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Amino-2-methylpropanol was used as the chemical modifying reagent of fatty acids to modify the carboxyl group into nitrogen-containing heterocycle which would effectively prevent the migration of carbon double bonds of the alkenyl in the electron impact source.

以2-氨基-2-甲基-丙醇为脂肪酸的化学修饰试剂,气相色谱-电子轰击质谱分析葵子油脂肪酸。2-氨基-2-甲基-丙醇将脂肪酸羧基修改为含氮杂环,使在EI源中避免了链烯基中碳碳双键的移动。

ConclusionMacroreticular resin-Colorimetric method is suitable for the determination of tota1 tritepenoidic acid from Dracocephalum moldavica L.

用大孔吸附树脂对香青兰除杂后富集利用显色法测定总三萜酸是可行的,该方法具有简便、快速、准确、重复性好等优点。

The original Seluohe Group contains at least four parts: Late Archean metamorphic rocks (zircon SHRIMP protolith ages 2517~2534 Ma), Late Paleozoic metamorphosed volcanic-sedimentary strata (zircon SHRIMP 252 Ma), Permian gneissic granitic complex (zircon SHRIMP 260 Ma), and Jurassic mylonitized granites (zircon SHRIMP 168 Ma).

原划分的色洛河群至少由4部分组成:新太古代变质火山-沉积地层(锆石SHRIMP年龄为2517~2534 Ma)、晚古生代变质火山-沉积地层(英安岩锆石SHRIMP年龄为252 Ma)、二叠纪片麻状杂岩体(锆石SHRIMP年龄为260 Ma)和侏罗纪糜棱岩化花岗岩(锆石SHRIMP年龄为168 Ma)。

[Objective]To explore the effect of continuous physiological osteogenic stress on the bone healing of canine iliopectineal crest.[Method]Ten adult mixed breed dogs without significant individual difference were made transverse fracture at bilateral iliopectineal crest 1.5 cm above the dome of acetabulum,which were fixed with ATMFS or steel plate respectively. The animals were sacrificed and specimens were procured at 2,4,6,8 and 12 weeks after operation.Samples from the fracture gaps were investigated by histology of HE and Masson staining,image pattern analysis of new bone formation.

探讨持续顺应生理力线的压应力对犬骨盆弓状线部骨折愈合的影响[方法]选用10只成年杂家犬,双侧髋臼臼顶上方1.5 cm处横形截骨,分别采用ATMFS(骨盆髋臼三维记忆内固定系统)柱固定器和5孔重建钢板内固定,于术后2、4、6、8、12周处死动物取材,行HE染色、Masson三色法染色组织学检查,图像分析新骨形成积分光密度值,研究不同应力作用模式下的骨盆骨折愈合情况。

A reversed-phase high performance liquid chromatographic method was established for determination of isothiocyanates in human urine , which used the reaction of propyl isothiocyanate with 1,2-benzenedithiol as reference instead of the synthesis of 1,3-benzodithiole-2-thione.

省去合成1,3 苯二硫杂环五烯 2 硫酮这一步骤,直接用异硫氰酸丙基酯与1,2 苯二硫酚反应作标准,建立了尿液中异硫氰酸酯的反相高效液相色谱测定方法。

Additionally, 75 volatile chemical constituents have been identified from the petroleum ether extracted part by capillary GC-MS, and the relative percentages of them are determined by GC method. The result showed that the volatile constituents of Musella lasiocarpa mainly includes advanced alkane, aliphatic acid and ester, aldehyde, ketone, aromatic and its heterocyclic compounds. With the compounds that have been isolated and identified from Musella lasiocarpa, the biogenensis pathway of new compound MT-3 is approached. Furthermore, the bacteriostasis of the 6 compounds to Escherichia coil, Pseudomonas aerusinosa, Bacillus megaterium, Sarcina lutea and Bacillus subtilic are determined by flat dilution method.

此外,从其石油醚萃取部分用毛细管色谱法分析鉴定出75种挥发性化学成分,并测定了各组分的相对百分含量,结果表明,地涌金莲挥发性化学成分以高级烷烃、高级脂肪酸酯及醛、酮、芳香和芳香杂环化合物为主;根据从地涌金莲中鉴出和分离得到的化合物,探讨了新结构化合物MT-3的生源代谢途径;采用平板稀释法测定了地涌金莲中六种化学成分对大肠杆菌、绿脓杆菌、巨大芽孢杆菌、藤黄八叠球菌和枯草芽孢杆菌的抑菌作用。

By means of UV、IR and GC, we preliminarily analyzed the components, structures and content of the fatty acids in Trichosanthes kirilowii oil, and we also analyzed the structure of trichosanic acid .

并采用杂环化法衍生化瓜蒌仁油,应用气相色谱-质谱联用法对瓜蒌酸进行结构鉴定及含量测定,确定了瓜蒌酸的结构为C18:39c,11t,13c,采用峰面积归一化法计算出其相对质量分数为41.82%。

The roses were still fresh-colored. One of them was lilac, one was magenta, and one was dull-ivory with touches of crimson.

蔷薇的花色还是鲜艳的,一朵紫红,一朵嫩红,一杂是病黄的象牙色中带着几分血晕。

In this research, large volume stainless pots, high-quality pottery pots and enamel pots, instead of traditional small volume pottery pots, were used in storing several kinds of fresh liquor like "Shuanggou Liquor" etc.and the analysis of stored liquor by gas chromatography and atomic absorption spectrum indicated that the application of large volume stainless containers, instead of the traditional pottery pots, could not only advance liquor aging , produce flavour and remove precipitate, develop soft liquor style, stabilize and improve liquor quality,harmonize the balance of components , decrease liquor loss and liquor storage space,but also promote oxidation , reduction, esterification and molecular hydrogen bond association in the process of liquor storage.

对&双沟酒&等各香型酒,利用大容器的不锈钢罐、优质陶缸和搪瓷罐代替传统小容积陶坛或陶缸贮存新酒作了试验研究。采用气相色谱和原子吸收光谱对贮酒分析,得出采用不锈钢等大容器代替传统小陶罐贮存酒,不但可使酒在贮存过程中进行氧化、还原、酯化和分子氢键缔合作用,促进酒体老熟去杂增香,使酒体柔和老熟、成分平衡协调,稳定和提高酒质;而且还可以降低酒的损耗和减少贮酒库占地面积。孙悟

In this paper, we study grass carp skin pretreatment conditions, using the method of sodium hydroxide adding hydrogen peroxide can bleaching and removing non-collagen and defatted to grass carp skin , the role of its collagen solubility effects.

本文研究了草鱼皮的预处理工艺条件,采用氢氧化钠中添加双氧水方法可以同时起到脱色、脱杂蛋白、脱脂肪的作用,以及其对胶原蛋白的溶解性的影响。

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However, as the name(read-only memory)implies, CD disks cannot be written onorchanged in any way.

然而,正如其名字所指出的那样,CD盘不能写,也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口,替代木托盘,免薰蒸,符合欧盟、北美各国对出口货物包装材料的法令要求;喷涂钢托盘适用于重载上货架之用,托盘表面根据需要制作成平板状、波纹状及间隔形式,满足不同的使用要求。

A single payment file can be uploaded from an ERP system to effect all pan-China RMB payments and overseas payments in all currencies.

付款指令文件可从您的 ERP 系统上传到我们的电子银行系统来只是国内及对海外各种币种付款。