最高

Dealcoholization temperature markedly influences the surface area and porosity of the resultant MAO-supports. When the support was pretreated at lower or higher temperature, the corresponding MAO-support shows very low surface area;2.XRD and IR analyses indicate that MAO has reacted with the residual ethanol in the supports, which is an important manner to get MAO fixed on the carrier. Morever, XPS analyse indicates that MAO can also be coordinated with MgCl_2, which is another way to get MAO fixed on the support;3.ICP and EDX analyses indicate that dealcoholization temperature not only determined the element content on the solid catalyst, but also influences the element distribution on the carrier;4.The activities of the supported phenoxy-imine catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature. The support (MSP-5) obtained by treating MgCl_2·2.56C_2H_5OH at 160℃for 4 h, then modified by MAO is very effective for immobilizing complex 3, the resultant solid catalyst (MSPC-5) shows very high activity in ethylene polymerization, and its kinetics of polymerization is stable during the reaction process. Finally, PEs with spherical morphology and high bulk density (over 0.35g/ml) were obtained, without reactor fouling;5.In this work, polymerization conditions such as alkylaluminums, Al/Zr ratio, temperature and H_2 had a pronounced effect on the activity of MSPC-5 and properties of PE;(3). New MgCl_2-Supported Single-Site Catalysts for Ethylene PolymerizationIn this work, a kind of new MgCl_2 support was obtained by anhydrous MgCl_2 co-milled with solid MAO, and it is a creative contribution. Then some single-site catalysts were supported on the new MgCl_2 support, and the resulted solid catalysts were tested in ethylene polymerization, the results indicated that:1.XRD and IR analyses indicate that MAO does be coordinated with MgCl_2, which is in good agreement with the results obtained by XPS;2.co-mlling time had no obvious effect on the texture of support after 12 hours;3.In this work, MgCl_2 was co-milled with solid MAO for different hours, and then complex 3 was supported on these co-milled supports. It was found that co-milling time markedly influences the activity of solid catalysts, but it had negligible effect on the kinetic profile and the properties of resultant PE.

XPS研究结果表明，MAO不仅仅只和乙醇作用，MAO还与MgCl_2本身有一定的作用，这是一个极为重要的发现；3、通过ICP和EDX表征，发现载体的脱醇温度直接影响着元素在固体催化剂中的含量及分布；4、脱醇温度极大地影响着负载苯氧基亚胺类催化剂的活性和聚合物的性能，特别是原始载体经160℃活化4小时制备得到的固体催化剂MSPC-5的活性明显高于其他脱醇温度条件下制得的固体催化，并且催化剂寿命长，表现出稳定的动力学行为，最终获得了高堆密度(大于0.35g／ml)的球形聚乙烯颗粒；5、本文选择MSPC-5为研究对象，考察了聚合反应参数对催化剂的活性及其聚合物的影响，研究发现：不同的烷基铝对催化剂具有非常重要的影响，特别足TIBA对MSPC-5的助催化活性最高，烷基铝的加入量有一个较佳值，聚合温度为80度时活性最高，H_2的加入使催化剂的活性明显降低且聚合物的分子量也减小；、新型氯化镁载体负载单活性中心催化剂催化乙烯聚合本文创造性采用固体MAO与无水氯化镁直接进行共研磨，制备出了一种的新型的氯化镁载体，并将该载体用于多种单活性中心催化剂的负载化研究，研究表明：1、通过BET、XRD的表征，再次证实了MAO与MgCl_2之间具有直接作用，与XPS的研究结果相一致；2、当研磨时间高于12小时时，延长研磨时间对载体的结构没有显著的影响；3、将配合物3负载于共研磨时间不同的一系列载体上，乙烯聚合结果表明，尽管共研磨时间对负载催化剂的活性具有明显的影响，但是它对聚合物的性能以及催化剂的影响不明显。

Dealcoholization temperature markedly influences the surface area and porosity of the resultant MAO-supports. When the support was pretreated at lower or higher temperature, the corresponding MAO-support shows very low surface area; 2.XRD and IR analyses indicate that MAO has reacted with the residual ethanol in the supports, which is an important manner to get MAO fixed on the carrier. Morever, XPS analyse indicates that MAO can also be coordinated with MgCl_2, which is another way to get MAO fixed on the support; 3.ICP and EDX analyses indicate that dealcoholization temperature not only determined the element content on the solid catalyst, but also influences the element distribution on the carrier; 4.The activities of the supported phenoxy-imine catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature. The support (MSP-5) obtained by treating MgCl_2·2.56C_2H_5OH at 160℃for 4 h, then modified by MAO is very effective for immobilizing complex 3, the resultant solid catalyst (MSPC-5) shows very high activity in ethylene polymerization, and its kinetics of polymerization is stable during the reaction process. Finally, PEs with spherical morphology and high bulk density (over 0.35g/ml) were obtained, without reactor fouling; 5.In this work, polymerization conditions such as alkylaluminums, Al/Zr ratio, temperature and H_2 had a pronounced effect on the activity of MSPC-5 and properties of PE;(3). New MgCl_2-Supported Single-Site Catalysts for Ethylene Polymerization In this work, a kind of new MgCl_2 support was obtained by anhydrous MgCl_2 co-milled with solid MAO, and it is a creative contribution. Then some single-site catalysts were supported on the new MgCl_2 support, and the resulted solid catalysts were tested in ethylene polymerization, the results indicated that: 1.XRD and IR analyses indicate that MAO does be coordinated with MgCl_2, which is in good agreement with the results obtained by XPS; 2.co-mlling time had no obvious effect on the texture of support after 12 hours; 3.In this work, MgCl_2 was co-milled with solid MAO for different hours, and then complex 3 was supported on these co-milled supports. It was found that co-milling time markedly influences the activity of solid catalysts, but it had negligible effect on the kinetic profile and the properties of resultant PE.

