有反应

During these years (1997-2000) in the research area of annonaceous acetogenins 5 natural products and a number of chiral-pure analogs of annonaceous acetogenins have been synthesized using sugars as the starting materials. Their high activity and selectivity against cell line of colon tumor and a relationship between activity and configuration have been found too. In the respect of inhibitor of sialidase two new methodologies for the synthesis of chiral-pure 3-deoxy-ulosonic acid using hetero-Diels-Alder reaction or asymmetric propargylation as the key reaction were developed. On the topic of anti-leukemia marine natural product clavulactone a synthetic method based on the free radical cyclization and starting from sugar has been developed. In other title of PKC inhibited agent sphingosine a new synthetic route with SN2' as the key reaction has also been disclosed.

项目期间（1997-2000）在番荔枝内酯方面从糖出发合成了五个天然产物和一批手性纯的类似物，它们对肠癌细胞有很高的活性和选择性，并与构型有关；在唾液酸酶抑制剂方面发展了二类全新手性纯高碳糖的合成方法－杂原子D－A反应或丙炔基不对称加成为关键的反应；抗白血病海洋天然产物群柱虫内酯方面研究了由糖出发和自由基环化反应的合成方法；对PKC 起抑制作用的鞘氨醇方面也开创了新的合成途径－由糖出发并以SN2'反应为关键反应。

At first in the preliminary design this paper computes the linear damping coefficient of the viscous damper employed in this project using Composite Response Spectra approach, meantime, this paper proves that reducing the exponent of velocity of the piston can increase the magnitude of the dissipative energy, because of the viscous damper employed in the practical project character nonlinear behavior; next this chapter performs analysis and comparison between the building without and with the viscous dampers aforementioned when the building suffers from various Time Domain Response, from the angle of displacement, interstroy drift, velocity, interstory velocity, acceleration, energy, maximum axial force of the dampers and of the column etc., in order to prove that the incorporating the viscous dampers into the buildings has great superiority on enhancing its aseismic performance ; furthermore, this chapter also expatiates on diverse assembly form of the viscous dampers that results in the adverse impact on the internal force of the structural member in this building, on the ground of which this segment bring about the preference of the assembly form of the viscous damper; finally this chapter points out the sphere of application of the analysis and computation using Composite Response Spectra approach in design: it is available in well-proportioned stiffness structures and isn抰 available in the structures that contain weak story. It is recommendable, particularly, to incorporate the fluid viscous dampers into this structure that contain weak story to refrain earthquake and reinforce, such as the Central Hall of Shanghai Exhibition Hall.

首先使用了反应谱分析法设计出欲附设的粘滞阻尼器的线性阻尼系数，由于实际工程所用的粘滞阻尼器具有非线性的特性，故而笔者又证明了降低速度指数对提高粘滞阻尼器的耗能量的优势所在；接着分别从位移、层间位移、速度、层间速度、加速度、能量、最大阻尼出力和柱轴力等不同的角度对结构在附设粘滞阻尼器前后的时程反应进行了分析对比，籍此在实际工程中证明了附设粘滞阻尼器对于提高结构的抗震性能的优越性；再者，笔者还阐述了采用不同的粘滞阻尼器布置方式对结构中构件内力特别是柱轴力和基座竖向反力产生的不利影响，并在此基础上提出了布置方式的优选；最后，指出了反应谱法在设计中的适用范围：对于均匀结构反应谱法能够使用，而对于含有薄弱层的结构反应谱法并不适用；对于类似于上海展览馆中央大厅的含薄弱层的结构尤其值得使用粘滞阻尼器的方法进行抗震加固。

The result of study was showed that the reaction of curing included BMI auto polymerization, BCE since auto polymerization, BCE copolymerizing with BMI, BCE with EP copolymerize reacting etc. The mechanical performance of the modified resin systems all increased in various degrees, however, electric performance and heat-resistance performance all dropped to some extent.

研究结果表明，体系的固化反应包含BMI自聚合反应、BCE自聚合反应、BCE与BMI共聚反应、BCE与EP共聚反应等，改性后树脂体系的力学性能都有不同程度的增加，而电学性能和热性能则都有所下降。

This paperindicated that it was good for condensation reaction when benzene-ring bearingelectron-attaching groups. It also showed that and the 6-hydroxyl group could bereacted with acyl halide, haloid ether and halo alkene, but not with halo alkane. It wasnot only the first time to find that the reaction product of D-mannitol and aromaticaldehyde is tri-condensation derivatives, but also the first time to obtain thep-phthaldehyde-sorbitol derivatives containing eight hydroxyl groups.

研究发现：苯环上有吸电子基团时对缩合反应有利；多元醇缩醛衍生物6-羟基除与酰氯反应外，也能和卤代酸酯、溴代烯反应，但不与卤代烷反应；首次发现D-甘露醇与醛反应主要得到三缩合物；首次合成了含有8个羟基的对苯二甲醛和山梨醇的缩合物。

The incidence of nausea and vomiting, dizziness in aripiprazole group were significantly different form risperidone group (x2=20.397,p.001; x2=10.557,p.01), but that of menoxenia, eps and increasing in weight in aripiprazole group were lower than in risperidone (x2=11.81-102.29,p.05), the other side effects were not significantly different.conclusions: aripiprazole difference from risperidone is in side effects, but not in therapeutic effects.

