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Preparation of the cathode includes:shaping under the press of 40Mpa, sintering at 550℃for 1 hour and at 900℃for 8 hours and threading with molybdenum bar; Considering the literatures we choose CaCl2 as salt for preparation titanium. Pretreatment of salt is for 1 hour at 100℃and for 2 hours at 300℃. Partial pressure of oxygen which need lower than 5.11×10-7Pa to reduct titanium oxides and hygroscopic property of salt need a sealed equipment to electrolyse. And finally successfully designed a satisfied one and the results show that the equipment can be satisfied the requirment of the experiment. Flow of the inert gas is 1.5L/min, the voltage is 2.8 V, temperature is 850℃and time is 2 hours during pre-electrolysis. Flow of the inert gas is 0.2L/min, the voltage is 3.1 V, temperature is 900℃and time changes with the mass of TiO2 during electrolysis, namely the greater need the longer time; To eliminate influence of salt and other impurities, the products need to wash with distilled water and dilute chlorhydric acid , then wash with dilute hydrochloric acid under supersonic wave assistant. Finally, electrometical properties of the electrolysis of TiO2 is researched by cyclic voltammetry and chronoamperometry, and results show that there are two main reodox steps, namely from TiO2 to TiO and from TiO to Ti.
阴极制备主要包括40MPa压力下模压成型、两段式烧结(1小时内升至550℃保温1小时,再1小时升温至900℃保温8小时)及烧结后TiO2块打孔用钼棒串接三个主要环节;实验中选用CaCl2作为电解熔盐,并对其进行预处理(100℃,保温1小时; 300℃,保温2小时);经热力学计算,还原钛氧化物的氧分压至少要低于5.11×10-7Pa,结合电解过程中所用熔盐CaCl2有极强的吸水性的特点,电解装置应有较高的密封性,自行设计了一套密封性可靠的电解装置,便于实验过程中熔盐预处理和氧分压的控制;通过干燥处理预电解过程中Ar流量大约为1.5L/min、电压为2.8 V、温度为850℃、时间为2小时,电解过程中Ar流量大约为0.2L/min、电压为3.1V、温度为900℃,实验结果表明电解时间与TiO2质量密切相关,质量越大需要电解的时间越长;通过自来水冲洗—稀盐酸浸泡、洗涤—在超声波辅助作用下稀盐酸洗涤,可减少熔盐及其它杂质对电解产物检测结果的影响;最后,通过循环伏安法、计时电流法对电解机理的研究,确定电解还原TiO2制备金属钛主要经历了TiO2-TiO-Ti的过程。
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According to analysis of flow field and velocity distribution in the mix tank,the results indicate that:using draft-tube in the mix tank,the axial flowing of liquid can be increased,the circumgyration around the impeller will be improved,and the strong mixed effect can be gained.
通过对有、无导流筒的搅拌槽内流场和速度的对比分析表明:导流筒强化了搅拌槽内上下液体的整体轴向流动,在近浆区域改善了液体的跟转,有强烈的混合效果,并且,在较为理想的流场分布下,有导流筒的搅拌槽功率消耗比无导流筒搅拌槽节省12%,其结果将为搅拌槽的整体结构优化提供有效途径。
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Results Compared with the model group, crocetin can significantly reduce the cardiac indexes, obviously decrease the level of MDA, LDH and CK in the serum. Crocetin can significantly increase the activities of Na +, K +-ATPase; Ca 2+, Mg 2+-APTase; GSH-Px. The histopathological changes confirmed the protective effects of crocetin on the myocardial injury.
结果 西红花酸能显著降低血清中CK和LDH的释放;也能显著降低血清和心脏匀浆中MDA水平,心脏重量参数显示对心肌水肿有明显的抑制作用;保护心肌GSH—Px;Na^ ,K^ —ATP酶和Ca^2 ,M8^2 -ATP酶活性,心脏病理切片表明西红花酿对心肌坏死有显著的保护作用。
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The growth inhibiting rate of T24 cell lines were detected by MTT methods, apoptosis of cells were detected by flow cytometry, the mechanism of apoptosis was analyzed by detecting the protein expression of Bcl-2, Bax, Caspase-9, Caspase-3 and cytoplastic protein Cytochrome C. 4 We injected live T24 cells into the subcutaneous space of nude mice and successfully built up the animal model of bladder carcinoma. The effect of CS-PAA-EPI polymer magnetic microspheres targeting chemotherapy was investigated by HE staining, TUNEL ,tumor weight and volume inhibition rate. Results: 1 TEM revealed that the CS-PAA polymer magnetic microspheres were regular spherical shape,the average diameter was 80nm in dry condition. By controlling the pH value of the medium,polymers had positive or negative zeta potential. VSM showed the CS-PAA polymer magnetic microspheres had superparamagnetic. The diameter of CS-PAA-EPI polymer magnetic microspheres were 200nm in solution by DLS examining,the embedding ratio was 20%,the EPI loading rate was 15%, which was higer than reported in other articles. 2 Raw eye observation found that the rat"s bladder of treatment group was brown color,which meaned the aggregation of iron particles, compared with the control group, iron stain found iron particles were assembled in rat"s bladder of the treatment group, the amount of iron particles in liver and spleen were less obviously.