XPS研究结果表明，MAO不仅仅只和乙醇作用，MAO还与MgCl_2本身有一定的作用，这是一个极为重要的发现； 3、通过ICP和EDX表征，发现载体的脱醇温度直接影响着元素在固体催化剂中的含量及分布； 4、脱醇温度极大地影响着负载苯氧基亚胺类催化剂的活性和聚合物的性能，特别是原始载体经160℃活化4小时制备得到的固体催化剂MSPC-5的活性明显高于其他脱醇温度条件下制得的固体催化，并且催化剂寿命长，表现出稳定的动力学行为，最终获得了高堆密度(大于0.35g／ml)的球形聚乙烯颗粒； 5、本文选择MSPC-5为研究对象，考察了聚合反应参数对催化剂的活性及其聚合物的影响，研究发现：不同的烷基铝对催化剂具有非常重要的影响，特别足TIBA对MSPC-5的助催化活性最高，烷基铝的加入量有一个较佳值，聚合温度为80度时活性最高，H_2的加入使催化剂的活性明显降低且聚合物的分子量也减小；、新型氯化镁载体负载单活性中心催化剂催化乙烯聚合本文创造性采用固体MAO与无水氯化镁直接进行共研磨，制备出了一种的新型的氯化镁载体，并将该载体用于多种单活性中心催化剂的负载化研究，研究表明： 1、通过BET、XRD的表征，再次证实了MAO与MgCl_2之间具有直接作用，与XPS的研究结果相一致； 2、当研磨时间高于12小时时，延长研磨时间对载体的结构没有显著的影响； 3、将配合物3负载于共研磨时间不同的一系列载体上，乙烯聚合结果表明，尽管共研磨时间对负载催化剂的活性具有明显的影响，但是它对聚合物的性能以及催化剂的影响不明显。

We can conclude that extraction can enhance tomato disease-resisting abilities. By studied on Dictarnnus dasycarps Turcz. antifeeding activity to Ostrinia furnacalis, Dictamnus dasycarps Turcz.

在处理浓度中，0.1g／ml的提取液对番茄叶片的诱导活性最好，用该浓度处理番茄叶片：6h后其PAL的OD值最高，为对照的2倍；4h后POD的OD值达到最高，为对照的1.5倍。

Dictamnus dasycarps Turcz. also have insecticidal activity to Ostrinia furnacalis, When the concentration was 10g/ml, correct decreased rate reached 92.86%, When the concentration was 0.675ml/g, the correct decreased rate reached 3.57%; Dictamnus dasycarps Turcz. at the range of testing concentration have lower stomach toxic effects to Ostrinia furnacalis.

通过白鲜皮对玉米螟杀虫活性的初步研究表明：白鲜皮对玉米螟表现出很强的拒食活性，在测定浓度范围内其拒食活性均在80％以上，最高可达97.22％。；白鲜皮提取液对玉米螟也有一定的毒杀活性，当浓度为10g／ml时其校正死亡率可达到92.86％，浓度为0.675ml／g时校正死亡率仅为3.57％；白鲜皮在测定浓度范围内对玉米螟的胃毒活性较低，最高才42.86％。

This is not surprising, given the closer proximity of Pengyang to the Asian inland dust sources; The average content of calcium carbonateis of Pengyang section is not only higher than that of central loess plateau, but also higher the west of Chinese Loess Plateau, which reflected Pengyang loess had been deposited by near Liupanshan\'s substances that contained more calcium carbonateis; The content of diffluent element of 10m depth in the section increased fast, which indicated that the modern eluviation and the leaching depth of loess may be stronger than our guess; The soil growth index can reflect the intensity of soil forming and the climatic changes; The "abrupt chang" of glacial and interglacial period was caused by strong soil-forming processes that enlarged the discrepancy of granularity between loess and paleosol. However, the magnetic susceptibility nearly cannot reflect the existence of S_8 and the magnetic susceptibility of S_7 is highest in the whole section, which is inconsistent with other studies that S_5 has the highest magnetic susceptibility.Thin-section examination shows that the micro-texture of the soil layers is divided into both cementing texture in S_7, S_5 and S_1, and granular texture in all others.