阿立哌唑组的恶心呕吐、头晕头昏不良反应比利培酮组多，差异具有显著性（x2=20.397，p.05；x2=10.557，p.05），利培酮组的月经紊乱、体重增加、锥体外系反应等不良反应均比阿立哌唑组多，差异具有显著性（x2=11.81-102.29， p均。05），其余不良反应均无显著性差异。结论：虽然阿立哌唑与利培酮在平均8周左右的疗效无显著性差异，但不良反应却有显著不同。

The nitrogen content in the product is affected by temperature, which is unfavorable in carbonthermic reduction and nitridation if it is over or below to 1420℃.

反应温度对产物的氮含量有重要影响，对于碳热还原氮化反应，过低或过高的温度都不利于反应进行，较适宜的温度为1420℃；而铝热还原氮化反应中，升温有利于提高反应速度，较适宜的温度为1460℃。

In range of 300℃～900℃, all the transition metal oxide catalysts could get high ammonia conversion, during the initial stages of the reaction, the SO〓 conversion is relatively low since the catalysts have not been sulfureted, but it increases gradually and attain constant with rising temperature and time continuance,〓 is better than other catalysts in reactivity and elemental sulfur selectivity; XRD indicates that, in the SO〓-SCR process, stable transition metal sulfide is generated which is very important to SO〓 reduction and transition metal sulfide probably is the active phase of catalyst, further the reduction of SO〓 by H〓 to H〓S is the limiting step of all process, then the activity is somewhat related to its lattice oxygen yet not so notable; XPS indicates that little sulfur on surface exists as S〓 in sulfate, showing that TiO〓 could restrain the generation of sulfate.

对于过渡金属氧化物催化剂的研究发现，在300℃～900℃范围内，不同的催化剂均可获得很高的NH〓转化率，反应初期由于催化剂还未硫化，所以SO〓的转化率较低，随着温度升高和反应时间的延续，SO〓的转化率逐渐升高并达到了稳定值；七种过渡金属氧化物中，以〓对于NH〓还原SO〓反应的活性和选择性最好；XRD结果表明在NH〓-SO〓反应后生成了稳定的硫化物相，硫化物对SO〓的还原过程具有重要作用，催化剂的活性相可能是过渡金属硫化物，而且在硫化物催化剂上进行的H〓还原SO〓生成H〓S的反应是整个过程的速率控制步骤，所以催化剂的活性与其自身的晶格氧的氧化还原能力有一定的联系，但关系不明显；XPS结果表明催化剂表面的硫大部分以过渡金属硫化物的形式存在，只生成少量的S〓，说明TiO〓催化剂能够较好的抑制硫酸盐的生成。

The progress levels of symptoms after pathogen infection showed that interaction of gray leaf spot pathogen and host has differentiation or polymorphism. The progress levels of symptoms is different.The aggressively has polymorphism. The pathogenicity of different isolates in same cultivar has polymorphism, or the host reaction type of same isolate in different cultivars has polymorphism.The host reaction type has differentiation. There are seven types of host reaction in cultivar and inbred after infected by GLS pathogen:Rectangular lesion without chlorotic halo, Rectangular lesion with chlorotic halo,Irregular lesion without chlorotic halo,Irregular lesion with chlorotic halo, Spot lesion with chlorotic halo,Rectangular and irregular lesionand Rectangular and spot lesion. The host reaction type is coalesced lesion when disease severely. Frequency of each reaction types is different.

通过对玉米灰斑病菌侵染后的显症过程的系统观察，可在组织水平上说明该病菌与寄主互作反应存在分化或多样性：玉米灰斑病菌不同菌株侵染后显症过程表现出明显的差异；玉米灰斑病菌在侵袭力上存在多样性，菌株间对同一种品种的致病性表现多样化，或者同一菌株对不同品种侵染引起的寄主反应表现为多样性；病斑反应型的分化，玉米灰斑病菌侵染玉米品种或自交系后，主要有7种病斑反应类型，即RH型、RN型、IRH型(不规则形具褪绿晕圈病斑)、IRN型(不规则形无褪绿晕圈病斑)、SH型、RI型(长矩形与不规则形混合病斑)和RS型(长矩形与斑点形混合病斑)，若发病严重，病斑连成片，而且这些反应类型出现的频率也不同。

Although many researchers have studied the synthesis of allyl phenyl ether by phase-transfer catalysis, no studies have used it in membrane reactor up to now. The purpose of this paper is to combine the studies of membrane reactor and phase-transfer catalysis. The membrane was used to stabilize the aqueous/organic interface at a fixed position, also the quaternary ammonium ion in the membrane was used as the catalyst to partake in the reaction system directly, and so it can also separate the product and reactants at the same time. A theoretical model is also presented.

中文摘要对於利用相间转移触媒催化技术来合成丙烯基苯基醚的反应，已有不少专家学者研究过，而至今还无在薄膜反应器中进行此反应之研究，本研究则是要结合薄膜反应器与相间转移触媒两者之特性，固定水油两相之界面，并且利用薄膜上的四级铵离子为触媒，直接在反应系统中参与反应，并同时分离产物及反应物，进而推导出相关之理论模型。

When surface of TiO2 powder is enveloped by carbon, the reduction is mainly solid-solid reaction between carbon and titanic oxide.

结果表明钛氧化物的还原是逐级进行的，反应过程伴随着相变，当TiO2粉末和C粉末均匀混合时还原碳化反应主要依赖于CO／CO2传质的气固反应，当TiO2颗粒表面被C包膜时主要是碳和钛氧化物之间的固固反应，当TiO2粉末和C粉末混合压球时则两种反应机理均有。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。