研究结果:1合成的CS-PAA磁性聚合物微球呈球形,大小均一,TEM测定其干态下粒径为80nm左右,磁化曲线证实具有超顺磁性,具有一定的PH敏感性,固载表柔比星后,水溶液性状稳定,无沉淀物,DLS测定直径约200nm左右,测定载药率为15%,较文献报道高,包封率为20%。2肉眼观察试验组大鼠膀胱表面呈褐色,可见大量的Fe粒子聚集,普鲁士兰染色法显示,试验组大鼠膀胱壁内有大量的Fe粒子,分布至膀胱壁全层,与对照组大鼠相比,试验组大鼠的肝、脾内的Fe粒子聚集量明显降低;HPLC测定结果与Fe染色相同;高剂量磁性CS-PAA-EPI生理盐水组及单纯EPI生理盐水组均在给药后14天出现血肌酐和尿素氮的升高,其他组大鼠血生化指标没有明显变化。3MTT法发现,高、中、低剂量磁性CS-PAA-EPI生理盐水组在外加磁场的协同作用下杀伤T24细胞效应明显高于单纯的EPI生理盐水组,FCM发现试验药物组可引起明显的肿瘤细胞凋亡,试验药物治疗组细胞胞浆内出现了由线粒体释放出的细胞色素C,试验组细胞Bcl-2蛋白减少,Bax蛋白变化不明显,Caspase-3、Caspase-9蛋白受到了激活活化。4高、中、低剂量磁性CS-PAA-EPI生理盐水组的瘤重抑制率和瘤体积抑制率均明显高于单纯的EPI生理盐水组(P<0.01),其中高剂量组的抑制率最高。
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The results show that there are obvious annual and decadal changes in East Asia summer monsoon circulation, and there are qui...
结果表明:东亚夏季风环流强度有明显的年际变化和年代际变化,且与赤道东太平洋SST有较好的负相关关系,其中又以与三个月前的海温变化关系最好。
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Still, the definition, operationalization, and classification of these concepts have all been criticized. In addition, when used in Cross-countries studies there have been glaring methodological errors. Furthermore, at the national level, electoral formula and district magnitude have only limited influence on disproportionality.
不过,本文研究发现:这些概念在界定、运作化与分类等方面都有争议;而且学者们所从事的跨国性比较研究,在方法论上也有明显的缺失;再者,当选规则与选举区规模,对全国层次选举结果不比例性的影响属次要因素,只有间接作用。
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RESULTS:Kugua Tea distinctly inhibited the increase of inflammatory edema caused by the inflammatory agents,reduced the generating heat caused by the fermentum,yet showed antidefatigation,promoting macrophage phagocytosis and bacteriostasis.
结果:苦瓜茶对致炎剂引起的炎性水肿均有明显的抑制作用,减轻酵母性发热,抗疲劳,提高巨噬细胞的吞噬功能,体外有明显抑菌作用。
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Firstly, wettability and adhesive properties of the major soy protein components conglycinin (7S) and glycinin (11S) after urea modification were characterized. Modified 7S and 11S soy proteins were evaluated for gluing strength with pine, walnut, and cherry plywood and for wettability using a bubble shape analyzer. The molecular structure change was studied by chemical analysis, DSC and Rheometer. The results showed that different adhesives had varying degrees of wettability on the wood specimens.
液滴形状分析结果表明不同的胶粘剂在不同的木块上有不同的湿润性能,7S蛋白经过尿素变性后在胡桃木和樱桃木上有较好的湿润性能,11S蛋白经过1 mol/L尿素变性后在松木上有好的湿润性能。1 mol/L尿素变性使得11S蛋白在三种木块上的胶粘强度在所有胶粘剂中为最大;3 mol/L尿素变性使得7S蛋白在胡桃木和樱桃木上的胶粘强度比11S的大,但在松木上的胶粘强度则是11S/3M高于7S/3M。
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Observation was made on the content of malondialdehyde. Results Compared with MC group, the increases of MDA content in the membrane induced by XanXO system, H2O2 or UV light in all of the three Punica granatum L.group were inhibited dosedependently.
结果 同MC组相比,三组石榴皮提取物对黄嘌呤-黄嘌呤氧化酶系统、H2O2及UV照射3种方法引起的细胞膜脂质过氧化产物丙二醛的生成增加均有抑制作用,且有一定的剂量依赖关系。
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Observation was made on the content of malondialdehyde. Results Compared with MC group, the increases of MDA content in the membrane induced by Xan?XO system, H2O2 or UV light in all of the three Punica granatum L.group were inhibited dose?dependently.
结果 同MC组相比,三组石榴皮提取物对黄嘌呤-黄嘌呤氧化酶系统、H2O2及UV照射3种方法引起的细胞膜脂质过氧化产物丙二醛的生成增加均有抑制作用,且有一定的剂量依赖关系。
- 推荐网络例句
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I am accused of being overreligious," she said in her quiet, frank manner,"but that does not prevent me thinking the children very cruel who obstinately commit such suicide.""
客人们在卡罗利娜·埃凯家里,举止就文雅一些,因为卡罗利娜的母亲治家很严厉。
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Designed by French fashion house Herm è s, this elegant uniform was manufactured in our home, Hong Kong, and was the first without a hat.
由著名品牌 Herm è s 设计,这件高贵的制服是香港本土制造,是我们第一套不配帽子的制服。
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Do not 'inflate' your achievements and/or qualifications or skills .
不要 '夸大' 你的业绩或成果,条件或者技能。