有反应

The 3,4-dimethoxybenzene was nitrated by mixed acid of HNO3-H2SO4 under the reaction temperature of 0~5℃. 3,4-dimethoxynitroben-zene was obtained by filtration, and its yield reached over 97%.

在0~5℃低温条件下，以硝酸和硫酸按比例配成的混酸进行硝化，反应结束后过滤得到3，4-二甲氧基硝基苯，该步反应的收率有97%。

The conducting wall in micro-tube preheats the inlet mixture by axial heat transfer. The existence of conducting wall will help to reach full reaction in the micro-tube. As the inlet velocity increases, both the existence of the surface catalytic combustion and the gas phase combustion become the limiting factors on combustion. Wall material and equivalence ratio of hydrogen/air mixture have important influence on catalytic combustion of hydrogen.

计算结果表明：表面催化反应对空间气相反应有抑制作用；在微型管道内，通过导热壁轴向间的传热，预热入口混合气体，使氢气燃烧更加充分；随着入口速度的增大，燃烧过程同时存在着表面催化反应和空间气相反应两种控制因素；管壁材料和当量比对氢气的催化燃烧过程有重要的影响。

Firstly, brand image and brand relationship were redefined and redivided. Moreover, the brand relationship scale in this thesis was redesigned. Secondly, the relationship between brand image, brand relationship and consumer response was examined, which is inadequate in former theories. Finally, this thesis employed an empirical research to test some propositions

本研究主要可能有以下一些创新：对品牌形象、品牌关系重新进行了界定，对其维度和类型进行了划分，并对品牌关系类型量表设计做了一些尝试和努力；对品牌形象、品牌关系和消费者反应之间的关联性进行了深入探讨；对品牌形象、品牌关系和消费者反应三者之间的联系进行了实证研究。

The results show that the sulfurized products have great oxidation tendency. With the increase of sulfidation temperature, sulfidation time and air speed, the oxidation tendency increase. And the existence of water has remarkable influence on the oxidation tendency of sulfurized products.

结果表明，干燥的H2S气体能和铁的氧化物发生硫化反应，硫化产物有较高的氧化自燃性，水浴温度高，硫化反应时间长，氧化时空气流速快以及水分的存在能明显加大自燃性。

The models of the ear swilling of mice and paw edema of rats were adopted to assay anti-inflammatory effect. Results 5-ASA(ig,75,150 and 300 mg.kg-1,for 3 d)significantly reduced the ear swelling of mice and the paw edema of rats and also decreased the writhing. 5-ASA at the dose of 300 mg.kg-1 ig,prolonged pain latency on hot-plate reaction.

结果 5-ASA片剂3种剂量(75、150及300 mg.kg-1，ig×3 d)对二甲苯诱导的小鼠耳肿胀度及蛋清诱导的大鼠踝关节肿胀度均有明显抑制作用；以上剂量还可明显抑制小鼠扭体反应，大剂量还可延长小鼠热板的舔足反应潜伏期。

Positive staining of oxytocin and vasopressin were in the cytosol of the neurons and the former gave less intensity,many positive varicosities for vasopressin were also noticed in neurite.

催产素的免疫阳性产物主要在细胞核周围的胞浆即核周质内，而加压素的免疫阳性物质除了在核周质内有很强的反应外，在突起内也可见很强的免疫反应。

The results showed that Kaidimycin was chemically neutral, macrocylic polylactones, stable and liable to dissolve into water and pyridine, slight to dissolve into methanol, ethanol and N-butanol, difficult to dissolve into ethyl acetate, acetone, benzene and chloroform. Chemical reaction of functional group of Kaidimycin showed that it had glycoside, amino acid and aldehyde, no reducing sugar, polypeptide and phenol.

凯地菌素属中等极性的、中性抗生素，极性纸层析结果与多烯类抗生素的纸层析结果相似：易溶于水、吡啶，微溶于甲醇、乙醇、正丁醇，不溶于乙酸乙酯、丙酮、苯、三氯化碳；对高温、光照和紫外处理有很好的稳定性；官能团反应试验结果发现，凯地菌素可能含有糖苷键、氨基酸伯氨基和醛基，不含有还原糖、多肽和酚基，高锰酸钾、浓硫酸反应与多烯大环内酯类抗生素的特性相似；并且依据纯品，采用生物法和分光光度法对摇床发酵液进行了效价的测定。

In order to study the aldol condensation of 2.15-hexadecanedione on the surface of aluminium, the intermolecular condensation mechanism of acetone occurring on aluminum was simulated by using semi-empirical AM1 method embodied in MOPAC 6.0 program package. The optimized structures and geometry parameters of 5 transition complexes and 4 intermediates were given.First, 2 molecules of acetone coordinated with aluminum by electrostatic attraction.One atom of hydrogen of acetone migrated to aluminum because of t...

为了研究2，15－十六烷二酮在氧化铝表面的环合机理，选择小分子丙酮为模型化合物，用量子化学半经验AM1方法研究双分子丙酮在氧化铝表面的醛醇缩合机理，给出了反应过程中的5个过渡态和4个中间体的结构和几何参数，该催化反应可以认为是氧化铝分子与两分子丙酮分子发生静电络合作用，然后借助氧原子的负电荷导致脱氢并实现缩合，根据中间体的能量变化，推测有较稳定的铝复合物生成。

The main species of the antimony catalysts are antimony trioxide, antimony acetate and the recent widely concerned ethylene glycol antimony.

此外，用于酯交换反应的锰、锌、钙、钴、铅等金属的醋酸盐对缩聚反应也有一定的催化作用。

When diaryl ketones were treated in DMF promoted by samarium metal with TMSCl as activator, diaryl ketones react with DMF followed by a carbene rearrangement to afford benzoins unexpectedly, with benzils were obtained as byproducts, the formation of which may be explained as a result arising from the auto-oxidation of benzoins. Further investigation found the reaction could also proceed smoothly when I〓 was used as an activator. The reaction could occur as well in SmI〓/THF, though benzoins were obtained in relatively low yields.

发现当有活化剂TMSCl存在时，金属钐能有效的促进二芳酮和DMF的发生反应，偶联后发生卡宾重排，意外地得到苯偶姻类化合物，同时伴随着少量的二芳基二酮副产物生成，我们推测二芳基二酮的生成可能从苯偶姻的自氧化而来；进一步的研究表明，用一定量的I〓活化金属钐，该反应也可以顺利的进行，并且可以得到相对更好的实验结果。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。