed filter series is the attached device of the flow meter,which can remover the air and solid impurity so as to ensure the flow metre accuracy and operation life.

消气过滤器是流量计附属设备,它具有消气、过滤液体中固体杂质的作用,从而保证流量计的计量精度,延长流量计的使用寿命。

Using polarizating microscope and reflecting microscope,we have studied the features of microstructure and basic composition of general silica brick and high quality silica brick used for large scale hot air stove and the effect of impurity content and high temperature reburning on microstructure.

用偏光和反光显微镜研究了普通硅砖与大型热风炉用优质硅砖的基本组成和显微结构特征,以及杂质含量和高温重烧对显微结构影响。

The liquid level can be measured. Said upper- and lower-limitation alarm is sound-light alarm. The valve can be controlled. The impurities in valve can be automatically removed by the reciprocating movement of valve, resulting in more convenient and more safe liquid level control.

本发明可对液位进行测量,具有上、下限报警功能,同时可以控制阀门开/关,并可通过阀门的往复运动自动清除阀内杂质、使液位控制更简便、更安全。

Usually, the pigment is extracted by acid aqueous or alcohol solution and purified by different kinds of resins.

该色素主要采用酸性水溶液或醇溶液直接浸提,利用不同类型的树脂进一步去除杂质,得到色素产品。

The effects of reaction temperature, pressure, the ratio of actual air amount to theoretical air amount, reflux rate, the contents of oil and impurities settled in alkali waste on the removal of sulfides, phenol and CODer were discussed.

同时对影响系统操作和氧化处理效果的反应温度、压力、空气比、回流量、含油量和杂质沉淀物等若干主要因素进行了分析论述。

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They weren't aggressive, but I yelled and threw a rock in their direction to get them off the trail and away from me, just in case.

他们没有侵略性,但我大喊,并在他们的方向扔石头让他们过的线索,远离我,以防万一。

In slot 2 in your bag put wrapping paper, quantity does not matter in this case.

在你的书包里槽2把包装纸、数量无关紧要。

Store this product in a sealed, lightproof, dry and cool place.

密封,遮光,置阴凉干燥处。