与其它剖面相比，彭阳剖面粒度总体上要比东部的洛川、西安，甚至西部的兰州、新疆东湾要粗；CaCO_3平均含量不仅高于黄土高原中部，也高于高原西部，反映出本剖面富含碳酸盐的六盘山近源沉积起到了很重要的作用；易溶元素含量在剖面10m处快速升高，淀积特征明显，反映出黄土受现代淋溶成土作用影响较大，黄土直立、疏松、多孔特性和高温与多雨组合的气候特点，使得元素淋溶、淀积的强度和深度超出了传统的认识和判断；烧失量与其它指标相比，不仅能区分冰期、间冰期；而且能够区分出次一级的冰阶、间冰阶，有较高的分辨率；土壤发育指数、红度能够反映土壤强度差异，是反映气候波动的较好指标；然而，磁化率不能反映古土壤S_8的存在，且S_7的磁化率在全剖面中最高，这与大多剖面S_5磁化率最高的特点不一致。4。

Ten contamination features are extracted from the contaminated insulator infrared image,viz.the highest , the lowest , the mean temperature of the background, the temperature variance of the background ,the highest ,the lowest ,the mean temperature of the contaminated insulator discal surface , the temperature variance of the insulator discal surface ,the maximum and the mean temperature increase of the discal surface contrasting to the mean temperature of the background .

本文研究从分割后的污秽绝缘子盘面图像中提取了10维原始污秽特征，即：绝缘子红外热像背景的最高温度、最低温度、平均温度、背景温度分布的方差值、盘面图像的最高温度、最低温度、平均温度、盘面温度分布的方差值、盘面温度的最大温升、盘面温度的平均温升。

Results The dermatophagoides farinae and pteronyssinus (62/118) were the most common allergen in inhalation group in 118 patients with allergic disease. Dogly or feline scurf was the next (35/118), then were ambrosia artemisiiofolia and muguort (14/118), cockroach(12/118), cypress, elm, Surname. Cottenuood (8/118), humulus scandens (7/118), polyvalent fungus(6/118). In food group the most common allergen was mutton or beef (13/118), then was cashew, peanut, soybean (11/118), wheat (10/118),milk (9/118), fish, shrimp, crab(5/118), mango(4/118),egg, chicken., yolk(1/118).The positive rates of total IgE level was 35.59%.

结果 118例变应性鼻炎患者中吸入组过敏原以以屋尘螨粉、尘螨(62/118)为最高，其后依次为猫毛皮屑、狗毛皮屑(35/118)、矮豚草、蒿(14/118)、蟑螂(12/118)、柏榆、梧桐、柳三角叶杨(8/118)、律草(7/118)、点青霉、分枝孢霉、烟曲霉、交链孢霉(6/118)；食入组过敏原以牛肉、羊肉(13/118)为最高，其后依次为腰果、花生、黄豆(11/118)、小麦(10/118)、牛奶(9/118)、鱼虾蟹(5/118)、芒果(4/118)、鸡蛋白、鸡蛋黄(1/118)；总IgE阳性率为35.59%。

The chemical weathering index, K/Na ratio, eluvial coefficientand A-CN-K diagram , can availably indicate the evolution of pedogenic environment. The A-CN-K and CIA-K/Na diagram showed that the Holocene paleosol was in the primary stage of weathering, which K-feldspar went through weak weathering and K was less leached with much leach of Ca and Na. The intensity of weathering went stronger gradually from west to east in the Weihe Valley.

对化学风化指数、K/Na比值、残积系数等化学综合参数的研究结果显示，各项地球化学参数可有效指示成壤环境与成壤强度；从A-CN-K风化趋势图和CIA-K/Na比较图中可知，渭河流域三个剖面风化程度最高的全新世古土壤基本处于同一风化阶段，即脱Ca、Na，尚未到达脱K的阶段，还是风化较弱的初级阶段，但三者的风化程度是存在差异的，风化程度XJN剖面最低，JYC-N剖面最高，ETC剖面介于其中，说明渭河流域自西北向东南风化程度逐渐增强。

Experiments showed that the contents of putrescine、spermidineand sperminein normal ovules were higher than those inabortive ones during the whole embryogenetic process.The highest levelswere reached 7 days after anthesis,with Put being the richest of thethree,then they declined.

试验结果表明：正常发育的胚珠中腐胺、亚精胺和精胺的含量在胚胎发育的各个阶段均高于败育胚珠，并在花后7d即达到最高值，其中Put的含量最高，随后都呈下降趋势。

Results showed that optimal conditions for high content of ergothioneine were moisture content at 40%, temperature at 30℃and polished adlay as medium, cubation 17 days (574.0 mg/kg dw), biomass was 139.0 mg/g dw.

经探讨后，以含水量40%之薏仁於30 ℃下培养17天后之麦角硫因量最高，可达574.0 mg/kg dw，再添加酵母萃取物为氮源可提高麦角硫因到824.8 mg/kg dw，生物质为139.0 mg/g dw；以含水量45%之荞麦於30 ℃下培养17天后之麦角硫因含量最高，可达580.6 mg/kg dw，生物质为163.4 mg/g dw，添加酵母萃取物为氮源，麦角硫因含量可达651.6 mg/kg dw。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。